Micro-reactor Channel Plugging Prevention via Ultrasonic Coupling

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Solution Overview

Problem

In micro-reactor continuous-reaction technology, plugging of channels due to by-products is a significant issue, especially at confluence and mixing areas, leading to increased pressure and reduced yield, which is costly to prevent using dry feeds and drying procedures, as they are expensive and sometimes dangerous.

Innovation Solution

The method involves generating ultrasonic waves within the channel-system using a process fluid to prevent or remove plugging by guiding the waves through plugging-susceptible areas, using piezo-electric transducers to couple the energy into the fluid flow, allowing for higher water content and reducing the risk of standing wave formation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If dry feeds are used to prevent plugging, then plugging is avoided, but cost increases and safety risks arise due to expensive and sometimes dangerous drying procedures

Engineering Contradiction:
Improveplugging preventionVSAvoidcost and safety of drying procedures
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The invention extracts and removes the harmful by-products (precipitates) from the reaction mixture using a separating agent that forms a second phase. This allows the use of non-dry feeds without plugging, as the by-products are continuously removed rather than prevented by drying the feeds beforehand

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

A separating agent is introduced as an intermediary substance that mediates between the reaction mixture and the by-products. This agent forms a second phase that selectively solubilizes or suspends the precipitates, allowing them to be separated and removed without requiring expensive drying procedures

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If drying procedures are applied to prevent plugging, then channel plugging is avoided, but operational complexity and cost increase significantly

Engineering Contradiction:
Improvechannel plugging preventionVSAvoiddrying procedure complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The harmful by-products are extracted from the reaction mixture by introducing a separating agent that creates a second phase. This continuous extraction process prevents plugging without requiring complex drying equipment or procedures

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention uses fluid dynamics and phase separation principles to remove by-products. The separating agent creates a second liquid phase that carries away precipitates through the reaction channel, using hydraulic principles rather than mechanical drying equipment

Inventive Principle:
Principle #29Pneumatics and hydraulics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively prevents plugging without the need for dry feeds or hazardous drying processes, maintaining reactor efficiency and safety while allowing for higher water content, up to 500 ppm, thereby reducing operational costs and ensuring continuous reactor operation.

Implementation Method 1

generating at least one ultrasonic wave travelling through the channel-system by coupling in a flow direction of at least one process fluid of a plurality of process fluids the at least one ultrasonic wave into the at least one process fluid

Methodology Applied
Scientific EffectUltrasonic wave: Ultrasound

Implementation Method 2

using piezo-electric transducers to couple the energy into the fluid flow

Methodology Applied
Scientific EffectPiezo-electric effect: Piezoelectric Effect

Data Source

PatentUS10058840B2Method for preventing plugging of a continuous-reaction channel-system and micro-reactor for carrying out the method
Publication Date: 2018.08.28 LONZA AG
  • US10058840B2 patent drawing
  • US10058840B2 patent drawing

AI summary

A method for preventing plugging of a continuous-reaction channel-system caused by a by-product of a continuous-reaction being carried out in said channel-system comprises the step of generating at least one ultrasonic wave travelling through said channel-system by coupling in a flow direction of at least one process fluid of a plurality of process fluids said at least one ultrasonic wave into said at least one process fluid.