Melt Infiltration Barrier Controls CMC Microstructure

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Solution Overview

Problem

Current methods for manufacturing ceramic matrix composites (CMCs) face challenges in achieving uniform infiltration and controlling the infiltration process, leading to inconsistencies in microstructure and reduced component life due to limited control over infiltration parameters such as time and temperature.

Innovation Solution

The use of a higher melting point barrier material between the infiltrant source and the CMC component, which dissolves to establish fluid communication and control the infiltration process, ensuring uniform infiltration and microstructure formation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If a wick is used to transfer infiltrant to the composite body, then infiltration can be achieved, but control over infiltration parameters (time and temperature) is limited

Engineering Contradiction:
Improveinfiltration parameter controlVSAvoidapparatus structure
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

A barrier material with intermediate melting point is introduced between the infiltrant source and the composite body. This barrier acts as a mediator that controls the timing of infiltration by remaining solid during heating and only melting when the infiltrant begins to flow, thereby providing precise control over infiltration start time and duration without requiring complex apparatus modifications

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The barrier material's melting point is specifically selected to be between the composite body temperature and the infiltrant melting point. By changing the physical state of the barrier from solid to liquid at a controlled temperature, the infiltration process is precisely timed and controlled, improving manufacturing precision without increasing device complexity

Inventive Principle:
Principle #35Parameter changes

2Manufacturing precision

If infiltrant is applied directly to the composite body, then infiltration occurs quickly, but microstructure uniformity and component density are compromised

Engineering Contradiction:
Improvemicrostructure uniformityVSAvoidinfiltration efficiency
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The barrier material is pre-positioned between the infiltrant source and the composite body before heating. During the heating process, the barrier remains solid and prevents premature infiltration. When the infiltrant temperature reaches the barrier's melting point, infiltration begins automatically, ensuring uniform microstructure formation while maintaining efficient infiltration timing

Inventive Principle:
Principle #10Preliminary action

3Manufacturing precision

If infiltration time is extended to improve density, then component degradation increases

Engineering Contradiction:
Improvecomponent densityVSAvoidcomposite body degradation
Core Design Contradiction:
Manufacturing precisionVSObject-affected harmful factors

Solution Approach 1:

The barrier material serves as a time-controlling intermediary that enables precise infiltration duration. By melting at a specific temperature, it automatically initiates and limits infiltration time, achieving high component density while preventing excessive exposure to molten infiltrant that would cause composite body degradation

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach results in higher density, longer component life, and improved mechanical performance of CMCs by allowing precise control over infiltration parameters, reducing degradation, and enhancing the uniformity of the microstructure.

Implementation Method 1

The use of a higher melting point barrier material between the infiltrant source and the CMC component, which dissolves to establish fluid communication

Methodology Applied
Scientific EffectDissolution: Solvation

Implementation Method 2

means for controlling fluid communications between the infiltrant source and the component

Methodology Applied
Scientific EffectFluid flow:

Data Source

PatentEP2970030B1Melt infiltration apparatus and method for molten metal control
Publication Date: 2019.12.25 ROLLS ROYCE CORP
  • EP2970030B1 patent drawingFigure 1~2
  • EP2970030B1 patent drawingFigure 3~3A
  • EP2970030B1 patent drawingFigure 4~5

AI summary

A method and apparatus for providing molten metal infiltration into a component is provided.