Dry Development of Metal-Containing Resist With Fluoride-Chloride Sequencing

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Solution Overview

Problem

Existing methods struggle to appropriately develop metal-containing resists, particularly in semiconductor manufacturing, where selective removal of exposed and unexposed regions is challenging.

Innovation Solution

A dry development method involving the sequential supply of a fluorine-containing gas to form a metal fluoride layer on unexposed regions, followed by a chlorine-containing gas to remove this layer, ensuring selective removal of unexposed regions while preserving exposed regions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Device complexity

If a single processing gas is used for development, then the process is simple, but the selectivity between exposed and unexposed regions is insufficient

Engineering Contradiction:
Improveprocess complexityVSAvoiddevelopment selectivity
Core Design Contradiction:
Device complexityVSManufacturing precision

Solution Approach 1:

The development process is segmented into two distinct sequential steps: first supplying a fluorine-containing processing gas to react with unexposed metal-containing resist, then supplying a chlorine-containing processing gas to remove the formed metal fluoride layer. This segmentation enables selective removal of unexposed regions while preserving exposed regions, achieving high development selectivity.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

A metal fluoride layer is formed as an intermediary substance during the development process. The fluorine-containing gas first reacts with the metal-containing resist to form this intermediate layer, which is then selectively removed by the chlorine-containing gas. This intermediary mechanism enables controlled selective removal.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Ease of operation

If conventional development methods are used, then the process is straightforward, but damage to the substrate occurs

Engineering Contradiction:
Improveprocess simplicityVSAvoidsubstrate damage
Core Design Contradiction:
Ease of operationVSObject-affected harmful factors

Solution Approach 1:

The invention changes the chemical parameters of the processing gases used in development. By using fluorine-containing gas followed by chlorine-containing gas, the process achieves selective removal with reduced substrate damage compared to conventional single-gas methods, while maintaining operational simplicity through sequential gas supply.

Inventive Principle:
Principle #35Parameter changes

3Productivity

If aggressive removal methods are used, then unexposed regions are removed effectively, but in-plane uniformity of the developed pattern deteriorates

Engineering Contradiction:
Improveremoval efficiencyVSAvoidin-plane uniformity
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The removal process is segmented into two chemical stages: fluorine reaction to form metal fluoride, then chlorine reaction to remove it. This segmentation enables effective removal of unexposed regions while maintaining in-plane uniformity of the developed pattern through controlled sequential processing.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method enables effective and selective development of metal-containing resists, achieving high selectivity and uniformity in the removal process, reducing damage to the substrate, and maintaining high in-plane uniformity of the developed pattern.

Implementation Method 1

supplying a first processing gas including a fluorine-containing gas into the chamber to form a metal fluoride layer on a surface of the second region

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 2

supplying a second processing gas including a chlorine-containing gas into the chamber to remove the metal fluoride layer

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Data Source

PatentEP4617778A1Dry developing method and dry developing device
Publication Date: 2025.09.17 TOKYO ELECTRON LTD
  • EP4617778A1 patent drawingFigure 1
  • EP4617778A1 patent drawingFigure 2
  • EP4617778A1 patent drawingFigure 3

AI summary

A dry development method includes (a) providing a substrate on a substrate support in a chamber, substrate including an underlying film and a metal-containing resist on the underlying film, the metal-containing resist including an exposed first region and an unexposed second region, (b) supplying a first processing gas including a fluorine-containing gas into the chamber to form a metal fluoride layer on a surface of the second region, and (c) supplying a second processing gas including a chlorine-containing gas into the chamber to remove the metal fluoride layer.