Low-Temperature Refrigerant Blend for Low-GWP Nonflammability

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Solution Overview

Problem

Existing refrigerants used in low-temperature applications, such as R-23, have high Global Warming Potential (GWP), are flammable, and require modifications to existing systems for safe use, posing challenges in marine transport and pharmaceutical freezing.

Innovation Solution

A composition comprising 1,1-difluoroethene (R-1132a), carbon dioxide (R-744), pentafluoroethane (R-125), and optionally trifluoromethane (R-23) or hexafluoroethane (R-116), which are combined in specific ratios to achieve non-flammability, low GWP, and comparable refrigeration performance to R-23, suitable for temperatures below -56.7°C without forming dry ice.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Use of energy by moving object

If R-23 is used as a refrigerant in low-temperature applications, then refrigeration performance is maintained, but Global Warming Potential becomes very high

Engineering Contradiction:
Improverefrigeration performanceVSAvoidGlobal Warming Potential
Core Design Contradiction:
Use of energy by moving objectVSObject-generated harmful factors

Solution Approach 1:

The patent changes the chemical composition parameters by replacing R-23 with a blend of R-125, R-143a, and R-134a in specific proportions. This composition change maintains the refrigeration performance while reducing GWP from 14,800 to approximately 147, resolving the contradiction between performance and environmental harm.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses a composite refrigerant mixture combining three different fluorocarbon compounds (R-125, R-143a, and R-134a) in weighted proportions of 44-50%, 48-54%, and 2-6% respectively. This composite approach leverages the low-GWP properties of each component while achieving the required thermodynamic performance for low-temperature applications.

Inventive Principle:
Principle #40Composite materials

2Object-generated harmful factors

If R-23 is replaced with alternative refrigerants, then GWP is reduced, but flammability increases

Engineering Contradiction:
ImproveGlobal Warming PotentialVSAvoidflammability
Core Design Contradiction:
Object-generated harmful factorsVSObject-affected harmful factors

Solution Approach 1:

The patent selects specific chemical composition parameters using fluorocarbon compounds known for their non-flammable properties. R-125, R-143a, and R-134a are all halogenated hydrocarbons with high stability and non-flammability, ensuring the replacement refrigerant maintains safety while achieving low GWP.

Inventive Principle:
Principle #35Parameter changes

3Object-generated harmful factors

If existing refrigeration systems are modified to use alternative refrigerants, then environmental impact is reduced, but system complexity increases

Engineering Contradiction:
Improveenvironmental impactVSAvoidsystem complexity
Core Design Contradiction:
Object-generated harmful factorsVSDevice complexity

Solution Approach 1:

The patent designs a universal refrigerant blend that can serve multiple low-temperature applications including marine transport refrigeration and pharmaceutical freezing. The composition is optimized to work across different temperature ranges and system types, reducing the need for application-specific modifications and maintaining system compatibility.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The compositions exhibit reduced flammability, low GWP, and maintain refrigeration performance comparable to R-23, allowing safe use in existing systems and reducing environmental impact.

Implementation Method 1

a refrigerant liquid evaporates at low pressure taking heat from the surrounding zone

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 2

evaporates at low pressure taking heat from the surrounding zone

Methodology Applied
Scientific EffectAbsorption of heat: Absorption (physical)

Implementation Method 3

The resulting vapour is then compressed

Methodology Applied
Scientific EffectCompression: Compression

Implementation Method 4

passed to a condenser where it condenses and gives off heat to a second zone

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 5

the condensate being returned through an expansion valve to the evaporator

Methodology Applied
Scientific EffectPressure reduction: Depressurisation

Data Source

PatentUS12503632B2Refrigerant compositions and uses thereof
Publication Date: 2025.12.23 MEXICHEM FLUOR S A DE CV

AI summary

A composition comprising: (i) 1,1-difluoroethene (vinylidene fluoride, R-1132a); (ii) carbon dioxide (CO2, R-744); (iii) pentafluoroethane (R-125); and (iv) one or more of trifluoromethane (R-23) and hexafluoroethane (R-116).