Spray-Freeze Drying of Microalgae for Low-Energy Nutrient Retention

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Solution Overview

Problem

Existing microalgae drying technologies face challenges such as high energy consumption, nutrient loss, and scalability issues, particularly in large-scale production, with a lack of efficient and cost-effective methods for maintaining viability and nutritional value.

Innovation Solution

A spray-freeze drying apparatus and method involving a main chamber with a cold surface particle collector, a drying chamber with electromagnetic radiation and vacuum pump, and a collection chamber, which freeze, dry, and collect microalgae efficiently, ensuring precise control over particle size and distribution.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of energy

If conventional drying methods are used for microalgae, then processing is simpler, but energy consumption is high and nutrient loss occurs

Engineering Contradiction:
Improveenergy consumptionVSAvoidprocess complexity
Core Design Contradiction:
Loss of energyVSDevice complexity

Solution Approach 1:

The invention utilizes phase transition of water from liquid to solid (freezing) and then from solid to gas (sublimation) to remove moisture from microalgae. The microalgae slurry is sprayed as droplets that freeze on contact with cold surfaces, and the frozen droplets undergo sublimation in a vacuum chamber, eliminating the need for high-temperature drying while preserving nutrients and reducing energy consumption.

Inventive Principle:
Principle #36Phase transitions

Solution Approach 2:

The invention employs a vacuum environment (inert atmosphere with removed oxygen and moisture) during the drying process to prevent oxidation of nutrients and biochemical compounds in microalgae. The vacuum chamber creates an oxygen-free environment that protects sensitive nutrients while enabling sublimation drying at lower temperatures.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

2Loss of substance

If spray-freeze drying is implemented, then nutrient retention is improved, but device complexity increases

Engineering Contradiction:
Improvenutrient lossVSAvoidapparatus complexity
Core Design Contradiction:
Loss of substanceVSDevice complexity

Solution Approach 1:

The invention divides the drying process into distinct sequential stages: (1) spraying microalgae slurry as fine droplets, (2) freezing droplets on cold surfaces, (3) transferring frozen droplets to vacuum chamber, and (4) sublimation drying. This segmentation allows each stage to be optimized independently, maintaining nutrient retention while managing system complexity through modular design.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention introduces an intermediary vacuum chamber between the freezing stage and the final product collection. This vacuum chamber serves as a mediator that enables sublimation drying without direct thermal contact, protecting nutrients from degradation while facilitating moisture removal. The vacuum environment acts as an intermediary medium that preserves biochemical integrity.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Productivity

If traditional drying methods are used, then equipment requirements are simpler, but scalability to large-scale production is limited

Engineering Contradiction:
ImprovescalabilityVSAvoidequipment complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The invention implements continuous operation where microalgae slurry is continuously sprayed, frozen, and dried in sequence. The spray nozzle continuously generates droplets, cold surfaces continuously freeze them, and the vacuum chamber continuously processes frozen droplets through sublimation. This continuous workflow enables large-scale production while maintaining the benefits of spray-freeze drying, overcoming the scalability limitations of batch processing methods.

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The apparatus achieves reduced energy consumption, maintains microalgae viability and nutritional value, and enables scalable production of dried microalgae with controlled particle size and distribution.

Implementation Method 1

These droplets are rapidly frozen using a cryogen, typically liquid nitrogen. This step solidifies the droplets, preserving the integrity of sensitive components and preventing the formation of large ice crystals.

Methodology Applied
Scientific EffectRapid freezing: Freezing

Implementation Method 2

Subsequently, the frozen droplets undergo sublimation under low temperature and pressure conditions, resulting in the production of dry, powdered products.

Methodology Applied
Scientific EffectSublimation: Sublimation

Data Source

PatentUS20260049765A1Apparatus and Method for Spray-Freeze Drying (SFD) of Microalgae
Publication Date: 2026.02.19 GEB IMPACT TECHNOLOGY CO LTD
  • US20260049765A1 patent drawing

AI summary

Disclosed is a spray-freeze drying (SFD) apparatus for continuous drying of microalgae. The apparatus includes a main chamber connected to a collector chamber and a compressor, designed to freeze fine droplets of microalgae and collect frozen particles. A drying chamber, positioned downstream of the main chamber, is coupled with a vacuum pump and an electromagnetic radiation source to remove moisture from the frozen microalgae, resulting in dried particles. The dried microalgae are then collected in a designated collection chamber. Additionally, a method is disclosed for continuous drying of microalgae using the SFD apparatus. The method involves spraying microalgae suspension as fine droplets towards a cold surface particle collector in the main chamber, freezing and collecting the particles, transferring them to the drying chamber, and removing moisture through the activation of the electromagnetic radiation source and vacuum pump, followed by collecting the dried microalgae in the collection chamber.