Menthol Packaging Caking Prevention via Spherical Particle Design

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Solution Overview

Problem

Solid coolants like menthol compounds tend to cake and sublime, leading to packaging and transportation challenges, which can result in hazardous goods classification and increased costs.

Innovation Solution

Standard packaging with specific filling instructions, such as not exceeding 50% volume and 10 kg weight, and using menthol compounds with characteristics like low fines content, favorable surface-to-volume ratio, and curved smooth surfaces, allows for storage and transport without caking, eliminating the need for mechanical treatment and hazardous packaging.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If solid coolants like menthol compounds are packaged in conventional packaging, then packaging and transportation costs increase and hazardous goods classification occurs, but caking and sublimation problems arise

Engineering Contradiction:
Improvepackaging simplicityVSAvoidproduct stability
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The patent changes the physical parameters of menthol compounds by controlling crystal modification (α-modification with melting point 42.5°C), particle size (0.1-2.0mm), and shape (spherical with smooth surface). These parameter changes reduce caking tendency and allow conventional packaging without hazardous goods classification

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite material system by combining menthol compounds with specific additives (0.1-10% by weight) such as waxes, fatty acids, or surfactants. This composite approach modifies the surface properties and reduces sublimation, enabling stable storage in conventional packaging

Inventive Principle:
Principle #40Composite materials

2Reliability

If menthol compounds are processed with aids such as release agents, then caking is prevented, but product purity and quality are compromised

Engineering Contradiction:
ImproveflowabilityVSAvoidproduct purity
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The patent achieves self-service by optimizing the inherent properties of menthol compounds themselves - controlling crystal modification to α-form, particle size to 0.1-2.0mm, and shape to spherical with smooth surfaces. The material's own properties prevent caking without requiring external release agents or additives

Inventive Principle:
Principle #25Self-service

3Manufacturing precision

If large crystals of menthol are produced through traditional crystallization, then product quality is maintained, but processing time and space requirements increase significantly

Engineering Contradiction:
Improvecrystal qualityVSAvoidspace-time yield
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The patent dramatically changes the particle size parameter from traditional large crystals (0.5-3cm) to fine particles (0.1-2.0mm). This parameter change is achieved through controlled crystallization processes that produce spherical particles with smooth surfaces, maintaining quality while increasing productivity by factors of 10-100 times

Inventive Principle:
Principle #35Parameter changes

4Volume of stationary object

If menthol compounds are stored at high filling heights, then packaging space is optimized, but caking increases under increased load and temperature

Engineering Contradiction:
Improvepackaging volume utilizationVSAvoidflowability
Core Design Contradiction:
Volume of stationary objectVSReliability

Solution Approach 1:

The patent applies spheroidality by producing spherical menthol particles with smooth surfaces. This spherical shape reduces contact area between particles, minimizing adhesion and caking forces. The curved surface geometry allows particles to roll rather than interlock, maintaining flowability even at high filling heights and temperatures

Inventive Principle:
Principle #14Spheroidality (Curvature)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Menthol compounds can be stored and transported in conventional packaging for at least 6 weeks without caking, reducing costs and avoiding hazardous goods classification, while maintaining product integrity.

Implementation Method 1

the melting points of these various modifications are between 33 and 43 °C... The melting point of the stable α-modification is therefore 42 to 43 °C

Methodology Applied
Scientific EffectMelting: Melting

Implementation Method 2

the high tendency of these substances to sublimate

Methodology Applied
Scientific EffectSublimation: Sublimation

Data Source

PatentEP4015075A1Standard packages with fixed cooling materials
Publication Date: 2022.06.22 SYMRISE GMBH & CO KG
  • EP4015075A1 patent drawingFigure 1
  • EP4015075A1 patent drawingFigure 2~6
  • EP4015075A1 patent drawingFigure 7

AI summary

Standard packaging with a maximum capacity of 25 l containing solid cooling agents is proposed, provided that (a) the packaging is filled with the cooling agents to a maximum of 50% by volume and (b) the amount of cooling agents in the packaging does not exceed a weight of 10 kg.