Lithium Phosphate Coated Cathode for Battery Stability

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Solution Overview

Problem

Lithium secondary batteries face degradation due to reactions between lithium compounds on the cathode active material surface and the electrolyte, leading to increased surface resistance and reduced battery performance.

Innovation Solution

A lithium phosphate layer is formed on the surface of lithium-transition metal oxide cathode active materials using phosphoric acid, which consumes residual lithium compounds and prevents degradation without hindering lithium ion movement.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Power

If a composite metal oxide is used as cathode active material, then battery capacity and power are improved, but surface degradation occurs due to reaction with electrolyte

Engineering Contradiction:
Improvebattery powerVSAvoidsurface stability
Core Design Contradiction:
PowerVSReliability

Solution Approach 1:

A lithium phosphate layer is introduced as an intermediary coating on the cathode active material surface. This layer acts as a protective barrier between the composite metal oxide and the electrolyte, preventing direct harmful reactions while allowing lithium ion transport, thus resolving the contradiction between maintaining high power performance and ensuring surface stability.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention creates a composite structure consisting of the cathode active material core and the lithium phosphate coating layer. This composite material approach combines the high capacity benefits of composite metal oxides with the protective and ion-conductive properties of lithium phosphate, simultaneously achieving improved power and reliability.

Inventive Principle:
Principle #40Composite materials

2Ease of manufacture

If lithium compound remains on cathode active material surface, then manufacturing simplicity is maintained, but surface resistance increases due to reaction with electrolyte

Engineering Contradiction:
Improvemanufacturing simplicityVSAvoidsurface resistance
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The lithium phosphate layer is formed as a preliminary treatment step before battery assembly. This preliminary action converts the problematic residual lithium compounds into a beneficial protective coating, preventing future surface resistance issues while maintaining manufacturing efficiency through a straightforward coating process.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The invention converts the harmful residual lithium compounds on the surface into beneficial lithium phosphate through reaction with phosphoric acid. This transformation turns the source of surface resistance and degradation into a protective layer that enhances surface stability and ion conductivity.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

3Reliability

If heterometal oxide coating is applied to cathode active material, then surface degradation is reduced, but manufacturing complexity and cost increase

Engineering Contradiction:
Improvesurface stabilityVSAvoidcoating process complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The invention uses phosphoric acid, a cheap and readily available material, to form the protective lithium phosphate layer. This approach replaces complex heterometal oxide coatings with a simpler, more cost-effective solution that achieves the same protective function without requiring sophisticated coating equipment or rare materials.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The invention changes the chemical composition parameters of the surface layer from complex heterometal oxides to simple lithium phosphate. This parameter change simplifies the coating composition while maintaining protective functionality, reducing manufacturing complexity and cost.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The lithium phosphate layer effectively reduces surface resistance, enhances battery performance by maintaining discharge capacity over cycles, and improves the cathode's thermal stability and reversibility.

Implementation Method 1

the at least one lithium compound reacts with the phosphoric acid to obtain a cathode active material coated with a lithium phosphate layer

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 2

a lithium phosphate layer formed on a surface of the cathode active material and consisting essentially of Li3PO4, LiOH, and Li2CO3

Methodology Applied
Scientific EffectIon conduction: Conduction (electrical)

Data Source

PatentEP3032619B1Cathode material for lithium secondary battery, and lithium secondary battery containing same
Publication Date: 2019.10.09 IND ACAD COOP GRP OF SEJONG UNIV
  • EP3032619B1 patent drawingFigure 1~2
  • EP3032619B1 patent drawingFigure 3
  • EP3032619B1 patent drawingFigure 4

AI summary

Provided are a cathode material for a lithium secondary battery, and a lithium secondary battery containing the same. The cathode material for a lithium secondary battery comprises: a cathode active material, which is a lithium-transition metal oxide, and a lithium phosphate layer coated on a surface of the cathode active material.