Methanation Reactor Flushing Device for Remote Area Purging

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Solution Overview

Problem

Existing reactors for catalytic methanation of gas mixtures containing carbon dioxide and hydrogen face challenges in effectively removing residual gas filling and impurities from remote spatial areas, leading to catalyst deactivation and inefficient flushing processes.

Innovation Solution

The reactor design includes an improved flushing arrangement that allows the scavenging gas to access and exchange gas in remote spatial areas through dedicated paths and access points, ensuring effective displacement of gas mixtures and reducing the amount of scavenging gas required, thereby enhancing the cleaning of the reactor vessel and reducing flushing time.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If the reactor is purged using conventional flushing arrangements, then the main flow path is cleaned, but remote spatial areas are not effectively flushed, leading to residual impurities and catalyst deactivation

Engineering Contradiction:
Improvecatalyst activityVSAvoidflushing effectiveness
Core Design Contradiction:
ReliabilityVSEase of operation

Solution Approach 1:

The purging system is segmented into multiple independent flushing paths, with each path equipped with its own control valve. This allows selective purging of specific remote spatial areas (first, second, and third remote areas) through dedicated access points, ensuring complete removal of residual gas mixtures from all reactor regions including those inaccessible to conventional single-path flushing arrangements

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Multiple control valves act as intermediaries to regulate and direct the purge gas flow to different remote spatial areas. Each control valve selectively opens access points to specific remote areas, enabling precise control over which regions are purged at any given time, thereby achieving complete flushing without requiring simultaneous opening of all access points

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If multiple control valves and access points are added to flush remote areas, then purging effectiveness is improved, but device complexity increases

Engineering Contradiction:
Improvepurging completenessVSAvoidnumber of control valves and access points
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The reactor vessel is segmented into distinct zones (main flow path and multiple remote spatial areas), each with its own access point and control valve. This segmentation allows independent control of purging operations in different regions, enabling complete purging through a systematic sequence rather than requiring complex simultaneous multi-point injection systems

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The purging system employs dynamic control through sequential operation of control valves. The control valves are operated in a predetermined sequence to progressively open access points to different remote areas, allowing the purge gas to dynamically traverse through all regions of the reactor. This sequential dynamic control achieves complete purging while keeping the number of simultaneously active components minimal

Inventive Principle:
Principle #15Dynamics

3Device complexity

If purge gas is directed only through the main flow path, then the structure remains simple, but remote areas accumulate impurities and byproducts

Engineering Contradiction:
Improveflushing arrangement structureVSAvoidimpurity accumulation
Core Design Contradiction:
Device complexityVSObject-generated harmful factors

Solution Approach 1:

The purging system applies local quality by providing targeted flushing to specific remote spatial areas through dedicated access points and control valves. Each remote area receives purified purge gas directly at its location, ensuring that impurities and byproducts are removed from each specific zone rather than relying on passive diffusion from the main flow path

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

Control valves serve as intermediaries that direct purge gas to specific remote spatial areas where impurities accumulate. By positioning control valves at strategic locations and opening them in sequence, the system mediates the delivery of clean purge gas to remote zones, preventing impurity accumulation without requiring a complete redesign of the reactor structure

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This design allows for complete flushing of remote areas, reducing the risk of catalyst deactivation and improving the production efficiency of the methanated gas mixture by minimizing residual impurities and by-products, while also reducing the required amount and time for flushing.

Implementation Method 1

A purging arrangement (10) for purging the reactor (1) with a purging gas is provided. An access point (50, 52, 56) for introducing and/or discharging the purging gas is provided in each remote area (30, 32, 34)

Methodology Applied
Scientific EffectGas flow displacement: Advection

Implementation Method 2

a catalyst (catalyst bed) arranged therein in a main flow path extending from a reactor inlet for the gas mixture to a reactor outlet for the methanized gas mixture

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentEP2794084B1Methanation reactor having a flushing device
Publication Date: 2019.02.20 HITACHI ZOSEN INOVA ETOGAS GMBH
  • EP2794084B1 patent drawingFigure 1

AI summary

The invention relates to a reactor for catalytic methanation of a gas mixture containing carbon dioxide and hydrogen by means of a reactor vessel. A catalyst that catalyses the methanation reaction is arranged in a main flow path extending from the reactor inlet for introducing the gas mixture to a reactor outlet for discharging the methanated gas mixture. The reactor vessel further comprises at least one spatial region that is located remotely from the main flow path but is open for the gas mixture on an inflow side toward the main flow path. The reactor can be flushed with a flushing gas by means of a flushing arrangement. The flushing arrangement has an access for guiding the flushing gas into the remotely located spatial region and/or out of the remotely located spatial region on a side that does not coincide with the inflow side. The invention further relates to a method for operating the reactor according to the invention.