Lithium Sulfide Reactor with Heat Insulation and Anti-Sulfurized Surface

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Solution Overview

Problem

Existing lithium sulfide production techniques face challenges in achieving high production efficiency and stability, as described in Patent Document 1, which limits the effectiveness of the methods for producing lithium sulfide.

Innovation Solution

A lithium sulfide producing device is designed with a reactor containing a lithium hydroxide filling part, a heating unit, and a hydrogen sulfide supply member, featuring a heat-insulating member above the lithium hydroxide to maintain uniform temperature, an anti-sulfurized inner surface, and an inverted funnel-shaped recovery member for efficient hydrogen sulfide supply and recovery, allowing precise control of hydrogen sulfide gas supply and maintaining high production efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If sulfur vapor is generated by heating sulfur in a lower portion of a reaction tank and reacted with hydrogen gas to generate hydrogen sulfide gas, then lithium sulfide can be produced by reacting with lithium hydroxide in an upper portion, but production efficiency is insufficient and stability is poor

Engineering Contradiction:
Improveproduction efficiencyVSAvoidstability of production efficiency
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The reaction tank is divided into distinct functional zones: a lower heating zone for sulfur vapor generation, a middle reaction zone for hydrogen sulfide production, and an upper lithium hydroxide reaction zone. This segmentation allows each zone to be optimized independently for its specific function, improving overall production efficiency and stability.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Hydrogen gas is introduced as an intermediary substance that reacts with sulfur vapor to form hydrogen sulfide gas, which then serves as the reactant for lithium sulfide production. This intermediary step enables controlled and stable progression of the reaction sequence, improving production reliability.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Productivity

If hydrogen sulfide gas is supplied to react with lithium hydroxide, then lithium sulfide is produced, but temperature uniformity affects reaction stability

Engineering Contradiction:
Improveproduction efficiencyVSAvoidtemperature uniformity
Core Design Contradiction:
ProductivityVSTemperature

Solution Approach 1:

Heating elements are strategically positioned in the lower portion of the reaction tank to generate sulfur vapor, while the upper portion where lithium hydroxide is located is designed to maintain uniform temperature distribution. This local quality approach ensures optimal temperature conditions in each region, improving reaction stability.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

Temperature control mechanisms monitor and adjust heating parameters to maintain uniform temperature distribution in the lithium hydroxide reaction zone. This feedback control ensures stable reaction conditions, improving production efficiency and consistency.

Inventive Principle:
Principle #23Feedback

3Manufacturing precision

If the inner surface of the device is anti-sulfurized, then sulfur contamination is reduced, but device complexity increases

Engineering Contradiction:
Improvepurity of lithium sulfideVSAvoiddevice complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The anti-sulfurized coating is applied to the inner surface of the reaction tank and equipment, creating a protective layer that automatically prevents sulfur contamination without requiring additional complex removal systems. This self-protecting feature simplifies the overall device design while ensuring high product purity.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The device achieves stable and high-efficiency production of lithium sulfide by maintaining a uniform temperature and efficient hydrogen sulfide supply, enhancing the production efficiency and stability of the lithium sulfide production process.

Implementation Method 1

a heating unit for heating lithium hydroxide

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 2

an interior of the reactor includes a heat-insulating member above the lithium hydroxide filling part

Methodology Applied
Scientific EffectThermal insulation: Thermal Insulation

Implementation Method 3

a hydrogen sulfide supply member connected to the reactor

Methodology Applied
Scientific EffectGas flow:

Implementation Method 4

reacting hydrogen sulfide with lithium hydroxide

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Data Source

PatentUS20240239659A1Lithium sulfide producing device and method for producing lithium sulfide
Publication Date: 2024.07.18 FURUKAWA COMPANY
  • US20240239659A1 patent drawing
  • US20240239659A1 patent drawing
  • US20240239659A1 patent drawing

AI summary

A lithium sulfide producing device (1-1) of the present invention is a lithium sulfide producing device for producing lithium sulfide by reacting hydrogen sulfide with lithium hydroxide, the lithium sulfide producing device including a reactor (1-3) having a lithium hydroxide filling part (1-2) inside, a heating unit for heating lithium hydroxide, and a hydrogen sulfide supply member connected to the reactor (1-3).