Low Migration Energy Curable Inks for UV LED Curing

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Solution Overview

Problem

Conventional UV ink systems are not suitable for high-speed printing with UV LED lamps, as they often fail to cure due to energy absorption by white pigments, leading to incomplete photopolymerization and potential contamination from residual monomers and photodecomposition products, particularly in food packaging applications.

Innovation Solution

The development of energy curable ink and coating compositions comprising 2-30 wt% 3-methyl-1,5-pentanediol diacrylate, photoinitiators, optical brightening agents, and minimal organic solvents, optimized for UV LED curing, ensuring low migration and adhesion to flexible substrates, and suitable for various energy curing methods.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Device complexity

If conventional UV ink systems are used with UV LED lamps, then the printing process can be simplified, but the ink fails to cure properly due to energy absorption by white pigments

Engineering Contradiction:
Improveprinting process complexityVSAvoidcuring effectiveness
Core Design Contradiction:
Device complexityVSReliability

Solution Approach 1:

The patent modifies the chemical composition parameters of the ink system by incorporating specific photoinitiators (Types I and II), monomers, and oligomers that are optimized for UV LED wavelengths. This parameter change enables the ink to cure effectively under UV LED lamps despite the presence of white pigments that absorb energy.

Inventive Principle:
Principle #35Parameter changes

2Ease of operation

If high amounts of monofunctional monomers are used in cured inks, then the ink achieves good printability and flow, but residual monomers migrate and contaminate the packaged product

Engineering Contradiction:
ImproveprintabilityVSAvoidmigration contamination
Core Design Contradiction:
Ease of operationVSObject-affected harmful factors

Solution Approach 1:

The patent creates a composite monomer system combining monofunctional and multifunctional monomers/oligomers. This composite approach allows the ink to maintain good printability from the monofunctional components while the multifunctional components provide crosslinking that reduces residual monomer content and migration, thus eliminating contamination.

Inventive Principle:
Principle #40Composite materials

3Object-affected harmful factors

If UV LED lamps are used for curing, then heat generation and ozone production are reduced, but the ink must be optimized for specific wavelengths which limits compatibility

Engineering Contradiction:
Improveheat and ozone generationVSAvoidink system compatibility
Core Design Contradiction:
Object-affected harmful factorsVSAdaptability or versatility

Solution Approach 1:

The patent develops a universal ink formulation that can be cured by multiple energy sources including UV LED lamps, conventional UV lamps, and electron beam irradiation. The ink system incorporates photoinitiators and monomers that respond to different wavelengths and energy types, making it adaptable to various curing technologies while maintaining the benefits of reduced heat and ozone generation.

Inventive Principle:
Principle #6Universality (Multi-functionality)

4Quantity of substance

If white pigment is added to achieve opaque white ink, then coverage and opacity are improved, but energy absorption increases preventing proper curing

Engineering Contradiction:
Improveopacity and coverageVSAvoidenergy available for photopolymerization
Core Design Contradiction:
Quantity of substanceVSUse of energy by moving object

Solution Approach 1:

The patent introduces photoinitiators as intermediary substances that absorb UV LED energy and transfer it to trigger polymerization. These photoinitiators act as mediators between the UV LED light source and the monomer/oligomer system, enabling curing to proceed even in the presence of white pigments that would otherwise block the energy transfer.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The ink and coating compositions achieve excellent cure, printability, and resistance to isopropanol rubs, with high adhesion to flexible substrates, while minimizing contamination and ensuring effective curing across different energy curing technologies, including UV LED, standard UV, and electron beam.

Implementation Method 1

Energy curable inks and coatings are often used in the printing of food packaging... Energy curing is faster and more efficient than conventional curing means... UV LED (light emitting diode) chip technology has grown considerably... wavelengths important for photo-polymerization of UV-sensitive inks

Methodology Applied
Scientific EffectPhotopolymerization: Photopolymerisation

Implementation Method 2

the optical brightening agent is a fluorescent brightening agent

Methodology Applied
Scientific EffectFluorescence: Fluorescence

Data Source

PatentEP3681938B1Low migration energy curable inks
Publication Date: 2024.12.18 SUN CHEMICAL CORP

AI summary

The present invention provides energy curable ink and coating compositions that comprise polymerizable compounds, photoinitiators, and colorants. The polymerizable compounds comprise one or more polymerizable monomers and/or oligomers, wherein at least a portion is 3-methyl-1,5-pentanediol diacrylate. The inks and coatings of the invention exhibit excellent print properties after UV-LED, standard UV mercury vapor lamp, and electron beam cure.