Localized Melt Infiltration for Ceramic Matrix Composites

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Solution Overview

Problem

Melt-infiltration processes for producing reinforced ceramic matrix composites are time-consuming and energy-intensive, and conducting these processes in a vacuum can lead to non-uniform infiltration and defects due to vaporization of the molten metal alloy infiltrant, especially in high-temperature structural applications.

Innovation Solution

A method involving localized heating of a green ceramic matrix composite article using a heat source such as a laser or electric arc to melt and introduce a metal alloy infiltrant into the interstices of the reinforcing structure, allowing capillary action to draw the infiltrant and improve infiltration efficiency, which can be conducted in an inert environment at atmospheric pressure to reduce vaporization.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional melt-infiltration processes are used to produce CMCs, then the composite articles can be formed with reinforced structure, but the process is time consuming and energy intensive

Engineering Contradiction:
Improveinfiltration process speedVSAvoidenergy consumption
Core Design Contradiction:
ProductivityVSUse of energy by moving object

Solution Approach 1:

The patent applies segmentation by dividing the infiltration process into localized regions rather than treating the entire green composite article uniformly. The molten infiltrant is introduced at specific locations and allowed to propagate through capillary action, enabling parallel processing of multiple regions and significantly reducing overall process time and energy consumption.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent implements local quality by applying heat and introducing infiltrant to specific localized regions of the green composite article rather than uniformly across the entire article. This allows different regions to be processed at different times and with different parameters, improving both speed and energy efficiency by focusing resources only where needed.

Inventive Principle:
Principle #3Local quality

2Manufacturing precision

If the infiltration process is conducted in a vacuum, then the molten metal alloy infiltrant can be introduced effectively, but vaporization of the infiltrant occurs causing non-uniform infiltration and defects

Engineering Contradiction:
Improveinfiltration uniformityVSAvoidvaporization of infiltrant
Core Design Contradiction:
Manufacturing precisionVSObject-affected harmful factors

Solution Approach 1:

The patent employs an inert atmosphere (such as argon or nitrogen) instead of vacuum to prevent vaporization of the molten infiltrant. The inert gas environment suppresses vapor pressure and prevents oxidation and other harmful reactions, allowing the infiltrant to remain in liquid state and infiltrate uniformly without defects while still enabling effective introduction of the molten alloy.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

Solution Approach 2:

The patent changes the environmental parameters from vacuum to inert atmosphere at controlled pressure, which fundamentally alters the vapor-liquid equilibrium of the infiltrant. This parameter change prevents vaporization while maintaining the fluidity and infiltrability of the molten alloy, achieving uniform infiltration without the harmful effects of vacuum processing.

Inventive Principle:
Principle #35Parameter changes

3Adaptability or versatility

If batch processing is used for melt-infiltration, then the process is simple to operate, but it does not allow in-situ process modifications to account for unexpected deviations

Engineering Contradiction:
Improveprocess modification capabilityVSAvoidprocess control system
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The patent implements feedback control by monitoring the infiltration process in real-time and allowing for in-situ modifications. Sensors detect parameters such as infiltrant flow rate, temperature, and infiltration progress, and this information is used to adjust process parameters dynamically, enabling the system to adapt to unexpected deviations while maintaining relatively simple operational procedures.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The patent transforms the static batch process into a dynamic process where parameters can be adjusted during infiltration. The system allows real-time modification of infiltrant introduction rate, heating rate, and atmospheric conditions based on actual process conditions, providing adaptability without requiring complex reconfiguration of the basic batch processing framework.

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method enhances the speed and energy efficiency of the infiltration process, enabling more precise control over infiltration parameters to achieve uniform densification and reduce defects, resulting in a densified ceramic composite article with minimal porosity.

Implementation Method 1

heating a localized region of the green composite article with a heat source

Methodology Applied
Scientific EffectLocalized heating: Heating

Implementation Method 2

melting a metal alloy infiltrant to form a molten metal alloy

Methodology Applied
Scientific EffectMelting: Melting

Implementation Method 3

capillary action draws the molten alloy infiltrant into the region

Methodology Applied
Scientific EffectCapillary action: Capillary Action

Implementation Method 4

The molten metal alloy infiltrant enters and occupies the interstices between the supporting structure of the green ceramic article

Methodology Applied
Scientific EffectInfiltration: Absorption (physical)

Data Source

PatentUS10834790B2Method for making ceramic matrix composite articles with progressive melt infiltration
Publication Date: 2020.11.10 ROLLS ROYCE HIGH TEMPERATURE COMPOSITES INC
  • US10834790B2 patent drawing
  • US10834790B2 patent drawing

AI summary

A method of melt infiltrating a green ceramic matrix composite (CMC) article, wherein the green CMC article includes a ceramic reinforcing structure. The method includes heating a localized region of the green CMC article; melting a metal alloy infiltrant to form a molten metal alloy; and introducing the molten metal alloy into the localized region to infiltrate the reinforcing structure of the green CMC article with the metal alloy infiltrant and form the CMC article.