Methanol Synthesis CO2 Recycling for Quantitative Carbon Utilization

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Solution Overview

Problem

Existing methanol production processes using synthesis gas result in significant carbon dioxide emissions and inefficient utilization of carbon dioxide and hydrogen, leading to unconverted gases and by-products that are not fully reused for further methanol synthesis.

Innovation Solution

A process that converts carbon dioxide and hydrogen into methanol using a low-pressure methanol synthesis unit, followed by a series of steps including expansion, distillation, and combustion to recycle carbon dioxide and hydrogen-containing streams, utilizing an oxygen-rich gas for combustion to minimize emissions and maximize methanol production.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If carbon dioxide and hydrogen are converted to methanol using low-pressure synthesis, then methanol production efficiency is improved, but unconverted gases and by-products are not fully reused leading to material loss

Engineering Contradiction:
Improvemethanol production efficiencyVSAvoidunconverted gases and by-products
Core Design Contradiction:
ProductivityVSLoss of substance

Solution Approach 1:

The patent recovers unconverted hydrogen and carbon dioxide from the synthesis off-gas through pressure swing adsorption and combustion units, converting them back to usable forms for continued methanol synthesis, thereby eliminating material loss while maintaining high production efficiency

Inventive Principle:
Principle #34Discarding and recovering

Solution Approach 2:

The process implements a feedback loop where off-gas components are continuously analyzed and fed back into the synthesis system after treatment, ensuring optimal utilization of reactants and maintaining steady-state efficiency without material waste

Inventive Principle:
Principle #23Feedback

2Quantity of substance

If synthesis gas is produced from natural gas or coal gasification, then methanol synthesis feedstock is obtained, but significant carbon dioxide emissions occur

Engineering Contradiction:
Improvesynthesis gas productionVSAvoidcarbon dioxide emissions
Core Design Contradiction:
Quantity of substanceVSObject-generated harmful factors

Solution Approach 1:

The patent converts the harmful carbon dioxide emissions from synthesis gas production into a beneficial resource by capturing and recycling CO2 back into the methanol synthesis process, transforming an environmental liability into a valuable feedstock component

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The combustion unit uses controlled oxidation with oxygen-rich gas to efficiently convert unconverted carbon monoxide and hydrogen into carbon dioxide, which is then recovered and reused, creating a closed-loop system that eliminates emissions while maintaining synthesis gas production

Inventive Principle:
Principle #38Strong oxidants (Accelerated oxidation)

3Loss of energy

If off-gas streams are sent to thermal utilization, then energy recovery is achieved, but carbon dioxide emissions increase

Engineering Contradiction:
Improveenergy recovery from off-gasVSAvoidcarbon dioxide emission
Core Design Contradiction:
Loss of energyVSObject-generated harmful factors

Solution Approach 1:

The patent introduces a carbon dioxide recovery unit as an intermediary between the combustion process and the environment, capturing CO2 before it is emitted and redirecting it back to the synthesis process, thereby decoupling energy recovery from harmful emissions

Inventive Principle:
Principle #24Intermediary (Mediator)

4Loss of substance

If hydrogen is recovered through pressure swing adsorption, then unconverted hydrogen is reused, but the gas stream not absorbed requires thermal utilization

Engineering Contradiction:
Improvehydrogen recoveryVSAvoidthermal utilization emissions
Core Design Contradiction:
Loss of substanceVSObject-generated harmful factors

Solution Approach 1:

The patent makes the combustion unit multi-functional by using it both to generate thermal energy and to produce carbon dioxide for the synthesis process, eliminating the need for separate thermal utilization and associated emissions while maximizing hydrogen recovery efficiency

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process achieves nearly complete conversion of carbon dioxide to methanol while minimizing carbon dioxide emissions, effectively reusing unconverted gases and by-products within existing methanol synthesis infrastructure.

Implementation Method 1

synthesis gas is converted under heterogeneous catalysis to methanol in a methanol synthesis reactor

Methodology Applied
Scientific EffectHeterogeneous catalysis: Catalysis

Implementation Method 2

a methanol- and water-enriched crude methanol stream (II) is first condensed out of the reaction mixture

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 3

feeding the carbon compounds in the streams separated off in the synthesis and isolation of the methanol, are converted to carbon dioxide

Methodology Applied
Scientific EffectCombustion: Combustion

Implementation Method 4

The further methanol-enriched liquid stream that remains after the outgassing is then subjected to a multistage distillation for the actual methanol recovery

Methodology Applied
Scientific EffectDistillation: Distillation

Data Source

PatentEP4093723B1Process for preparing methanol from carbon dioxide and hydrogen with quantitative carbon dioxide utilization
Publication Date: 2026.04.08 BASF SE
  • EP4093723B1 patent drawingFigure 1
  • EP4093723B1 patent drawingFigure 2
  • EP4093723B1 patent drawingFigure 3

AI summary

A process for preparing methanol from carbon dioxide and hydrogen in a methanol synthesis unit and working up the reaction mixture obtained stepwise to isolate the methanol, wherein the carbon dioxide, carbon monoxide, dimethyl ether and methane components of value from the streams separated off in the isolation of the methanol from the methanol reaction stream are combusted with an oxygenous gas, and the carbon dioxide in the resultant flue gas is separated off in a carbon dioxide recovery unit and recycled to the methanol synthesis unit.