Dry Analytical Element for Pancreatic Lipase Using Alkylarylsulfonate Surfactants

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Solution Overview

Problem

Current dry analytical elements for pancreatic lipase analysis have low selectivity and multianalyte correlation, making them inadequate for reliable diagnosis of pancreatic diseases, and existing methods face challenges in maintaining substrate dispersion and particle size uniformity, leading to reduced reaction rates and increased environmental impact.

Innovation Solution

A dry analytical element comprising long-chain fatty acid glyceride, monoglyceride lipase, and a glycerine measurement reagent, with two or more anionic surfactants, specifically alkylarylsulfonates, to enhance pancreatic lipase selectivity and multianalyte correlation, using a water-impermeable support and layers of reagents and development materials like porous membranes and fabrics.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If long-chain fatty acid glyceride is used as substrate for pancreatic lipase measurement, then selectivity for pancreatic lipase is improved, but substrate dispersion and particle size uniformity deteriorate

Engineering Contradiction:
Improveselectivity for pancreatic lipaseVSAvoidsubstrate dispersion and particle size uniformity
Core Design Contradiction:
Measurement precisionVSStability of the object's composition

Solution Approach 1:

The patent introduces a protective colloid as an intermediary substance to stabilize the dispersion of long-chain fatty acid glyceride substrate. The protective colloid prevents substrate aggregation and maintains uniform particle size distribution, resolving the contradiction between achieving high selectivity through long-chain substrate use and maintaining stable dispersion characteristics.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Stability of the object's composition

If surfactant or protective colloid is used to disperse substrate, then substrate dispersion is improved, but environmental burden increases

Engineering Contradiction:
Improvesubstrate dispersionVSAvoidenvironmental burden
Core Design Contradiction:
Stability of the object's compositionVSObject-affected harmful factors

Solution Approach 1:

The patent employs a protective colloid that can be easily degraded and has minimal environmental impact, replacing conventional surfactants that persist in the environment. This approach maintains effective substrate dispersion while significantly reducing environmental burden through the use of biodegradable materials.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

3Stability of the object's composition

If triolein is emulsified and dispersed using ultrasound, then initial dispersion is improved, but aggregation occurs during drying and storage

Engineering Contradiction:
Improveinitial dispersionVSAvoiddispersion stability over time
Core Design Contradiction:
Stability of the object's compositionVSDuration of action of stationary object

Solution Approach 1:

The patent applies preliminary action by incorporating the protective colloid into the substrate dispersion process before drying and storage. This pre-protection prevents aggregation from occurring in the first place during subsequent processing and storage, rather than attempting to restore dispersion after aggregation has occurred.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent utilizes parameter changes by optimizing the concentration and type of protective colloid to maintain dispersion stability across varying conditions of drying and storage. By adjusting the protective colloid parameters, the system maintains stable dispersion without aggregation over extended periods.

Inventive Principle:
Principle #35Parameter changes

4Stability of the object's composition

If decrease in oil-water interface surface area occurs, then substrate stability is improved, but reaction rate decreases

Engineering Contradiction:
Improvesubstrate stabilityVSAvoidreaction rate
Core Design Contradiction:
Stability of the object's compositionVSProductivity

Solution Approach 1:

The patent employs parameter changes by optimizing the protective colloid concentration and substrate particle size distribution to maintain a large effective oil-water interface surface area while preventing aggregation. This allows the system to achieve both substrate stability and high reaction rate simultaneously through controlled parameter optimization.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution significantly improves the correlation coefficient of multianalyte correlation and lipase activity, providing higher specificity and accuracy in pancreatic lipase analysis without increasing colipase amounts, thus enhancing diagnostic reliability and reducing environmental impact.

Implementation Method 1

the development layer and/or the reagent layer comprise two or more anionic surfactants wherein at least one of the anionic surfactants is an alkylarylsulfonate

Methodology Applied
Scientific EffectSurfactant: Surfactant

Implementation Method 2

monoglyceride lipase, and a glycerine measurement reagent

Methodology Applied
Scientific EffectEnzyme: Enzyme

Implementation Method 3

using a water-impermeable support and layers of reagents and development materials like porous membranes and fabrics

Methodology Applied
Scientific EffectPorosity: Porosity

Data Source

PatentEP2003450B8Dry analytical element for pancreatic lipase measurement
Publication Date: 2014.02.26 FUJIFILM CORP

AI summary

It is an object of the present invention to provide a dry analytical element for pancreatic lipase analysis having high selectivity with respect to pancreatic lipase, whose multianalyte correlation has been improved. The present invention provides a dry analytical element for measurement of pancreatic lipase contained in a body fluid, which comprises at least one development layer and/or reagent layer containing diglyceride or triglyceride of long-chain alkyl fatty acid having 12 to 22 carbon atoms, monoglyceride lipase, and a glycerine measurement reagent, wherein the development layer and/or the reagent layer comprise two or more types of anionic surfactants and at least one type of the anionic surfactant is alkylarylsulfonate.