Liquid distributor with a mixer

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Solution Overview

Problem

Existing devices for distributing and mixing liquids in cryogenic distillation columns, particularly in large air separation plants, fail to achieve complete mixing and uniform distribution, leading to inefficiencies in separation processes and reliability issues due to debris accumulation.

Innovation Solution

The apparatus comprises a collector, mixer, conduits, predistributor, and final distributor, with a filter option, designed to collect, mix, and distribute liquids uniformly across the column cross-sectional area, using conduits to transpose liquid from one sector to another, ensuring symmetric distribution and mixing, and optionally includes a filter to prevent debris accumulation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If existing liquid distribution devices are used in large cryogenic distillation columns, then the column can operate, but complete mixing and uniform distribution cannot be achieved

Engineering Contradiction:
Improveliquid distribution uniformityVSAvoidmixing device structure
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The liquid distribution device is segmented into multiple functional components: a collector that divides liquid into sectors, multiple conduits that transport liquid between sectors, a mixer that combines liquid from different sectors, and a predistributor that redistributes mixed liquid. This segmentation allows each component to perform a specific function, achieving complete mixing and uniform distribution while maintaining manageable structural complexity.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Conduits serve as intermediaries that transport liquid between the collector and mixer, enabling circumferential transposition of liquid sectors. The conduits act as mediators that facilitate the mixing process by redirecting liquid flow paths, allowing liquid from different sectors to be combined in the mixer before distribution.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Productivity

If liquid is not completely mixed in distillation columns, then separation efficiency decreases

Engineering Contradiction:
Improveseparation efficiencyVSAvoidoperational reliability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The device performs preliminary mixing action before liquid distribution by collecting liquid in sectors, transposing sectors through conduits, and combining them in a mixer. This preliminary mixing ensures that liquid is completely mixed before entering the distillation column, thereby improving separation efficiency and operational reliability.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The device incorporates feedback mechanisms where the mixer receives liquid from multiple conduits representing different sectors, combines them, and the predistributor redistributes the mixed liquid uniformly. This feedback loop ensures that mixing adequacy is achieved before distribution, improving both separation efficiency and operational reliability.

Inventive Principle:
Principle #23Feedback

3Reliability

If debris accumulates in the column, then operational reliability deteriorates

Engineering Contradiction:
Improveoperational reliabilityVSAvoiddebris accumulation
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The device extracts harmful debris from the liquid stream by incorporating filtration elements within the collector and/or mixer components. Debris is separated and removed from the liquid before distribution into the distillation column, preventing accumulation and maintaining operational reliability.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The device provides beforehand protection against debris accumulation by integrating filters in the liquid path before distribution. This prior cushioning measure prevents debris from entering the distillation column, thereby protecting the system and maintaining operational reliability.

Inventive Principle:
Principle #11Beforehand cushioning (Prior cushioning)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This solution achieves complete mixing and uniform distribution of liquids, enhancing separation efficiency and reliability by compensating for mixing inadequacies and protecting the column from debris, resulting in shorter bed heights and improved operational reliability.

Implementation Method 1

The conduits are adapted to receive and transmit downward at least a portion of the liquid from the collector to the mixer

Methodology Applied
Scientific EffectFluid flow through conduits:

Implementation Method 2

The mixer is adapted to receive and mix at least a portion of the liquid collected on the collector

Methodology Applied
Scientific EffectMixing: Stirring

Data Source

PatentEP2790804B1Liquid distributor with a mixer
Publication Date: 2019.10.16 AIR PROD & CHEM INC
  • EP2790804B1 patent drawingFigure 1
  • EP2790804B1 patent drawingFigure 2A~2C
  • EP2790804B1 patent drawingFigure 2D~2G

AI summary

An apparatus for distributing a flow of a liquid descending in an inner space of a packed column includes: a collector to collect the flow of the liquid; a mixer below and vertically spaced apart from the collector to receive and mix the liquid collected; a first conduit to receive and transmit at least part of the liquid from a first sector of the collector to a first zone of the mixer; and a second conduit to receive and transmit at least part of the liquid from a second sector of the collector to a second zone of the mixer. A geometric center of the first sector of the collector is positioned circumferentially away from a geometric center of the first zone of the mixer and/or a geometric center of the collector's second sector is positioned circumferentially away from a geometric center of the mixer's second zone.