Lithium-Ion Electrolyte Flash Point and Ionic Conductivity

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Solution Overview

Problem

Current electrolytes for lithium-ion batteries face challenges in achieving high safety, performance, and longevity due to issues such as low flash points, toxic decomposition products, high flammability, and reduced lithium ion mobility, which are not adequately addressed by existing solutions like organic carbonates, solid electrolytes, gel polymer electrolytes, or ionic liquids.

Innovation Solution

A mixture of cyclic carbonates and sulfone derivatives with a lithium source as a conductive salt, which provides a high flash point above 85°C, improved ionic conductivity, and enhanced stability, while maintaining high cell performance even at elevated charge and discharge rates.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If organic carbonates are used as electrolyte, then ionic conductivity is improved, but flash point decreases and flammability increases

Engineering Contradiction:
Improveionic conductivityVSAvoidflammability
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent uses a composite electrolyte system combining cyclic carbonate (EC) and sulfone derivative (DMSO) in specific ratios (95:5 to 50:50 by weight), creating a composite material that leverages the high ionic conductivity of carbonates while the sulfone derivative elevates the flash point above 85°C, thus resolving the contradiction between conductivity and flammability

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent changes the chemical composition parameters by introducing sulfone derivatives as additives (5-50 wt%) to modify the electrolyte's physical properties, specifically raising the flash point while maintaining ionic conductivity through optimized concentration ratios of the components

Inventive Principle:
Principle #35Parameter changes

2Object-affected harmful factors

If ionic liquids are used as electrolyte additive, then safety is improved, but lithium ion mobility decreases

Engineering Contradiction:
ImprovesafetyVSAvoidlithium ion mobility
Core Design Contradiction:
Object-affected harmful factorsVSSpeed

Solution Approach 1:

The patent replaces expensive ionic liquids with a cost-effective sulfone derivative (DMSO) that provides similar safety benefits (flash point >85°C) without the severe mobility reduction, achieving a practical compromise between safety and performance at lower cost

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The patent optimizes the concentration of sulfone derivative (5-50 wt%) to achieve the minimum effective amount for safety improvement while minimizing the negative impact on lithium ion mobility, thus resolving the contradiction between safety enhancement and ion transport

Inventive Principle:
Principle #35Parameter changes

3Object-affected harmful factors

If sulfolane is used as electrolyte component, then flash point is improved, but viscosity increases

Engineering Contradiction:
Improveflash pointVSAvoidviscosity
Core Design Contradiction:
Object-affected harmful factorsVSStability of the object's composition

Solution Approach 1:

The patent extracts the essential safety function (flash point elevation) from sulfolane and achieves it through a different chemical approach using DMSO, which provides comparable flash point improvement without the severe viscosity penalty, thus separating the desired safety effect from the unwanted viscous effect

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent creates a composite electrolyte where DMSO (sulfone derivative) combines with cyclic carbonate to achieve both high flash point and acceptable viscosity by leveraging the low-viscosity properties of carbonate to counterbalance the viscosity increase from the sulfone component

Inventive Principle:
Principle #40Composite materials

4Object-affected harmful factors

If flash point is increased above 85°C, then safety is improved, but cell performance may deteriorate

Engineering Contradiction:
ImprovesafetyVSAvoidcell performance
Core Design Contradiction:
Object-affected harmful factorsVSProductivity

Solution Approach 1:

The patent systematically varies the composition ratio of cyclic carbonate to sulfone derivative (95:5 to 50:50 by weight) to find the optimal parameter range that simultaneously achieves flash point >85°C and maintains cell performance at 75% or more of available capacity, thus resolving the safety-performance trade-off

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The proposed electrolyte achieves a flash point of over 140°C without compromising cell performance at C rates up to 2C, ensuring both safety and efficiency, with specific capacities maintained at 75% of available capacity and sufficient lithium diffusion, while being non-toxic and cost-effective.

Implementation Method 1

high ionic conductivity, especially sufficient lithium-ion conductivity

Methodology Applied
Scientific EffectIonic conduction: Conduction (electrical)

Implementation Method 2

The cyclic carbonate and the sulfone derivative serve as solvents in which the conductive salts and additives are dissolved

Methodology Applied
Scientific EffectDissolution: Solvation

Data Source

PatentEP3155686B1Electrolyte, cell and battery comprising the electrolyte, and use of the electrolyte
Publication Date: 2019.08.14 KARLSRUHER INST FUR TECH
  • EP3155686B1 patent drawingFigure 1
  • EP3155686B1 patent drawingFigure 2~3
  • EP3155686B1 patent drawingFigure 4~5

AI summary

The invention relates to an electrolyte for lithium-ion batteries, comprising a mixture of ethylene carbonate (EC) and/or mono- or polyfluorinated ethylene carbonate, at least one sulfone derivative and at least one lithium source as a conducting salt, wherein the mixture has a flash point above 85°C. The invention further relates to the use of the electrolyte as an electrolyte in a lithium-ion cell and to a lithium-ion battery comprising the electrolyte.