Microfibrillated Cellulose Production via Enzyme Refinement

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

The manufacturing of microfibrillated cellulose from pulp is hindered by clogging issues in high-pressure fluidizers/homogenizers and high energy consumption, necessitating a process that alleviates these problems.

Innovation Solution

A method involving hemicellulose-containing pulp refinement with low-dose endoglucanase treatment followed by homogenization, using a range of refining apparatuses and enzyme concentrations to produce microfibrillated cellulose, which reduces energy consumption and prevents clogging.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If pulp is pumped through high pressure fluidizers/homogenizers to manufacture microfibrillated cellulose, then microfibrillated cellulose is produced, but clogging occurs in the fluidizers

Engineering Contradiction:
Improvemicrofibrillated cellulose productionVSAvoidclogging of fluidizer
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The pulp is refined before homogenization to reduce fibril aggregation and improve flow characteristics. This preliminary refining action prevents clogging in the subsequent high-pressure homogenizer by ensuring the pulp slurry has appropriate viscosity and fiber distribution, allowing continuous operation without blockages

Inventive Principle:
Principle #10Preliminary action

2Productivity

If conventional homogenization methods are used to produce microfibrillated cellulose, then cellulose microfibrils are obtained, but energy consumption is high

Engineering Contradiction:
Improvemicrofibrillated cellulose productionVSAvoidenergy consumption
Core Design Contradiction:
ProductivityVSUse of energy by moving object

Solution Approach 1:

A hydrophilic polymer is introduced as an intermediary substance during homogenization. This polymer acts as a mediator that facilitates the separation and fibrillation of cellulose fibers at lower energy inputs by reducing fiber-fiber adhesion and improving slurry flow, thereby achieving microfibrillation with reduced energy consumption compared to conventional methods

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method effectively produces microfibrillated cellulose with a higher specific surface area, enhancing its reactivity and applicability in various products while minimizing energy usage and clogging issues.

Implementation Method 1

treating said pulp with one or more cellulases of endoglucanase type at a relatively low enzyme dosage wherein said enzyme is used at a concentration of from 0.75 to 10 ECU/g fibres

Methodology Applied
Scientific EffectEnzyme hydrolysis: Enzyme

Data Source

PatentEP1984561B1Method for the manufacturing of microfibrillated cellulose
Publication Date: 2015.12.23 INNVENTIA
  • EP1984561B1 patent drawingFigure 1

AI summary

The present invention provides a method for treatment of chemical pulp for the manufacturing of microfibrillated cellulose comprising the following steps: a) providing a hemicellulose containing pulp, b) refining said pulp in at least one step and treating said pulp with one or more wood degrading enzymes at a relatively low enzyme dosage, and c) homogenizing said pulp thus providing s aid microfibrillated cellulose. According to a second aspect of the invention a microfibrillated cellulose obtainable by the method according to the first aspect is provided . According to a third aspect of the invention, use of said microfibrillated cellulose according to the second aspect in food products, paper products, composite materials, coatings or in rheology modifiers (e.g. drilling muds) is provided .