Metal Production via Alkoxide Electrolysis

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Solution Overview

Problem

Current methods for producing titanium and rare earth metals are costly and involve handling corrosive and difficult-to-work-with compounds like titanium chloride, necessitating a more efficient and less corrosive process.

Innovation Solution

The method involves converting titanium dioxide into titanium alkoxide, which is then electrolyzed in an electrolytic cell with an alkali-ion selective membrane to produce titanium metal and recoverable alkali metal alkoxide, reducing the need for additional reactants and simplifying the process.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If traditional methods are used to produce titanium metal from minerals like rutile, then titanium metal can be produced, but the process becomes expensive and involves handling corrosive compounds like titanium chloride

Engineering Contradiction:
Improveease of handling reaction materialsVSAvoidcorrosiveness of reaction materials
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The patent changes the chemical form of the titanium precursor from corrosive titanium chloride to non-corrosive titanium alkoxide. This parameter change in the chemical composition eliminates the harmful corrosive properties while maintaining the ability to produce titanium metal through electrolysis. The titanium alkoxide can be handled more easily and safely compared to traditional titanium chloride-based processes.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If traditional electrolytic processes are used, then metal production is achieved, but additional reactants are consumed and cannot be recovered

Engineering Contradiction:
Improveproduction efficiencyVSAvoidloss of reactants
Core Design Contradiction:
ProductivityVSLoss of substance

Solution Approach 1:

The patent implements a reactant recovery system where the alkali metal alkoxide produced during electrolysis is not discarded but instead recovered and reused as a reactant. The alkali metal ions migrate through the membrane and react with the titanium alkoxide to form titanium metal and alkali metal alkoxide, which can then be循环利用 in the process, reducing reactant consumption and waste.

Inventive Principle:
Principle #34Discarding and recovering

3Ease of manufacture

If conventional electrolytic cells are used, then electrolysis can be performed, but the process lacks reactant recovery and reuse mechanisms

Engineering Contradiction:
Improveprocess simplicityVSAvoidcomplexity of electrolytic cell structure
Core Design Contradiction:
Ease of manufactureVSDevice complexity

Solution Approach 1:

The patent introduces an alkali-ion selective membrane as an intermediary component in the electrolytic cell. This membrane selectively allows alkali metal ions to pass through while blocking other ions, enabling the recovery and reuse of alkali metal alkoxide. The membrane acts as a mediator that facilitates the separation and recovery process without significantly complicating the overall cell structure.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach reduces the corrosiveness of the reaction materials, makes the process more manageable, and allows for the recovery and reuse of reactants, potentially lowering production costs and improving efficiency.

Implementation Method 1

separating the cathode compartment from the anode compartment with an alkali-ion selective membrane that allows alkali metal ions to migrate from the anode compartment to the cathode compartment

Methodology Applied
Scientific EffectIon migration: Electrophoresis

Implementation Method 2

electrolyzing the electrolytic cell to cause alkali metal ions to migrate from the anode compartment into the cathode compartment and react with the metal alkoxide (M(OR) x ) thereby producing the metal

Methodology Applied
Scientific EffectElectrolysis: Electrolysis

Data Source

PatentEP2870277B1Apparatus and method of producing metal in a nasicon electrolytic cell
Publication Date: 2021.04.14 ENLIGHTEN INNOVATIONS INC
  • EP2870277B1 patent drawingFigure 1
  • EP2870277B1 patent drawingFigure 2
  • EP2870277B1 patent drawingFigure 3

AI summary

A process of producing metal that includes adding a quantity of a alkoxide (M(OR)x) or another metal salt to a cathode compartment of an electrolytic cell and electrolyzing the cell. This electrolyzing causes a quantity of alkali metal ions to migrate into the cathode compartment and react with the metal alkoxide, thereby producing metal and an alkali metal alkoxide. In some embodiments, the alkali metal is sodium such that the sodium ions will pass through a sodium ion selective membrane, such as a NaSICON membrane, into the cathode compartment.