Metal-Doped Silicon Oxide Anode Material for Expansion Damage Control

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Solution Overview

Problem

Silicon-based negative electrode active materials in lithium secondary batteries face issues with volume expansion and damage during charge/discharge cycles, leading to reduced lifespan and capacity performance.

Innovation Solution

A negative electrode active material is developed using silicon-based oxide particles with a metal distributed on their surface or inside, featuring a compressive fracture strength of 170 MPa to 380 MPa and Si crystal grains of 3 nm to 20 nm, which are heat-treated with a metal-containing material to enhance structural stability and prevent damage.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If silicon-based negative electrode active material is used to achieve high capacity and high energy density, then capacity and energy density are improved, but volume expansion and particle damage occur during charge/discharge cycles

Engineering Contradiction:
ImprovecapacityVSAvoidparticle integrity
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent uses a composite structure consisting of silicon-based oxide particles embedded in a porous carbon matrix. The carbon matrix provides structural support and prevents particle damage during volume expansion, while the silicon-based oxide particles provide high capacity. This composite approach resolves the contradiction by combining materials with complementary properties.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent employs porous carbon material as the matrix structure. The porous structure accommodates volume expansion of silicon-based oxide particles during lithiation, preventing particle cracking and maintaining structural integrity. The pores act as buffer spaces that absorb expansion stress, thereby preserving particle integrity while maintaining high capacity.

Inventive Principle:
Principle #31Porous materials

2Quantity of substance

If silicon-based negative electrode active material is used to achieve high capacity, then energy density is improved, but lifespan properties deteriorate due to volume expansion and particle damage

Engineering Contradiction:
ImprovecapacityVSAvoidlifespan
Core Design Contradiction:
Quantity of substanceVSDuration of action of stationary object

Solution Approach 1:

The composite structure of silicon-based oxide particles in a porous carbon matrix provides both high capacity and long lifespan. The carbon matrix protects silicon particles from degradation during cycling, while the porous structure accommodates volume changes. This combination maintains structural integrity over many cycles, resolving the contradiction between capacity and lifespan.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent applies different material properties to different regions: silicon-based oxide particles provide high capacity in specific locations, while the surrounding porous carbon matrix provides structural stability and protection. This local differentiation allows the system to achieve both high capacity and long lifespan by optimizing each region for its specific function.

Inventive Principle:
Principle #3Local quality

3Quantity of substance

If conventional silicon-based active material is used, then high capacity is achieved, but cracks and damage to active material particles occur during charge/discharge

Engineering Contradiction:
ImprovecapacityVSAvoidparticle strength
Core Design Contradiction:
Quantity of substanceVSStrength

Solution Approach 1:

The patent creates a composite where porous carbon matrix surrounds and supports silicon-based oxide particles. The carbon matrix provides mechanical strength and prevents particle cracking, while silicon-based oxide particles maintain high capacity. This composite structure resolves the contradiction between capacity and particle strength.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The porous carbon matrix acts as a flexible protective shell around silicon-based oxide particles. This shell can accommodate volume expansion and contraction during charge/discharge cycles without breaking, thereby protecting the internal particles from mechanical damage while maintaining their high capacity.

Inventive Principle:
Principle #30Flexible shells and thin films

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution effectively prevents active material damage and improves lifespan performance by controlling volume expansion and maintaining high capacity properties, resulting in enhanced battery performance.

Implementation Method 1

heat-treated with a metal-containing material to enhance structural stability and prevent damage

Methodology Applied
Scientific EffectHeat treatment: Heat Treatment

Data Source

PatentUS12107265B2Negative electrode active material, preparation method thereof, and negative electrode and secondary battery including same
Publication Date: 2024.10.01 LG ENERGY SOLUTION LTD

AI summary

The present invention relates to a negative electrode active material including silicon-based oxide particles and a metal distributed on a surface, inside, or on the surface of and the inside the silicon-based oxide particles, wherein compressive fracture strength measured at a pressure of 100 mN is 170 MPa to 380 MPa, and the silicon-based oxide particles contain Si crystal grains having a crystal grain size of 3 nm to 20 nm.