Liquid Reactant Pressure Control for Metastable Compound Yield

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Solution Overview

Problem

Existing methods for controlling chemical reactions involving liquid phases either completely prevent or guarantee cavitation, making it difficult to access metastable compounds with good yields.

Innovation Solution

A method that controls chemical reactions by subjecting a liquid reactant to a pressure change, maintaining a pressure minimum up to 105% of the cavitation pressure without causing cavitation, using suitable frequencies and electrical fields for improved kinetic control, thereby producing metastable compounds with enhanced yields.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If cavitation is completely prevented in liquid phase reactions, then reaction reliability is improved, but access to metastable compounds is lost

Engineering Contradiction:
Improvereaction reliabilityVSAvoidaccess to metastable compounds
Core Design Contradiction:
ReliabilityVSAdaptability or versatility

Solution Approach 1:

The patent applies dynamic control of pressure parameters, continuously adjusting the pressure minimum during the reaction process to maintain it between 90-105% of the cavitation pressure. This dynamic approach allows the system to operate in a metastable regime where cavitation is suppressed but its effects are enhanced, enabling access to metastable compounds while maintaining reaction reliability.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The invention changes the pressure parameter from a static prevention approach to a dynamic control approach, maintaining pressure minimum at a specific percentage (90-105%) of the cavitation pressure rather than completely preventing pressure drops. This parameter change enables the system to exploit near-cavitation effects for producing metastable compounds while avoiding actual cavitation damage.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If cavitation is guaranteed in liquid phase reactions, then kinetic control is improved, but reaction reliability deteriorates

Engineering Contradiction:
Improvekinetic controlVSAvoidreaction reliability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent applies partial action by maintaining pressure minimum at 90-105% of cavitation pressure, which is close to but does not fully reach the cavitation point. This partial approach provides sufficient kinetic control enhancement through near-cavitation effects while avoiding the reliability deterioration caused by full cavitation. The system gets 90-105% of the kinetic control benefit with minimal cavitation occurrence.

Inventive Principle:
Principle #16Partial or excessive action

3Productivity

If pressure minimum is set at 105% of cavitation pressure, then kinetic control is improved, but cavitation risk increases

Engineering Contradiction:
Improvekinetic controlVSAvoidcavitation risk
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The patent implements feedback control by continuously monitoring the pressure minimum and adjusting it to maintain a specific relationship (90-105%) with the cavitation pressure. This feedback mechanism ensures that the system operates optimally for kinetic control while automatically preventing excessive pressure drops that would cause harmful cavitation. The feedback loop balances productivity improvement with harm prevention.

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach allows for the production of kinetically controlled, valuable, and versatile metastable compounds with improved yields and cost-effectiveness, particularly in refining fuels.

Implementation Method 1

the pressure minimum corresponds to a maximum 105%, preferably no greater than 103%, and especially preferably no greater than 101% of the cavitation pressure of the reactant, without causing cavitation in the reactant

Methodology Applied
Scientific EffectCavitation pressure: Cavitation

Implementation Method 2

conducting a reaction close to the cavitation point, preferably supported by suitable frequencies, electrical fields and/or currents

Methodology Applied
Scientific EffectElectrical field effect on chemical reaction: Electric Field

Data Source

PatentUS11766655B2Method for controlling a chemical reaction and apparatus for carrying out said method
Publication Date: 2023.09.26 HEION GMBH
  • US11766655B2 patent drawing
  • US11766655B2 patent drawing
  • US11766655B2 patent drawing

AI summary

The invention relates to a method for controlling a chemical reaction which creates a product, wherein at least one reactant that is present in a liquid phase is subjected to a pressure change.