Liquid Metal Composition Control in PVD Evaporators

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Solution Overview

Problem

In high-speed physical vapor deposition (PVD) processes, the composition of liquid metal in an evaporator changes due to differing vapor pressures of metals, leading to enrichment with impurities and instability in the metal coating on substrates, which is costly to address with high-purity feeding materials and inefficient with existing external feeding methods.

Innovation Solution

An apparatus and method using two vessels to control the composition of liquid metal in an evaporator, employing magnetohydrodynamic (MHD) pumps and induction heating to circulate and mix liquid metal, with level and flow sensors, and valves to maintain a stable composition by compensating for evaporation rates through controlled feeding from a secondary vessel.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If high purity feeding material is used to address impurity enrichment, then coating quality is improved, but manufacturing cost increases considerably

Engineering Contradiction:
Improvecoating qualityVSAvoidmanufacturing cost
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The invention extracts and removes impurities from the liquid metal composition in the evaporator by utilizing the vapor pressure differences between metals. The system continuously monitors composition and adjusts feeding rates to compensate for preferential evaporation of high vapor pressure metals, thereby extracting impurities without requiring high purity feeding materials.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention implements a feedback control system that continuously monitors the liquid metal composition in the evaporator and adjusts the feeding rates from multiple vessels accordingly. This closed-loop control maintains stable coating composition by compensating for changes in real-time, eliminating the need for expensive high purity materials.

Inventive Principle:
Principle #23Feedback

2Stability of the object's composition

If the evaporator size is increased to control liquid metal composition changes, then composition stability is improved, but space requirements in the vacuum chamber increase

Engineering Contradiction:
Improvecomposition stabilityVSAvoidspace requirements
Core Design Contradiction:
Stability of the object's compositionVSArea of stationary object

Solution Approach 1:

The invention divides the liquid metal supply system into multiple separate vessels, each containing different metal compositions. This segmentation allows independent control of each metal's feeding rate to the evaporator, enabling precise composition management without requiring a larger evaporator volume.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention implements dynamic control of metal feeding rates based on real-time composition monitoring. The system continuously adjusts the feeding rates from multiple vessels to compensate for preferential evaporation, maintaining composition stability through active control rather than relying on large evaporator volume.

Inventive Principle:
Principle #15Dynamics

3Duration of action of moving object

If external liquid metal source is used to feed the evaporator, then composition control time is extended, but device complexity increases

Engineering Contradiction:
Improvecomposition control timeVSAvoiddevice complexity
Core Design Contradiction:
Duration of action of moving objectVSDevice complexity

Solution Approach 1:

The invention combines multiple liquid metal vessels with different metal compositions into a unified feeding system. By coordinating the feeding from multiple vessels simultaneously, the system achieves extended composition control duration while managing complexity through integrated control of multiple sources.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach maintains a stable vapor composition and coating quality by continuously adjusting the liquid metal composition in the evaporator, reducing impurity enrichment and composition changes, while minimizing space requirements and operational costs.

Implementation Method 1

the means to feed the liquid metal from the first vessel to the evaporator comprises a supply line provided with a magnetohydrodynamic (MHD) pump

Methodology Applied
Scientific EffectMagnetohydrodynamic effect: Magnetohydrodynamic Effect

Implementation Method 2

Such an evaporator is for instance used in a physical vapour deposition (PVD) process wherein a metal vapour is deposited on a substrate

Methodology Applied
Scientific EffectInduction heating: Induction Heating

Data Source

PatentEP3066229B1Method for controlling the composition of liquid metal in an evaporator device
Publication Date: 2020.08.26 TATA STEEL NEDERLAND TECH BV
  • EP3066229B1 patent drawingFigure 1~2
  • EP3066229B1 patent drawingFigure 3~4

AI summary

The invention relates to an apparatus and method for controlling the composition of liquid metal fed to an evaporator in a vacuum chamber used in a physical vapour deposition process.