Inverted T-Shaped MBE Chamber Under Vector Magnetic Field

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Solution Overview

Problem

Current molecular beam epitaxy systems face challenges in growing high-quality spin semiconductor materials with uniform magnetic domain structures and efficient spin current polarization due to limitations in magnetic field control, interface quality, and surface contamination during characterization.

Innovation Solution

A molecular beam epitaxy system under a vector strong magnetic field with an inverted T-shaped ultrahigh vacuum growth and characterization chamber, equipped with a liquid-helium-free spiral magnet, dual-layer cooling, and in-situ characterization apparatus, allowing for precise control of magnetic fields and atomic-scale growth, and enabling in-situ characterization to avoid surface contamination.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If multiple components are equipped in the chamber to achieve fine growth of magnetic thin film material and in-situ characterization, then the growth quality and characterization precision are improved, but the device complexity increases

Engineering Contradiction:
Improvegrowth qualityVSAvoiddevice complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent combines multiple evaporation sources, ion sources, and in-situ characterization apparatus into a single integrated molecular beam epitaxy chamber. This merging approach allows all components to share the same ultrahigh vacuum environment and strong magnetic field, achieving fine growth quality and in-situ characterization capability while avoiding the need for separate systems.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The chamber is designed as a multi-functional system that simultaneously performs molecular beam epitaxy growth, in-situ transport characterization, and spin electron transport measurement. The strong magnetic field chamber serves multiple purposes: providing magnetic field for spin control, maintaining ultrahigh vacuum for clean growth, and enabling in-situ measurements without sample exposure to air.

Inventive Principle:
Principle #6Universality (Multi-functionality)

2Force

If the strong magnet chamber size is kept small (inner diameter smaller than 10 cm), then the magnetic field strength is improved, but the space for accommodating multiple components is reduced

Engineering Contradiction:
Improvemagnetic field strengthVSAvoidchamber volume
Core Design Contradiction:
ForceVSVolume of moving object

Solution Approach 1:

The patent employs a vertical chamber configuration where evaporation sources and ion sources are positioned above the substrate, utilizing the vertical dimension rather than horizontal space. This allows multiple components to be accommodated in a compact horizontal footprint while maintaining strong magnetic field strength, as the chamber height can be extended without increasing the magnetic field chamber's horizontal dimensions.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

3Measurement precision

If the sample is exposed to air for spin detection, then the detection capability is improved, but the surface contamination increases and spin characteristics are influenced

Engineering Contradiction:
Improvedetection capabilityVSAvoidsurface contamination
Core Design Contradiction:
Measurement precisionVSObject-affected harmful factors

Solution Approach 1:

The patent implements in-situ transport characterization that allows spin detection to be performed within the ultrahigh vacuum chamber without breaking vacuum or exposing the sample to air. The chamber maintains vacuum conditions throughout the growth and characterization process, preventing surface contamination while enabling spin electron transport measurement through the chamber wall using external probes.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system achieves high-quality spin semiconductor growth with extended spin relaxation time and polarization, enabling precise control and characterization of spin electron transport, overcoming previous limitations in magnetic field control and surface contamination.

Implementation Method 1

molecular beam epitaxy under vector strong magnetic field

Methodology Applied
Scientific EffectMagnetic field: Magnetic Field

Implementation Method 2

improving larmor procession of spin electrons

Methodology Applied
Scientific EffectLarmor precession:

Implementation Method 3

the magnetic moment of the material is basically parallel to the plane of the thin film

Methodology Applied
Scientific EffectMagnetic moment alignment: Magnetism

Implementation Method 4

molecular beam epitaxy under vector strong magnetic field

Methodology Applied
Scientific EffectMolecular beam epitaxy: Epitaxy

Implementation Method 5

molecular beam epitaxial growth of the thin film material can be realized

Methodology Applied
Scientific EffectPhysical vapor deposition: Physical Vapour Deposition

Implementation Method 6

the free path of molecules would be increased significantly (an average free path of the molecules can reach tens of meters under the vacuum of 10−4 Pa)

Methodology Applied
Scientific EffectVacuum: Vacuum

Implementation Method 7

the free path of molecules would be increased significantly

Methodology Applied
Scientific EffectMean free path:

Implementation Method 8

the in-situ transport characterization of the sample is performed in an ultrahigh vacuum environment with strong magnetic field

Methodology Applied
Scientific EffectIn-situ measurement:

Implementation Method 9

the spin detection is generally carried out outside the sample preparation chamber

Methodology Applied
Scientific EffectSpin detection:

Data Source

PatentUS10738394B2Molecular beam epitaxy under vector strong magnetic field and in-situ characterization apparatus thereof
Publication Date: 2020.08.11 XIAMEN UNIV
  • US10738394B2 patent drawing
  • US10738394B2 patent drawing
  • US10738394B2 patent drawing

AI summary

The present invention discloses a molecular beam epitaxy under vector strong magnetic field and an in-situ characterization apparatus thereof. The apparatus mainly consists of an inverted T-shaped ultrahigh vacuum growth and characterization chamber with a compact structure and a strong magnet. The inverted T-shaped vacuum chamber portion, which disposed in the room-temperature chamber of the strong magnet, includes a compact epitaxial growth sample stage, a device capable of rotating angle between the growth and magnetic field directions, and an in-situ characterization apparatus. The portion disposed below the strong magnet includes a molecular beam source component such as evaporation source, plasma source etc., and a vacuum-pumping system. The present invention surmounts effectively the technical problems between the small volume of the strong magnetic field chamber and numerous components of the growth and test system, and realizes the molecular beam epitaxial growth and in-situ characterization under the strong magnetic field.