MCrAlX Coating Diffusion Barrier for Superalloy Lifetime

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Solution Overview

Problem

Current MCrAlY coatings used in gas turbines face limitations due to suboptimal yttrium content, high sulfur content, and rising costs of rare earth elements, leading to accelerated oxidation, corrosion, and reduced coating lifetime, especially at high temperatures.

Innovation Solution

The introduction of minor elements like ruthenium, iridium, molybdenum, silicon, hafnium, and tantalum reduces the need for yttrium, forming a diffusion barrier and minimizing interdiffusion, while keeping sulfur content below 10ppm, resulting in an MCrAlX alloy coating with improved thermal stability and mechanical durability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If high yttrium content is used in MCrAlY coatings to achieve pegging and scavenge effects for oxidation and corrosion resistance, then oxidation and corrosion resistance is improved, but yttrium oxide inclusions provide fast oxygen diffusion routes that accelerate oxidation and coating lifetime is reduced

Engineering Contradiction:
Improveoxidation and corrosion resistanceVSAvoidcoating lifetime
Core Design Contradiction:
ReliabilityVSDuration of action of stationary object

Solution Approach 1:

The patent optimizes the yttrium content parameter to a specific range (0.5-5 wt%) rather than using high amounts, and introduces additional minor elements (re 0.1-1.0 wt%, ta 0.1-1.0 wt%, hb 0.1-1.0 wt%) to achieve the desired protection without forming excessive yttrium oxide inclusions that accelerate oxidation

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite coating system combining MCrAlY base alloy with multiple minor elements (yttrium, rhenium, tantalum, hafnium, and optionally others like iridium, ruthenium, silicon, molybdenum, nickel, cobalt, manganese, boron, carbon, nitrogen, oxygen, sulfur, phosphorus, zinc, magnesium, calcium, strontium, barium). This composite approach provides synergistic effects where multiple elements work together to enhance oxidation resistance while controlling yttrium oxide formation

Inventive Principle:
Principle #40Composite materials

2Ease of manufacture

If high sulfur content (>10ppm) is present in MCrAlY coating to reduce manufacturing costs, then coating production is easier, but coating lifetime is shortened

Engineering Contradiction:
Improvecoating productionVSAvoidcoating lifetime
Core Design Contradiction:
Ease of manufactureVSDuration of action of stationary object

Solution Approach 1:

The patent strictly controls the sulfur content parameter to be below 10 ppm (specifically 0.001-10 ppm), representing a significant reduction from conventional coatings with >10 ppm sulfur. This parameter optimization eliminates the harmful effect of sulfur on coating lifetime while maintaining manufacturing feasibility through precise compositional control

Inventive Principle:
Principle #35Parameter changes

3Device complexity

If conventional MCrAlY coating composition is used to maintain simplicity, then device complexity is low, but interdiffusion between coating and superalloy substrates consumes aluminum reservoir rapidly reducing coating lifetime

Engineering Contradiction:
Improvecoating composition complexityVSAvoidcoating lifetime
Core Design Contradiction:
Device complexityVSDuration of action of stationary object

Solution Approach 1:

The patent develops a composite MCrAlX alloy coating system with base elements (Ni: 50-80 wt%, Co: 0-30 wt%, Al: 5-20 wt%, Cr: 5-15 wt%) and multiple minor elements (re 0.1-1.0 wt%, ta 0.1-1.0 wt%, hb 0.1-1.0 wt%, and optional additional elements). This composite composition creates a more stable diffusion barrier that reduces aluminum reservoir consumption through interdiffusion while maintaining a manageable compositional structure

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The minor elements (re, ta, hb, and others) act as intermediary elements between the MCrAlY base coating and the superalloy substrate, forming a more effective diffusion barrier that slows down interdiffusion processes and reduces the consumption of the aluminum reservoir, thereby extending coating lifetime

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The MCrAlX coating system enhances temperature capacity and extends coating lifetime compared to conventional MCrAlY coatings, offering superior oxidation resistance and mechanical durability with reduced rare earth element usage and sulfur content.

Implementation Method 1

The introduction of minor elements like ruthenium, iridium, molybdenum, silicon, hafnium, and tantalum reduces the need for yttrium, forming a diffusion barrier and minimizing interdiffusion

Methodology Applied
Scientific EffectDiffusion barrier: Diffusion Barrier

Implementation Method 2

When further increasing engine efficiency, output power, availability and reliability in the current gas turbine development, this effort is often limited by temperature capacity and lifetime of protective coatings for protection against hot corrosion and oxidation

Methodology Applied
Scientific EffectThermal insulation: Thermal Insulation

Implementation Method 3

Today's MCrAlY coatings rely very much on yttrium incorporation to have so called pegging and scavenge effects to increase oxidation and corrosion resistance of the coatings

Methodology Applied
Scientific EffectOxidation resistance: Oxidation

Data Source

PatentEP2729598B1Coating, coating layer system, coated superalloy component
Publication Date: 2019.10.30 SIEMENS AG
  • EP2729598B1 patent drawingFigure 1~2

AI summary

The invention relates to a coating, a coating layer system and a coated superalloy component preferably to be used in a gas turbine's hot gas path. Today' s MCrAlY coatings rely very much on yttrium incorpora¬ tion to have so called pegging and scavenge effects to in- crease oxidation and corrosion resistance of the coatings. It is proposed following MCrAlX coatings consisting of: Nickel based coating consisting of: 15 to 40 wt% Co, 10 to 25 wt% Cr, 5 to 15 wt% Al, 0,05 to 1 wt% Y and/or at least one of elements from LA series, 0,05 to 8 wt% Ru or Fe, 0 to 1 wt% Ir, 0,05 to 5 wt% Mo, 0 to 3 wt% Si, 0 to 5 wt% Ta, 0 to 2 wt% Hf, and unavoidable impurities, and a balance of nickel. Cobalt based coating consisting of: 15 to 40 wt% Ni, 15 to 28 wt% Cr, 5 to 15 wt% Al, 0,05 to 1 wt% Y and/or at least one of elements from La series, 0,05 to 5 wt% Ru and/or Mo, 0 to 2 wt% Ir, 0 to 3 wt% Si, 0 to 5 wt% Ta, Hf and unavoidable impurities, and a balance of cobalt.