Shielding in a separation column

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Solution Overview

Problem

In mass transfer columns, particularly air separation columns, uniform liquid distribution is critical for efficient mass transfer, but traditional designs often result in liquid droplet deflection due to interactions with ascending vapor streams, leading to maldistribution and poor performance, especially at high production rates.

Innovation Solution

The introduction of a shield wall affixed to the liquid distributor, which extends downward to direct ascending vapor streams closer to the packing surface, creating a static pressure zone with low vapor velocity, thereby reducing the affected droplet residence time and minimizing droplet deflection.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If the spacing between liquid distributor and packing is reduced, then droplet deflection is minimized, but device complexity and manufacturing difficulty increase

Engineering Contradiction:
Improveliquid distribution uniformityVSAvoidcolumn structure complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

A shield wall is introduced as an intermediary component between the liquid distributor and packing. The shield wall redirects vapor flow away from falling droplets, preventing vapor-droplet interactions that cause deflection. This allows maintaining a larger spacing while achieving the same liquid distribution uniformity that would otherwise require a small spacing.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Productivity

If vapor flow rate is increased for high production rates, then productivity improves, but droplet deflection increases due to stronger vapor streams

Engineering Contradiction:
Improveproduction rateVSAvoidliquid distribution uniformity
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The shield wall acts as a protective intermediary that shields falling droplets from the influence of high-velocity vapor streams. By redirecting vapor flow along the shield wall surface, the harmful vapor-droplet interactions are prevented even at high vapor flow rates, allowing high productivity to be maintained without sacrificing liquid distribution uniformity.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Manufacturing precision

If spacing is reduced to minimize deflection, then liquid distribution uniformity improves, but the affected droplet residence time increases due to fabrication limits

Engineering Contradiction:
Improveliquid distribution uniformityVSAvoiddroplet residence time in spacing
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

The shield wall introduces a new mechanism for protecting droplets - not by reducing the spacing distance, but by blocking the harmful vapor flow path. The shield wall creates a low-velocity zone behind it where droplets can fall without deflection, effectively reducing the residence time in the affected zone while maintaining a larger overall spacing for fabrication reasons.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This design significantly reduces droplet deflection and enhances liquid distribution uniformity, leading to improved mass transfer efficiencies and sustained performance at high production rates.

Implementation Method 1

creating a static pressure zone with low vapor velocity

Methodology Applied
Scientific EffectStatic pressure zone:

Implementation Method 2

direct ascending vapor streams closer to the packing surface

Methodology Applied
Scientific EffectVapor stream deflection:

Implementation Method 3

The liquid falls down the mass transfer column as a result of gravity

Methodology Applied
Scientific EffectGravity: Gravitation

Implementation Method 4

the vapor rises up the mass transfer column as a result of an established pressure gradient along the length of the column section

Methodology Applied
Scientific EffectPressure gradient: Pressure Gradient

Data Source

PatentEP2691164B1Shielding in a separation column
Publication Date: 2021.03.17 AIR PROD & CHEM INC
  • EP2691164B1 patent drawingFigure 1~2
  • EP2691164B1 patent drawingFigure 3
  • EP2691164B1 patent drawingFigure 4~5

AI summary

A liquid distributor and method for distribution of a liquid in a mass transfer column, the distributor includes at least one riser comprising at least one riser wall, the at least one riser wall extends from a first surface of the distributor in a first direction of the mass transfer column; at least one shield, the at least one shield extends from a second surface of the distributor opposite the first surface and extending in a second direction opposite the first direction; and at least one liquid distribution aperture extending from the first surface of the distributor through the second surface of the distributor, the at least one shield has a length extending in the second direction such that a gap is created between the at least one shield and a packing, the height of the gap between the shield and the packing is about 10 mm to 75 mm.