Lipid Purification via Thermal Settling and Filtration

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Solution Overview

Problem

Conventional methods are ineffective in purifying lipid materials with high impurity levels, making them unsuitable for use as fuel or chemical sources due to the inability to remove impurities to the required quality within a feasible timeframe.

Innovation Solution

A method involving storing lipid materials at elevated temperatures to settle impurities, separating the oily sludge phase, further processing, and optionally purifying it with heat treatment and solvent addition to remove impurities like polyethylene and phosphorus compounds, allowing for rapid purification and improved purity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional purification methods are used on lipid materials with high impurity levels, then the purification process becomes too lengthy and inefficient, but the impurities cannot be removed to the required quality standard

Engineering Contradiction:
Improvepurification qualityVSAvoidpurification time
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

The patent changes the temperature parameter during the purification process. By heating the lipid material to elevated temperatures (above the melting point but below degradation temperatures), the viscosity decreases and impurity separation becomes more efficient. This parameter change enables both high purification quality and reduced processing time, resolving the technical contradiction between purification quality and purification time.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs a composite approach by combining multiple purification techniques: settling tank separation, filtration through porous materials, and activated carbon treatment. This composite methodology achieves high purification quality (removing polyethylene, phosphorus compounds, and other impurities) while maintaining reasonable processing time by distributing the purification function across multiple mechanisms working in sequence.

Inventive Principle:
Principle #40Composite materials

2Manufacturing precision

If lipid materials with high impurity levels are used directly, then the material is unsuitable for fuel or chemical production, but conventional methods cannot remove impurities to the required quality

Engineering Contradiction:
Improveimpurity removal efficiencyVSAvoidprocessing efficiency
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The patent extracts impurities from the lipid material through a multi-stage process. First, impurities are allowed to settle in a settling tank where they separate by density. Then, the supernatant is filtered through porous materials and activated carbon to remove remaining impurities including polyethylene and phosphorus compounds. This extraction approach achieves high impurity removal efficiency (reaching fuel-quality standards) while maintaining processing efficiency through the systematic removal of different impurity types at each stage.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent introduces intermediary substances and processes to facilitate impurity removal. Activated carbon serves as an intermediary material that adsorbs organic impurities and colored substances. The settling tank acts as an intermediary separation zone where impurities can be removed before final filtration. These intermediaries enable high impurity removal efficiency without compromising processing efficiency, as they target specific impurity types selectively.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method significantly reduces purification time, achieving high impurity removal rates (up to 99% for polyethylene) and producing lipid materials suitable for use as fuels or chemicals, thereby overcoming the limitations of existing techniques.

Implementation Method 1

storing the lipid material in a settling tank at elevated temperature

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 2

allowing the impurities to settle to the bottom of the settling tank to thereby form an oily sludge phase

Methodology Applied
Scientific EffectSedimentation: Sedimentation

Implementation Method 3

said purifying step e) comprises a heat treatment step comprising the steps of: i. heating said oily sludge phase to a temperature of from about 150° C. to about 300° C.

Methodology Applied
Scientific EffectHeat treatment: Heat Treatment

Data Source

PatentUS10738264B2Method for purification of animal or vegetable fats
Publication Date: 2020.08.11 NESTE OYJ
  • US10738264B2 patent drawing
  • US10738264B2 patent drawing
  • US10738264B2 patent drawing

AI summary

Present invention relates to a novel process for purification of lipid material for further use as such as e.g. a source of fuel or chemicals.