Lithium-Doped Nickel Oxide Anode for Alkaline Electrolysis

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Solution Overview

Problem

Alkaline water electrolysis systems using nickel anodes face degradation due to power fluctuations, leading to reduced durability and increased risk of electric current leakage, especially when using renewable energy sources with large power fluctuations.

Innovation Solution

A nickel-based anode with a lithium-containing nickel oxide catalytic layer, where the molar ratio of lithium to nickel (Li/Ni) is between 0.005 and 0.15, is formed on a conductive substrate through a heat treatment process at 900°C to 1000°C, enhancing durability and corrosion resistance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If a nickel anode is used in alkaline water electrolysis with renewable energy sources, then the system can utilize large power fluctuations, but the nickel anode degrades due to oxidation and reduction reactions under reverse current conditions

Engineering Contradiction:
Improveadaptability to power fluctuationsVSAvoidanode durability
Core Design Contradiction:
Adaptability or versatilityVSReliability

Solution Approach 1:

The patent applies composite materials by combining nickel substrate with coating layers of nickel oxide, nickel hydroxide, and lithium compounds. This composite structure prevents the nickel substrate from direct contact with the alkaline electrolyte, thereby preventing oxidation and reduction reactions that cause degradation under reverse current conditions, while maintaining the ability to withstand power fluctuations from renewable energy sources

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent uses an intermediary approach by introducing coating layers (nickel oxide, nickel hydroxide, and lithium compounds) between the nickel substrate and the alkaline electrolyte. These coating layers act as mediators that prevent harmful direct contact and chemical reactions, while still allowing the electrode to function properly during electrolysis operations with varying power inputs

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If the nickel anode is maintained at low potential to prevent oxidation, then reverse current reactions are reduced, but electric current leakage occurs through shared pipes in large cells

Engineering Contradiction:
Improveanode stabilityVSAvoidelectric current leakage
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent applies composite materials by combining nickel substrate with coating layers of nickel oxide, nickel hydroxide, and lithium compounds. This composite structure prevents the nickel substrate from direct contact with the alkaline electrolyte, thereby preventing oxidation and reduction reactions that cause degradation under reverse current conditions, while maintaining the ability to withstand power fluctuations from renewable energy sources

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent uses an intermediary approach by introducing coating layers (nickel oxide, nickel hydroxide, and lithium compounds) between the nickel substrate and the alkaline electrolyte. These coating layers act as mediators that prevent harmful direct contact and chemical reactions, while still allowing the electrode to function properly during electrolysis operations with varying power inputs

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The anode maintains high performance and stability over long-term use, reducing the impact of power fluctuations and preventing electric current leakage, making it suitable for alkaline water electrolysis with renewable energy sources.

Implementation Method 1

a catalytic layer formed on the surface of the conductive substrate and made of lithium-containing nickel oxide

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 2

The following production reaction of nickel oxide is assumed to proceed. Ni + 2OH -

Methodology Applied
Scientific EffectOxidation: Oxidation

Implementation Method 3

a nickel-based anode with a lithium-containing nickel oxide catalytic layer, where the molar ratio of lithium to nickel (Li/Ni) is between 0.005 and 0.15, is formed on a conductive substrate through a heat treatment process at 900°C to 1000°C

Methodology Applied
Scientific EffectHeat treatment: Heat Treatment

Implementation Method 4

preventing electric current leakage

Methodology Applied
Scientific EffectElectrical resistance: Electrical Resistance

Data Source

PatentEP3064614B1Anode for alkaline water electrolysis
Publication Date: 2018.06.20 DE NORA PERMELEC LTD
  • EP3064614B1 patent drawingFigure 1~2B
  • EP3064614B1 patent drawingFigure 3
  • EP3064614B1 patent drawingFigure 4A~4B

AI summary

An anode for alkaline water electrolysis includes a conductive substrate having at least a surface made of nickel or a nickel-base alloy and a lithium-containing nickel oxide catalytic layer formed on a surface of the substrate. The molar ratio (Li/Ni) of lithium and nickel in the catalytic layer is in the range of 0.005 to 0.15.