Lithium-Sulfur Battery Electrolyte for Dendrite and Polysulfide Control

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Solution Overview

Problem

Lithium-sulfur batteries face issues with the formation of lithium dendrites and the leaching of lithium polysulfide, leading to reduced capacity and shortened cycle life due to the high reactivity of lithium metal and solubility of polysulfides in the electrolyte, which current protective layers and electrolyte compositions fail to adequately address.

Innovation Solution

An electrolyte for lithium-sulfur batteries comprising a carbonate compound as an additive and specific non-aqueous organic solvents, including ether and heterocyclic compounds, forms a protective layer on the lithium metal surface, suppressing polysulfide leaching and enhancing electrode stability and efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Use of energy by moving object

If lithium metal is used as negative electrode active material to achieve high capacity and high energy density, then the theoretical specific capacity reaches 3,860 mAh/g and energy density is maximized, but lithium dendrite formation occurs due to passivation layer collapse, causing short circuits and reducing battery lifetime

Engineering Contradiction:
Improveenergy densityVSAvoidbattery lifetime
Core Design Contradiction:
Use of energy by moving objectVSReliability

Solution Approach 1:

A protective layer comprising a polymer matrix and lithium dendrite absorbing material is introduced as an intermediary between the lithium metal negative electrode and the electrolyte. This protective layer prevents direct contact between lithium metal and electrolyte, suppressing dendrite formation while maintaining high capacity and energy density characteristics of lithium metal electrodes

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The protective layer is constructed as a composite material system combining a polymer matrix with lithium dendrite absorbing material dispersed within it. This composite structure provides both mechanical protection and chemical suppression of dendrite growth, resolving the contradiction between maintaining lithium metal's high energy density and ensuring battery reliability

Inventive Principle:
Principle #40Composite materials

2Reliability

If a protective layer is formed on lithium metal surface to suppress dendrite formation, then battery lifetime is improved, but the protective layer undergoes degeneration such as hardening or swelling during charging/discharging, reducing effectiveness

Engineering Contradiction:
Improvebattery lifetimeVSAvoidprotective layer stability
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The protective layer is designed with specific compositional parameters: a polymer matrix with controlled molecular weight and composition, and lithium dendrite absorbing material at optimized concentration ranges. These parameter optimizations ensure the protective layer maintains structural stability and functional effectiveness throughout charging/discharging cycles without hardening or swelling degradation

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The protective layer is designed as a flexible thin film structure that can accommodate volume changes of lithium metal during charging/discharging cycles. The polymer matrix provides flexibility and adaptability, allowing the protective layer to maintain intimate contact with the lithium metal surface while preventing dendrite formation, thus maintaining both reliability and compositional stability

Inventive Principle:
Principle #30Flexible shells and thin films

3Reliability

If lithium salt concentration in electrolyte is increased to improve battery characteristics, then electrochemical performance is enhanced, but electrolyte loss increases and dendrite generation is promoted

Engineering Contradiction:
Improvebattery characteristicsVSAvoidelectrolyte loss
Core Design Contradiction:
ReliabilityVSLoss of substance

Solution Approach 1:

The protective layer acts as an intermediary barrier that prevents direct interaction between high-concentration electrolyte and lithium metal surface. This allows the use of electrolyte compositions optimized for electrochemical performance without suffering from the typical drawbacks of electrolyte loss and dendrite generation, as the protective layer mediates the interface interactions

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The electrolyte improves the stability and uniformity of the negative electrode, suppresses lithium dendrite formation, and maximizes the capacity of the positive electrode, resulting in a longer lifetime and improved capacity realization for lithium-sulfur batteries.

Implementation Method 1

as lithium metal reacts easily with electrolyte due to its high chemical/electrochemical reactivity, a passivation layer is formed on the surface of the negative electrode

Methodology Applied
Scientific EffectElectrochemical reaction:

Implementation Method 2

suppressed the reaction between electrolyte and lithium metal or the formation of lithium dendrites to some extent by controlling the chemical reactivity of the electrolyte

Methodology Applied
Scientific EffectChemical reactivity control:

Data Source

PatentEP3993130B1Lithium-sulfur battery electrolyte and lithium-sulfur battery comprising same
Publication Date: 2025.11.26 LG ENERGY SOLUTION LTD
  • EP3993130B1 patent drawingFigure 1
  • EP3993130B1 patent drawingFigure 2
  • EP3993130B1 patent drawingFigure 3

AI summary

An electrolyte for a lithium-sulfur battery including a lithium salt, a non-aqueous organic solvent, and an additive. The non-aqueous organic solvent includes an ether compound and a heterocyclic compound. The heterocyclic compound includes one or more double bonds and comprises an oxygen atom or a sulfur atom. The additive includes a carbonate compound.