Portable Micro-Preconcentrator Manifold for Low-Concentration Air Sampling

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Solution Overview

Problem

Current chemical-analysis systems face challenges in effectively detecting vapor-phase chemical compounds due to their diffuse concentrations, particularly in portable settings where smaller IMS and GC systems are deployed for applications like chemical weapon detection and human-breath analysis, requiring a preconcentrator to enhance detection performance.

Innovation Solution

A preconcentrator system designed for air samples, incorporating multiple preconcentrators with a delivery structure that routes sample airflow concurrently or individually, integrated into unmanned aerial systems, and featuring sorbent materials and heaters for efficient compound trapping and release, along with GPS data integration and microfabrication techniques for miniaturization.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If a preconcentrator is installed to enhance detection performance by trapping and concentrating analytes, then measurement precision is improved, but device complexity increases

Engineering Contradiction:
Improvedetection performanceVSAvoidsystem complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The micro-preconcentrator is integrated within the portable chemical-analysis system, with the preconcentrator housing containing sorbent material and heating elements nested within the overall device structure. This nesting approach allows the preconcentrator to be embedded in the portable system without significantly increasing external dimensions, resolving the contradiction between enhanced detection performance and device complexity

Inventive Principle:
Principle #7Nested doll (Nesting)

Solution Approach 2:

The preconcentrator utilizes sorbent material with porous structure to trap and concentrate analytes from air samples. The porous material provides high surface area for analyte adsorption, enabling effective preconcentration in a compact form factor, thus improving measurement precision without proportionally increasing device complexity

Inventive Principle:
Principle #31Porous materials

2Measurement precision

If multiple preconcentrators are used to sample at multiple locations, then measurement precision is improved, but device complexity increases

Engineering Contradiction:
Improvesampling capabilityVSAvoidsystem complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The system is divided into multiple discrete preconcentrator units, each capable of independent sampling at different locations. Each preconcentrator is a separate module that can be individually deployed, allowing parallel sampling at multiple sites while maintaining manageable system complexity through modular architecture

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Each preconcentrator module is designed with universal functionality to perform the same sampling and preconcentration operations. This multi-functionality allows any preconcentrator in the set to be used interchangeably, simplifying the overall system design while enabling multi-location sampling capability

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Ease of operation

If portable chemical-analysis systems are deployed in the field, then ease of operation is improved, but measurement precision deteriorates due to diffuse concentrations

Engineering Contradiction:
ImproveportabilityVSAvoiddetection accuracy
Core Design Contradiction:
Ease of operationVSMeasurement precision

Solution Approach 1:

The preconcentrator performs preliminary concentration of analytes from air samples before the actual chemical analysis. By pre-concentrating the sample in the portable field device, the system overcomes the diffuse concentration problem while maintaining portability, thus improving measurement precision without sacrificing ease of operation

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The preconcentrator acts as an intermediary component between the air sample intake and the chemical analysis instrument. It mediates the transition from diffuse air samples to concentrated analyte samples, enabling portable field deployment while maintaining detection accuracy through the intermediate concentration step

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The preconcentrator system significantly enhances the detection performance of chemical compounds, enabling efficient sampling and analysis in portable settings, such as unmanned aerial systems and agricultural applications, while reducing power consumption and increasing selectivity and specificity of analyte capture.

Implementation Method 1

trapping and concentrating analytes

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

trigger a release of absorbed compounds from the sorbent material

Methodology Applied
Scientific EffectDesorption: Desorption

Data Source

PatentUS11491436B2Portable micro-preconcentrator to facilitate chemical sampling and subsequent analysis
Publication Date: 2022.11.08 RGT UNIV OF CALIFORNIA
  • US11491436B2 patent drawing
  • US11491436B2 patent drawing
  • US11491436B2 patent drawing

AI summary

The disclosed embodiments relate to the design of a preconcentrator system for preconcentrating air samples. This preconcentrator system includes a plurality of preconcentrators that preconcentrate the air samples prior to chemical analysis, and a delivery structure comprising a manifold that selectively routes a sample airflow to the plurality of concentrators so that the plurality of preconcentrators receive a sample airflow concurrently or individually.