Light Control Particle Manufacturing via Methanol Granulation

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Solution Overview

Problem

The existing methods for manufacturing light control particles face challenges in achieving optimal particle size and shape due to the sensitivity of water content, making it difficult to reproduce light control particles with desired properties for industrial applications.

Innovation Solution

Incorporating methanol in a specified amount during the granulating step of the manufacturing process, alongside elemental molecular iodine, an alkaline earth metal iodide, and a heterocyclic compound, helps reduce the effect of water on particle size and shape, ensuring reproducibility and optimal properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If water content is strictly controlled in the reaction system, then light control particles with optimal particle size and shape can be obtained, but the manufacturing process becomes difficult to implement in mass production due to the narrow permissible range and difficulty in adjusting water amount

Engineering Contradiction:
Improveparticle size and shape controlVSAvoidindustrial applicability
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The patent introduces a surfactant as an intermediary substance that mediates between water and the reaction components. The surfactant allows water to be present in the reaction system without adversely affecting particle size and shape, thereby enabling easier manufacturing while maintaining precision. The surfactant concentration is controlled within specific ranges (0.1-10 wt% relative to water, or 0.01-5 wt% relative to total reaction mixture) to achieve optimal results.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If the amount of water is precisely measured and adjusted, then reproducible light control particles can be manufactured, but the process complexity and difficulty increase significantly

Engineering Contradiction:
ImprovereproducibilityVSAvoidprocess complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The surfactant serves as a mediator that eliminates the need for precise water measurement and adjustment. By adding the surfactant, the system becomes tolerant to variations in water content, thereby maintaining reproducibility without increasing process complexity. The surfactant effectively buffers the system against water content fluctuations.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Manufacturing precision

If water amount is varied to optimize particle properties, then particle size and shape can be adjusted, but the narrow permissible range makes it impractical for industrial production

Engineering Contradiction:
Improveparticle properties optimizationVSAvoidmass production capability
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The surfactant enables mass production by decoupling particle property optimization from strict water content control. With the surfactant present, a broader range of water amounts can be used while maintaining optimal particle properties, thereby enabling scalable industrial production without sacrificing manufacturing precision.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach allows for the stable production of light control particles with desired dimensions and shape, enhancing the reproducibility and industrial applicability of the manufacturing method.

Implementation Method 1

Incorporating methanol in a specified amount during the granulating step of the manufacturing process, alongside elemental molecular iodine, an alkaline earth metal iodide, and a heterocyclic compound, helps reduce the effect of water on particle size and shape

Methodology Applied
Scientific EffectSolvation: Solvation

Implementation Method 2

The light control particles in the light control film undergo Brownian movement in the state that no electric field is applied thereto, thereby adsorbing, scattering or reflecting light

Methodology Applied
Scientific EffectBrownian motion: Brownian Motion

Implementation Method 3

When an electric field is applied thereto, the light control particles are polarized, thereby being arranged in directions parallel to each other in accordance with the electric field

Methodology Applied
Scientific EffectPolarization: Polarisation

Data Source

PatentUS8520294B2Method for manufacturing light control particles and light control film using light control particles obtained by the method
Publication Date: 2013.08.27 GAUZY
  • US8520294B2 patent drawing
  • US8520294B2 patent drawing
  • US8520294B2 patent drawing

AI summary

Disclosed is a method for manufacturing light control particles usable for a light control material comprising:a resin matrix made from a polymeric medium that is cured by irradiating with an energy beam; anda light control suspension comprising: a dispersing medium; and the light control particles that are dispersed in the dispersing medium so as to be in a flowing state,the method comprising the step of granulating after mixing elemental molecular iodine (A), an alkaline earth metal iodide (B), and a heterocyclic compound (C) with each other in a medium,wherein in the step of granulating, reaction is carried out in the presence of methanol in an amount of not less than 50 parts by mass but not more than 110 parts by mass relative to 100 parts by mass of the whole of components (A), (B) and (C). In this way, it is possible to provide a method for manufacturing light control particles wherein the effect of water is decreased in a granulating step of the method in order to yield effectively light control particles having a particle size and shape optimal for light control material and further a good reproducibility is attained.