Lithium-Sulfur Battery Solid Nitrate Holder for Shuttle Suppression

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Solution Overview

Problem

Lithium-sulfur batteries face a decrease in coulombic efficiency due to the dissolution of lithium polysulfides in the electrolyte solution, leading to a shuttle phenomenon that reduces discharge capacity and increases charge capacity, and existing additives like lithium nitrate are consumed quickly, limiting the number of cycles with high efficiency.

Innovation Solution

Incorporating a lithium nitrate holder in a solid state, positioned on the outermost layer of the cell stack, to continuously supply lithium nitrate during battery operation, maintaining high coulombic efficiency for a long cycle.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If lithium nitrate is added to the electrolyte solution to prevent shuttle phenomenon, then coulombic efficiency is improved, but lithium nitrate is gradually consumed resulting in rapid decrease in efficiency after consumption

Engineering Contradiction:
Improvecoulombic efficiencyVSAvoidcycle life
Core Design Contradiction:
ReliabilityVSDuration of action of moving object

Solution Approach 1:

The lithium nitrate holder enables the system to self-replenish lithium nitrate during battery operation. The holder automatically supplies lithium nitrate to the electrolyte solution as it dissolves, maintaining a stable concentration without external intervention, thus resolving the contradiction between improving efficiency and extending cycle life.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

Lithium nitrate is pre-loaded in the holder in a solid state before battery operation begins. This preliminary preparation ensures that lithium nitrate is readily available to be supplied to the electrolyte solution when needed, preventing the shuttle phenomenon from the start and maintaining efficiency throughout extended cycling.

Inventive Principle:
Principle #10Preliminary action

2Reliability

If lithium polysulfide dissolves in electrolyte solution, then electrochemical reaction area is reduced, but adding lithium nitrate additive is consumed quickly

Engineering Contradiction:
Improvecapacity retentionVSAvoidlithium nitrate amount
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The lithium nitrate is extracted from the electrolyte solution and stored separately in the holder in solid state. This separation allows the lithium nitrate to be replenished on-demand from the holder, preventing its rapid consumption while maintaining its function of reducing lithium polysulfide dissolution and protecting capacity.

Inventive Principle:
Principle #2Taking out (Extraction)

3Duration of action of stationary object

If lithium nitrate holder is positioned on outermost layer of cell stack, then continuous supply is achieved, but device structure becomes more complex

Engineering Contradiction:
Improveoperational durationVSAvoidbattery structure
Core Design Contradiction:
Duration of action of stationary objectVSDevice complexity

Solution Approach 1:

The lithium nitrate holder is designed to perform multiple functions: it stores lithium nitrate in solid state, controls its dissolution rate, and positions itself on the outermost layer for optimal supply to the electrolyte solution. This multi-functionality achieves continuous supply while minimizing structural complexity by integrating these functions into a single component.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The lithium nitrate holder in a solid state ensures continuous supply of lithium nitrate, preventing a decrease in coulombic efficiency and maintaining it at 98% or more for 200 cycles or more, thereby enhancing the battery's lifetime and performance.

Implementation Method 1

lithium nitrate holder in a solid state... continuously supply lithium nitrate during the operation of battery

Methodology Applied
Scientific EffectDissolution: Solvation

Implementation Method 2

lithium polysulfide having a high sulfur oxidation number is a material with strong polarity, and is readily dissolved in an electrolyte solution including a hydrophilic organic solvent

Methodology Applied
Scientific EffectDissolution: Solvation

Implementation Method 3

Lithium polysulfide dissolved in the electrolyte solution diffuses from a positive electrode due to a difference in the concentration

Methodology Applied
Scientific EffectDiffusion: Diffusion

Implementation Method 4

an oxidation reaction of lithium occurs in a negative electrode of a lithium-sulfur battery, and a reduction reaction of sulfur occurs in a positive electrode

Methodology Applied
Scientific EffectElectrochemical reaction: Redox Reactions

Data Source

PatentEP4191736B1Lithium secondary battery
Publication Date: 2026.02.25 LG ENERGY SOLUTION LTD
  • EP4191736B1 patent drawingFigure 1~2
  • EP4191736B1 patent drawingFigure 3~4
  • EP4191736B1 patent drawing

AI summary

The present invention relates to a lithium secondary battery comprising a lithium nitrate holder in a solid state, which is capable of continuously supplying lithium nitrate while operating the battery, thereby maintaining high coulombic efficiency for a long period of time.