Liquid Analyzer Flow Control for Viscous Sample Blockages

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Solution Overview

Problem

The existing liquid analyzers face challenges with handling viscous milk products containing particles and additives, which can cause blockages and viscosity issues in the flow system, particularly when using measurement cuvettes dimensioned for mid-infrared analysis.

Innovation Solution

A liquid analyzer with a flow system that includes a positive displacement pump and pressure monitoring, allowing for automatic adjustment of flow rate based on viscosity and detection of blockages, along with a controller to regulate pump operation and initiate back-flushing to prevent clogging, and a filter system to manage particle entry and re-entry.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If a measurement cuvette of precise thickness is used for mid-infrared analysis, then measurement precision is improved, but the device becomes more susceptible to blockages from particles and difficult to handle with viscous liquids

Engineering Contradiction:
Improvemeasurement precisionVSAvoidblockage susceptibility
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The pump module is designed with variable speed capability, allowing the flow rate to be dynamically adjusted according to sample viscosity. This enables the system to maintain reliable operation with both low-viscosity and high-viscosity samples while preserving measurement precision through consistent flow control.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

A pressure monitor provides real-time feedback on system pressure, enabling the controller to detect blockages and automatically adjust pump operation or initiate back-flushing procedures. This feedback mechanism prevents blockages from compromising measurement precision while maintaining system reliability.

Inventive Principle:
Principle #23Feedback

2Productivity

If the flow rate is increased to improve productivity, then analysis speed is improved, but viscous samples become difficult to transport and blockages are more likely

Engineering Contradiction:
Improveanalysis speedVSAvoidblockage susceptibility
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The pump module operates at variable speeds that can be optimized for each sample type. For viscous samples, the pump speed is reduced to prevent blockages, while for low-viscosity samples, higher speeds maintain productivity. This dynamic adjustment resolves the contradiction between speed and reliability.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The system proactively monitors pressure and automatically initiates back-flushing when blockages are detected, preventing complete system failure. This preliminary anti-action maintains productivity by quickly clearing blockages rather than allowing them to halt analysis.

Inventive Principle:
Principle #9Preliminary anti-action

3Measurement precision

If particles are allowed to enter the measurement zone, then sample representativity is improved, but blockages and measurement errors increase

Engineering Contradiction:
Improvesample representativityVSAvoidblockages
Core Design Contradiction:
Measurement precisionVSObject-affected harmful factors

Solution Approach 1:

The flow path is segmented into different zones with appropriate filtration at strategic locations. This allows particles to be filtered from the sample stream before reaching the measurement zone, preventing blockages while maintaining sample representativity through controlled filtration.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The system implements periodic back-flushing to clear particles from the measurement zone and conduits. This periodic cleaning action prevents particle accumulation and blockages while allowing representative sampling during normal operation.

Inventive Principle:
Principle #19Periodic action

4Reliability

If back-flushing is implemented to prevent blockages, then reliability is improved, but additional system complexity and operation time are required

Engineering Contradiction:
Improveblockage preventionVSAvoidsystem complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The system automatically monitors pressure and initiates back-flushing when blockages are detected, without requiring manual intervention. This self-service capability improves reliability while minimizing the impact of the additional function on overall system complexity.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The pressure monitor provides feedback that triggers automatic back-flushing only when necessary. This feedback-controlled approach prevents unnecessary back-flushing operations, reducing the impact on productivity while maintaining reliability through targeted blockage prevention.

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system ensures robust and versatile liquid handling, maintaining accurate flow and preventing blockages, even with high viscosity samples, by dynamically adjusting pump speed and reversing flow to clear blockages, thus enhancing the reliability of compositional analysis.

Implementation Method 1

a first pump module, preferably comprising a positive displacement pump such as a syringe pump, coupled to the liquid conduits and being operable to effect liquid flow therein

Methodology Applied
Scientific EffectPositive displacement:

Implementation Method 2

a first pressure monitor disposed to measure pressure between the sample intake and the at least one measurement zone and a controller adapted to receive an output from the first pressure monitor representative of the measured pressure

Methodology Applied
Scientific EffectPressure measurement:

Implementation Method 3

the controller is adapted to control the operation of the first pump module to regulate the liquid flow in the liquid conduits in dependence thereon

Methodology Applied
Scientific EffectFlow regulation:

Implementation Method 4

initiate back-flushing to prevent clogging

Methodology Applied
Scientific EffectBack-flushing:

Data Source

PatentEP3204749B1Liquid analyser
Publication Date: 2018.06.06 FOSS ANALYTICAL AS
  • EP3204749B1 patent drawingFigure 1
  • EP3204749B1 patent drawingFigure 2

AI summary

A liquid analyzer (2) comprises a liquid sample intake (4) for immersion in a liquid sample (6); at least one measurement zone (16;16'); and a first pump module (P1) operable to effect liquid flow from sample intake (4) towards the at least one measurement zone (16;16'). A first pressure monitor (36) is provided to measure pressure between the sample intake (4) and the at least one measurement zone (16'16') and the operation of the first pump module (P1) to regulate the liquid flow in the liquid conduits (22) is regulated in dependence thereon.