Liquid Separator for Continuous Three-Phase Mixture Separation

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Solution Overview

Problem

Current methods struggle to efficiently separate solid and gas phase products from three-phase mixtures of liquids, solids, and gases, particularly at high temperatures, while retaining the liquid phase within the vessel.

Innovation Solution

The system employs a vessel with a gas inlet and outlet, a liquid with an upper surface, and a solid phase, along with a liquid separator configured to remove liquid droplets generated by the gas and solid phases. This is achieved through various configurations, including floating solids, perforated structures, packed columns, and cyclonic separators, to minimize liquid entrainment and maximize separation efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If gas and solid phases are separated from three-phase mixtures at high temperatures, then separation efficiency is improved, but liquid entrainment in the gas stream increases

Engineering Contradiction:
Improveseparation efficiencyVSAvoidliquid carryover
Core Design Contradiction:
Manufacturing precisionVSLoss of substance

Solution Approach 1:

The separation process is divided into multiple sequential stages: initial gas-solid separation in the upper vessel portion, followed by liquid droplet removal in a downstream separator. This segmentation allows each stage to optimize for its specific function, improving overall separation efficiency while minimizing liquid entrainment in the final gas stream

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

A liquid separator acts as an intermediary component between the three-phase mixture and the final gas outlet. This intermediary device specifically targets and removes liquid droplets from the gas stream without affecting the already-separated gas and solid phases, thereby reducing liquid carryover while maintaining separation efficiency

Inventive Principle:
Principle #24Intermediary (Mediator)

2Loss of substance

If liquid separator is added to remove liquid droplets, then liquid carryover is reduced, but device complexity increases

Engineering Contradiction:
Improveliquid carryoverVSAvoidseparation system complexity
Core Design Contradiction:
Loss of substanceVSDevice complexity

Solution Approach 1:

The liquid separator is extracted as a distinct, modular component from the main reaction vessel. This allows the separator to be independently optimized for liquid droplet removal while the main vessel maintains its primary function for three-phase mixing and initial separation, reducing overall system complexity through functional decomposition

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The liquid separator is designed to perform multiple functions: removing liquid droplets from the gas stream, preventing liquid carryover to downstream equipment, and maintaining system pressure. This multi-functionality reduces the need for additional separate components, thereby limiting the increase in device complexity

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Productivity

If continuous separation is implemented, then productivity is improved, but energy consumption increases

Engineering Contradiction:
Improveseparation rateVSAvoidenergy consumption
Core Design Contradiction:
ProductivityVSUse of energy by moving object

Solution Approach 1:

Gas and solid phases are preliminarily separated in the upper portion of the vessel before the gas stream enters the liquid separator. This preliminary separation reduces the workload on the liquid separator and minimizes the energy required for continuous operation, as the separator only needs to handle liquid droplet removal rather than complete three-phase separation

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The system utilizes the natural buoyancy and density differences of the phases to achieve separation without requiring external energy input for pumping or forced circulation. Gas bubbles rise naturally through the liquid, carrying solids to the surface, where they are separated by gravity, enabling continuous operation with minimal energy consumption

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The described methods and devices enable the continuous separation of high temperature three-phase mixtures, effectively removing gas and solid phases while retaining the liquid phase, thereby producing clean gas-solid suspensions or streams with minimal liquid carryover.

Implementation Method 1

passing bubbles of the gas through the liquid, where a solid is present within the liquid; passing the gas out of an upper liquid surface

Methodology Applied
Scientific EffectBuoyancy: Archimedes' Principle (Buoyancy)

Implementation Method 2

separating the solid from the liquid at the upper liquid surface; removing at least a portion of the droplets of the liquid

Methodology Applied
Scientific EffectPhase separation: Density Gradient

Data Source

PatentUS20250144548A1Continuous separation of multiphase mixtures
Publication Date: 2025.05.08 MOLTEN INDUSTRIES INC
  • US20250144548A1 patent drawing
  • US20250144548A1 patent drawing
  • US20250144548A1 patent drawing

AI summary

A reaction system includes a vessel having a gas inlet and a gas outlet, a liquid within the vessel, a solid phase and a gas phase present within the vessel, and at least one liquid separator disposed within the vessel. The liquid has an upper liquid surface within the vessel, and the liquid separator is configured to remove at least a portion of liquid droplets generated based on the gas phase and the solid phase passing through the liquid.