Lithium-Transition Metal Composite Cathode for High-Rate Battery Performance

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Solution Overview

Problem

Conventional cathode active materials for lithium secondary batteries face challenges such as high cost, limited lifespan, and poor high-rate charge/discharge characteristics due to instability and phase changes, particularly with lithium cobalt oxides and lithium nickel oxides, while lithium manganese oxides have low capacity and conductivity issues.

Innovation Solution

A lithium-transition metal composite oxide with a specific composition, including excess lithium and nickel with an oxidation number of at least 2, along with manganese and cobalt, is used to maintain a stable crystal structure and enhance rate characteristics by controlling the average oxidation number of transition metals and adjusting molar ratios to ensure lithium ion mobility.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If lithium cobalt oxide (LiCoO2) is used as cathode active material, then excellent lifespan and charge/discharge efficiency are achieved, but cost increases significantly due to expensive cobalt

Engineering Contradiction:
Improvelifespan and charge/discharge efficiencyVSAvoidcost
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent uses a composite oxide material with formula Li1+aNi1/2-bMn1/2+bO2, combining nickel and manganese in specific ratios within a lithium oxide matrix. This composite approach achieves the desired performance while controlling cost by optimizing the mix of expensive (nickel) and inexpensive (manganese) transition metals.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent systematically varies compositional parameters (a, b values representing lithium excess and nickel-manganese ratio) to optimize performance. By changing these parameters, the material achieves excellent lifespan and efficiency comparable to LiCoO2 while using cheaper nickel-manganese composition.

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If lithium nickel oxide (LiNiO2) is used to reduce cost and increase discharge capacity, then cost and capacity improve, but crystal structure stability deteriorates due to phase transfer under charge/discharge cycles

Engineering Contradiction:
Improvedischarge capacityVSAvoidcrystal structure stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The patent creates a composite oxide Li1+aNi1/2-bMn1/2+bO2 that combines nickel (providing high capacity) with manganese (providing structural stability). The synergistic combination allows the material to maintain crystal structure stability while achieving high discharge capacity comparable to pure lithium nickel oxide.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent optimizes the local composition by controlling the nickel-to-manganese ratio parameter (b) to create specific regions with different properties. This allows high-capacity nickel-rich regions coexist with stability-providing manganese-rich regions within the same crystal structure.

Inventive Principle:
Principle #3Local quality

3Temperature

If lithium manganese oxide (LiMnO2 or LiMn2O4) is used to achieve low cost and excellent thermal stability, then cost and thermal stability improve, but discharge capacity and conductivity decrease

Engineering Contradiction:
Improvethermal stabilityVSAvoiddischarge capacity and conductivity
Core Design Contradiction:
TemperatureVSQuantity of substance

Solution Approach 1:

The patent develops a composite oxide Li1+aNi1/2-bMn1/2+bO2 that integrates manganese (providing thermal stability) with nickel (providing high capacity and conductivity). The composite structure allows the material to simultaneously achieve excellent thermal stability and high discharge capacity with good conductivity.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent optimizes compositional parameters to balance thermal stability and performance. By adjusting the nickel-manganese ratio and lithium excess parameter, the material achieves optimal combination of thermal stability, discharge capacity, and conductivity that surpasses conventional lithium manganese oxides.

Inventive Principle:
Principle #35Parameter changes

4Reliability

If excess lithium is added to improve rate characteristics and maintain stable crystal structure, then rate characteristics and structural stability improve, but manufacturing precision requirements increase

Engineering Contradiction:
Improverate characteristics and structural stabilityVSAvoidcompositional control precision
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The patent defines specific parameter ranges (0 < a ≤ 0.4 and 0 < b ≤ 0.25) that guarantee optimal performance. These quantified parameters provide clear manufacturing targets, making it easier to control composition within acceptable tolerances while achieving excellent rate characteristics and structural stability.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent intentionally adds excess lithium (parameter a) beyond stoichiometric requirements to ensure complete occupation of lithium sites and maintain structural stability during cycling. This deliberate excess compensates for potential lithium loss during manufacturing and cycling, ensuring consistent performance.

Inventive Principle:
Principle #16Partial or excessive action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution provides a cathode active material with improved stability and enhanced rate characteristics under high-rate charge/discharge conditions, maintaining a stable crystal structure and increasing the coulombic force between transition metals and oxygen, resulting in superior performance compared to conventional materials.

Implementation Method 1

increasing the coulombic force between transition metals and oxygen

Methodology Applied
Scientific EffectCoulombic force: Coulomb's Law

Implementation Method 2

lithium-transition metal composite oxide... stable crystal structure

Methodology Applied
Scientific EffectIonic bonding: Chemical Bonding

Implementation Method 3

ensure lithium ion mobility

Methodology Applied
Scientific EffectIon diffusion: Diffusion

Data Source

PatentEP2206182B1Cathode active material for lithium secondary battery
Publication Date: 2019.04.24 LG CHEM LTD
  • EP2206182B1 patent drawingFigure 1~2
  • EP2206182B1 patent drawingFigure 3~4
  • EP2206182B1 patent drawingFigure 5~6

AI summary

Provided is a cathode active material for a lithium secondary battery, including a lithium-transition metal composite oxide represented by the following formula (1), which contains an excess of lithium, so as to exhibit enhanced rate characteristics under high rate charge/discharge conditions: Lii+aNi'bNi"cMndCoeO2 (1) wherein each of a, b, c, d and e has the same meaning as defined in the disclosure. The cathode active material according to the present invention includes an excess of lithium and, different from conventional technologies, a lithium-transition metal composite oxide containing a nickel element with a predetermined oxidation number, so that the active material exhibits a stable crystal structure and excellent rate characteristics under high rate charge/discharge conditions.