Metallic Particle Preforms for Faster, Uniform Brazed Sintering

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Solution Overview

Problem

Current sintering processes for electronic components face challenges with high viscosity braze pastes and suspensions, leading to uneven application, decanting issues, and suboptimal adherence due to agglomeration and oxidation of metallic particles during desolvation on the substrate, which prolongs the process and increases the risk of loss of consistency.

Innovation Solution

A pretreatment process involving desolvation and compaction of metallic particle suspensions or pastes to create a preform with controlled shape, thickness, and density, using filtration, vacuum desolvation, and compacting techniques to produce a preform of metallic particles for improved sintering on substrates.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If desolvation is performed on the substrate after paste application, then the sintering process can proceed, but the process time increases and adherence becomes suboptimal due to agglomeration

Engineering Contradiction:
Improveadherence qualityVSAvoidprocess cycle time
Core Design Contradiction:
ReliabilityVSLoss of time

Solution Approach 1:

The patent applies preliminary action by performing desolvation and compacting operations on the paste before it is applied to the substrate. The paste is desolvated to remove solvents and binders, then compacted into a preform with controlled density and shape. This preformed state is then applied to the substrate, eliminating the need for post-application desolvation and preventing agglomeration during the process.

Inventive Principle:
Principle #10Preliminary action

2Stability of the object's composition

If high viscosity paste is used for brazing, then metallic particles are well-bound, but application becomes difficult and decanting problems occur

Engineering Contradiction:
Improvepaste consistencyVSAvoidapplication ease
Core Design Contradiction:
Stability of the object's compositionVSEase of operation

Solution Approach 1:

The patent segments the brazing process into distinct stages: paste preparation with controlled viscosity for easy application, desolvation to remove solvents and binders, compacting to achieve desired density, and final sintering. This segmentation allows each stage to be optimized independently - the paste can be formulated for easy application, then transformed into a compact preform that maintains stability without requiring high viscosity throughout the entire process.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent applies parameter changes by systematically modifying the physical and chemical properties of the paste through controlled desolvation and compacting. The solvent content is reduced, binder content is adjusted, and density is increased through compaction. These parameter transformations convert the paste from a high-viscosity, hard-to-apply state to a stable, compact preform that is easy to handle and apply to the substrate.

Inventive Principle:
Principle #35Parameter changes

3Ease of operation

If suspension is used instead of paste, then application is easier, but decanting problems and nozzle blocking occur

Engineering Contradiction:
Improveapplication easeVSAvoidprocess reliability
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The patent applies preliminary action by converting the suspension into a compacted preform before application. The suspension undergoes desolvation to remove excess liquid, followed by compacting to achieve controlled density and eliminate the fluid characteristics that cause decanting and nozzle blocking. The resulting solid preform maintains the ease of placement associated with suspensions while eliminating their reliability problems.

Inventive Principle:
Principle #10Preliminary action

4Device complexity

If paste is applied directly to substrate, then process is simple, but adherence is suboptimal due to agglomeration during desolvation

Engineering Contradiction:
Improveprocess complexityVSAvoidadherence quality
Core Design Contradiction:
Device complexityVSReliability

Solution Approach 1:

The patent applies preliminary action by performing desolvation and compacting operations before substrate application. The paste is desolvated to remove solvents and binders, then compacted into a dense preform with controlled porosity. This preformed state ensures uniform particle distribution and prevents agglomeration when applied to the substrate, significantly improving adherence quality.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent employs pneumatic techniques during the compacting stage to achieve controlled density and uniform particle distribution in the preform. Gas pressure or vacuum techniques are used to compact the desolvated paste material, ensuring consistent density and eliminating voids that would lead to agglomeration and poor adherence during subsequent sintering.

Inventive Principle:
Principle #29Pneumatics and hydraulics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method reduces cycle times, ensures precise control over brazing height and alignment, and produces preforms with high mechanical strength and minimal non-metallic compounds, enhancing the efficiency and reliability of the sintering process.

Implementation Method 1

the suspension of metallic or metallic oxalate grains is subjected to a prior filtration step to filter it through a membrane filter arranged over a suction device

Methodology Applied
Scientific EffectFiltration: Filter (physical)

Implementation Method 2

the desolvation step may be performed in a vacuum and at a temperature of between 60° C. and 100° C.

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 3

the desolvation step may be performed in a vacuum

Methodology Applied
Scientific EffectVacuum: Vacuum

Implementation Method 4

a compacting step of the desolvated brazing composition such as to obtain a preform of metallic particles or metallic oxalate

Methodology Applied
Scientific EffectCompression: Compression

Data Source

PatentUS12048971B2Manufacturing process and device for preforms intended for brazing electronic, photonic, thermal or mechanical components
Publication Date: 2024.07.30 ISP SYST SRL
  • US12048971B2 patent drawing
  • US12048971B2 patent drawing
  • US12048971B2 patent drawing

AI summary

The invention relates to a pretreatment process for a brazing composition that comprises metallic particles with a granulometry in the order of the micrometer or nanometer, one or several binders and one or several solvents, said process comprising:a desolvation step of the brazing composition, so as to obtain a desolvated brazing composition,then a compacting step of the desolvated brazing composition so as to obtain a preform of metallic particles, said preform being able to be used for the sintering of an electronic, photonic, thermal or mechanical component onto a substrate,the brazing composition being represented either by a brazing paste, or by a suspension of metallic or metallic oxalate grains in suspension in a solvent.