Membrane Contactor Pressure Control for Acid Gas Wetting

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Membrane contactors for acid gas removal are adversely affected by pore wetting, leading to increased mass transport resistance and degradation of performance, with existing solutions being application-specific and not providing a universal solution.

Innovation Solution

A membrane contactor system where the feed gas pressure is maintained above the liquid absorbent pressure, allowing a portion of the gas to bubble through the liquid absorbent, with precise control of gas and liquid phase pressures to minimize wetting, and a regenerative system to recycle and strip acid gases from the absorbent.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Area of stationary object

If membrane contactor is used for acid gas removal, then large contacting area to volume ratio is achieved, but pore wetting occurs causing mass transport resistance increase

Engineering Contradiction:
Improvecontacting areaVSAvoidmembrane performance
Core Design Contradiction:
Area of stationary objectVSReliability

Solution Approach 1:

The patent changes the pressure parameter by maintaining gas phase pressure higher than liquid phase pressure, which reverses the traditional pressure differential approach. This parameter change prevents liquid from penetrating into membrane pores, thereby preventing pore wetting while maintaining the large contacting area advantage of membrane contactors.

Inventive Principle:
Principle #35Parameter changes

2Reliability

If selective top layer is added to prevent wetting, then pore wetting is reduced, but resistance to mass transfer increases

Engineering Contradiction:
Improvewetting resistanceVSAvoidmass transfer rate
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

Instead of modifying the membrane structure by adding a selective top layer, the patent changes the operating pressure parameters. By maintaining gas pressure higher than liquid pressure, the system prevents wetting through operational control rather than structural modification, thus avoiding the mass transfer resistance that would result from adding a dense protective layer.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If gas pressure is increased to prevent liquid penetration, then pore wetting is prevented, but gas bubbling through liquid increases

Engineering Contradiction:
Improvewetting preventionVSAvoidgas slippage
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent converts the potentially harmful gas slippage (unabsorbed gas bubbling through liquid) into a beneficial recirculating flow. The gas that bubbles through the liquid is collected and recirculated back to the gas inlet, transforming what would be a loss into a useful process feature that maintains pressure differential and prevents wetting.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The system implements feedback by recirculating the gas that bubbles through the liquid back to the gas inlet. This feedback loop ensures continuous maintenance of the pressure differential across the membrane and optimizes the balance between preventing wetting and minimizing gas slippage losses.

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively prevents wetting, maintaining high efficiency over time by ensuring membrane fibers remain immersed in liquid and allowing controlled gas slippage, which improves overall process performance and extends membrane contactor lifespan.

Implementation Method 1

the liquid absorbent absorbs the at least one gas from the mixed gaseous feed stream

Methodology Applied
Scientific EffectAbsorption: Absorption (physical)

Implementation Method 2

The absorption is based on the chemical reaction between the selected amine and gas molecules

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 3

a porous membrane which divides the absorption module into a gas-feed chamber and an absorbent chamber

Methodology Applied
Scientific EffectPermeation: Permeation

Implementation Method 4

Desorbing said at least one gas from the rich liquid absorbent in the second membrane contactor

Methodology Applied
Scientific EffectDesorption: Desorption

Data Source

PatentEP3765172B1Membrane contactor
Publication Date: 2022.06.22 SAUDI ARABIAN OIL CO
  • EP3765172B1 patent drawingFigure 1
  • EP3765172B1 patent drawingFigure 2
  • EP3765172B1 patent drawingFigure 3

AI summary

A membrane contactor for separating components from a feed gas stream comprises a housing, a feed gas inlet for receiving the feed gas stream at a first pressure, and a liquid inlet or receiving a stream of liquid at a second pressure, the liquid containing an absorbent for reacting components of the gas stream and a slip gas outlet. The contactor also includes a plurality of fibers with pore channels in contact with the feed gas incoming from the gas inlet on a first side, and in contact with liquid incoming from the liquid inlet on a second side, producing a gas-liquid interface at the pore channels. Liquid is prevented from wetting the pore channels by maintaining the first pressure of the gas stream higher than the liquid stream, and a portion of the gas stream bubbles through as slip gas into the liquid stream due to the elevated pressure.