Microemulsion Flowback Aid Composition for Oil Well Recovery

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Solution Overview

Problem

Conventional flowback aids for oil and gas wells often require solvents and fail to effectively enhance relative permeability and fluid recovery due to phase trapping, leading to reduced well productivity.

Innovation Solution

A novel microemulsion flowback aid composition comprising an oil-like phase with nonionic surfactants having a hydrophilic-lipophilic balance (HLB) of less than 9, a coupling agent, a water-soluble or dispersible nonionic surfactant, and additional surfactants, which forms a thermodynamically stable single-phase microemulsion in situ within the subterranean reservoir, reducing surface tension and enhancing fluid recovery without the need for solvents.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If conventional flowback aids containing solvents and surfactants are used, then some fluid recovery is achieved, but phase trapping occurs that reduces relative permeability and well productivity

Engineering Contradiction:
Improvefluid recoveryVSAvoidrelative permeability
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent changes the chemical composition parameters by using solvent-free microemulsion formulations with specific surfactant combinations (HLB values 3-16) and precise weight ratios (5:95 to 45:55 surfactant to co-surfactant). These parameter changes enable the formation of stable microemulsions that reduce interfacial tension without causing phase trapping, thereby improving both fluid recovery and maintaining relative permeability

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates composite microemulsion systems combining multiple surfactants (ionic and nonionic) with co-surfactants in specific ratios. This composite approach produces a synergistic effect where the combination of surfactants with different HLB values provides both the stability needed for fluid recovery and the permeability maintenance needed to prevent well damage

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If traditional flowback aid formulations with oils and solvents are used, then surfactant action is achieved, but unwanted deposits and emulsion formation occur in the well

Engineering Contradiction:
Improvesurfactant actionVSAvoiddeposits and emulsion formation
Core Design Contradiction:
Quantity of substanceVSObject-generated harmful factors

Solution Approach 1:

The patent extracts and eliminates solvents and conventional oils from the flowback aid formulation, replacing them with water-based microemulsion systems. This removal of harmful components prevents deposit formation and unwanted emulsions while retaining the essential surfactant functionality needed for fluid recovery

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention changes the formulation parameters by using specific surfactant concentration ranges (0.1-10% by weight) and co-surfactant ratios (45:55 to 55:45 surfactant to co-surfactant) that promote stable microemulsion formation without creating harmful deposits. The use of surfactants with specific HLB values (3-16) ensures optimal performance without side effects

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution effectively enhances fluid recovery and relative permeability, reduces well damage, and improves oil and gas production by forming stable microemulsions that solubilize nonpolar materials and prevent emulsion formation, thereby increasing flowback efficiency and reducing unwanted deposits.

Implementation Method 1

reducing surface or interfacial tension and/or increasing contact angle, and thereby allowing enhanced fluid recovery

Methodology Applied
Scientific EffectSurface tension reduction: Surface Tension

Implementation Method 2

reducing surface or interfacial tension and/or increasing contact angle

Methodology Applied
Scientific EffectContact angle increase: Wetting

Implementation Method 3

forming a thermodynamically stable single-phase microemulsion in situ within the subterranean reservoir

Methodology Applied
Scientific EffectMicroemulsion formation: Microemulsion

Implementation Method 4

solubilize nonpolar materials and prevent emulsion formation

Methodology Applied
Scientific EffectSolubilization: Solvation

Data Source

PatentUS9701888B2Microemulsion flowback aid composition and method of using same
Publication Date: 2017.07.11 CHAMPIONX LLC

AI summary

Disclosed and claimed is a microemulsion flowback aid composition and a method of enhancing recovery of oil or gas during fracturing or stimulation processes. The microemulsion flowback aid composition includes (i) an oil-like phase comprising at least one nonionic surfactant having a hydrophilic-lipophilic balance (HLB) of less than about 9; (ii) a coupling agent capable of stabilizing the microemulsion flowback aid composition; (iii) at least one water-soluble or dispersible nonionic surfactant that is different from the at least one nonionic surfactant in the oil-like phase; (iv) at least one additional surfactant selected from anionic, cationic, amphoteric, and combinations thereof; and (v) water.