Mass Spectrum Partial Structure Estimation Using Fragment Peaks

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Solution Overview

Problem

Current methods for estimating partial structures of unknown compounds from mass spectra lack precision, particularly in distinguishing fragment peaks from other signals, leading to degraded estimation accuracy.

Innovation Solution

A partial structure estimation apparatus and method that generate explanatory variables from peak and peak interval compositions using machine learning, focusing solely on fragment peaks to improve estimation precision by registering and generating models based on known compounds' mass spectra.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If all peaks in the mass spectrum are used for partial structure estimation, then the estimation can be performed using available data, but the precision is degraded due to interference from non-fragment peaks

Engineering Contradiction:
Improvepartial structure estimation precisionVSAvoidinterference from non-fragment peaks
Core Design Contradiction:
Measurement precisionVSObject-affected harmful factors

Solution Approach 1:

The mass spectrum peaks are segmented into fragment peaks and non-fragment peaks based on their characteristics. The estimation model processes only the fragment peak data, separating the useful information from interfering signals to improve estimation precision.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The method extracts and selects only the fragment peaks from the complete set of mass spectrum peaks. By taking out the relevant fragment peak information and excluding non-fragment peaks, the model achieves more accurate partial structure estimation without interference from irrelevant signals.

Inventive Principle:
Principle #2Taking out (Extraction)

Data Source

PatentEP4235681A1Partial structure estimation apparatus and method of generating partial structure estimation model
Publication Date: 2023.08.30 JEOL LTD
  • EP4235681A1 patent drawingFigure 1
  • EP4235681A1 patent drawingFigure 2
  • EP4235681A1 patent drawingFigure 3

AI summary

A partial structure estimation apparatus (20) is configured to generate a first explanatory variable by performing composition estimation for each peak in a mass spectrum acquired from a sample, and to generate a second explanatory variable by performing composition estimation for each peak interval in the mass spectrum. The partial structure estimation apparatus (20) is further configured to then estimate a partial structure as an objective variable based on the first explanatory variable and the second explanatory variable. In a partial structure estimation model generation apparatus (12), a partial structure estimation model (18) is generated through machine learning using a training data set.