Lyophilized Reagent Storage in Microfluidic Devices

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Solution Overview

Problem

Conventional microfluidic devices face challenges in storing reagents in a liquid state, which complicates rapid and simultaneous performance of multiple pathological tests, requiring skilled personnel and large equipment, and existing solutions like lyophilized beads or pellets have limitations in efficiency and compatibility.

Innovation Solution

A method of loading liquid reagents into microfluidic devices and lyophilizing them using a freezing and drying process, including sublimation, to create a stable form that can be easily dissolved, with the option to add fillers and surfactants for improved reagent storage and compatibility.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Speed

If reagents are stored in liquid state in microfluidic device, then rapid analysis can be performed, but storage stability deteriorates and device complexity increases

Engineering Contradiction:
Improveanalysis speedVSAvoidreagent storage stability
Core Design Contradiction:
SpeedVSStability of the object's composition

Solution Approach 1:

The patent applies parameter changes by transitioning the reagent from liquid state to lyophilized (freeze-dried) state, altering its physical properties to achieve long-term storage stability while maintaining rapid analysis capability when rehydrated with the biological sample

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent implements preliminary action by pre-loading lyophilized reagents into the microfluidic device during manufacturing, so that the device is ready for rapid analysis without requiring reagent preparation at the time of use, thus achieving both speed and stability

Inventive Principle:
Principle #10Preliminary action

2Stability of the object's composition

If lyophilized beads are used as disclosed in US 5,776,563, then reagent storage is improved, but manufacturing complexity and cost increase

Engineering Contradiction:
Improvereagent storage stabilityVSAvoiddevice manufacturing ease
Core Design Contradiction:
Stability of the object's compositionVSEase of manufacture

Solution Approach 1:

The patent extracts the reagent from its traditional liquid formulation and converts it to lyophilized powder form, which can be directly loaded into the device during manufacturing without requiring separate bead formation processes, thereby improving manufacturability while maintaining storage stability

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent makes the microfluidic device itself serve multiple functions: it acts as both the reaction chamber and the storage container for lyophilized reagents, eliminating the need for separate reagent delivery mechanisms and simplifying the overall device structure

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Measurement precision

If conventional large automated equipment is used, then test accuracy is improved, but device size and cost increase

Engineering Contradiction:
Improvetest accuracyVSAvoiddevice size
Core Design Contradiction:
Measurement precisionVSVolume of stationary object

Solution Approach 1:

The patent segments the large automated testing system into a compact microfluidic device that integrates sample processing, reagent mixing, and analysis functions in a single chip-scale platform, maintaining accuracy through precise microfluidic control while dramatically reducing device size

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent replaces complex mechanical systems with microfluidic principles, using pressure-driven flow and capillary action to transport fluids and mix reagents, thereby achieving accurate analysis in a compact device without large mechanical components

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method allows for efficient storage and easy dissolution of reagents, enabling rapid and accurate biochemical analysis with improved economic efficiency and compatibility, reducing the need for large equipment and skilled personnel, and facilitating the manufacture of devices for multiple testing items.

Implementation Method 1

The lyophilizing may include a freezing process and a drying process, the drying process using sublimation in at least some portions of the drying process.

Methodology Applied
Scientific EffectSublimation: Sublimation

Implementation Method 2

The lyophilizing may include a freezing process and a drying process

Methodology Applied
Scientific EffectFreezing: Freezing

Data Source

PatentEP2080554B1Method of storing analytical reagent into microfluidic device
Publication Date: 2013.03.20 SAMSUNG ELECTRONICS CO LTD
  • EP2080554B1 patent drawingFigure 1
  • EP2080554B1 patent drawingFigure 2
  • EP2080554B1 patent drawingFigure 3

AI summary

Provided is a method of storing a reagent in a microfluidic device. The reagent, in a liquid form, is loaded into reaction chambers arranged on the microfluidic device; followed by lyophilization as being contained in the microfluidic device.