Microfiltration Membrane Saccharified Liquid Solid Separation

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Solution Overview

Problem

The production of sugar liquids from cellulose-containing biomass is hindered by the high cost and inefficiency of conventional solid-liquid separation methods, particularly when dealing with biomass having a lignin content of not more than 8.5%, which often results in incomplete removal of solid components and membrane clogging.

Innovation Solution

A method involving the saccharification of pretreated cellulose-containing biomass with a lignin content of not more than 8.5%, followed by direct filtration through a microfiltration membrane to form a cake on the membrane surface, which is then peeled off and collected, thereby avoiding the use of large-scale solid-liquid separation devices and reducing equipment costs.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional solid-liquid separation devices (filter press, screw press, centrifugation) are used, then separation capacity is sufficient, but equipment cost and operation cost increase significantly

Engineering Contradiction:
Improveseparation capacityVSAvoidequipment cost
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent uses a microfiltration membrane (thin film structure) to replace conventional large-scale solid-liquid separation devices. The membrane has pore sizes of 0.01-5 μm that can effectively separate solid components from saccharified liquid, achieving reliable separation capacity while dramatically reducing equipment cost and complexity.

Inventive Principle:
Principle #30Flexible shells and thin films

Solution Approach 2:

The microfiltration membrane is a porous material with specific pore sizes (0.01-5 μm) that allows liquid passage while retaining solid particles. This porous structure enables effective solid-liquid separation without requiring large-scale equipment, solving both separation capacity and equipment cost issues.

Inventive Principle:
Principle #31Porous materials

2Ease of manufacture

If conventional solid-liquid separation methods are used, then equipment is available, but solid component removal is insufficient and membrane clogging occurs

Engineering Contradiction:
Improveprocess availabilityVSAvoidsolid component removal efficiency
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The patent changes the pore size parameter of the filtration membrane to 0.01-5 μm, which is optimized for removing solid components from saccharified liquid. This parameter change enables complete solid component removal and prevents membrane clogging, improving reliability while maintaining process availability.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces conventional mechanical separation systems (filter press, screw press, centrifugation) with a membrane filtration system. This substitution achieves superior solid component removal efficiency and prevents clogging by using the membrane's porous structure to physically block particles, rather than relying on mechanical forces that may be insufficient.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Device complexity

If microfiltration membrane treatment is applied directly to saccharified liquid, then equipment cost is reduced, but membrane clogging increases

Engineering Contradiction:
Improveequipment costVSAvoidmembrane clogging
Core Design Contradiction:
Device complexityVSObject-affected harmful factors

Solution Approach 1:

The patent applies preliminary saccharification treatment to convert cellulose and hemicellulose into fermentable sugars before membrane filtration. This preliminary action reduces the complexity and viscosity of the liquid, preventing membrane clogging while enabling the use of cost-effective microfiltration membranes for solid component removal.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent optimizes the pore size parameter of the microfiltration membrane to 0.01-5 μm, which is large enough to allow efficient liquid passage but small enough to block solid components. This parameter optimization prevents membrane clogging while maintaining low equipment cost.

Inventive Principle:
Principle #35Parameter changes

4Reliability

If multiple separation stages (solid-liquid separation device + microfiltration membrane) are used, then solid component removal is improved, but operation cost increases

Engineering Contradiction:
Improvesolid component removalVSAvoidoperation cost
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent merges the saccharification and filtration processes into a single integrated system. The microfiltration membrane performs both solid component removal and acts as the final clarification step, eliminating the need for separate solid-liquid separation devices and reducing operation cost while maintaining reliable solid component removal.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables efficient separation of solid components from the saccharified liquid, reducing operational costs and preventing membrane clogging, resulting in a cost-effective production of sugar liquids without the need for large-scale equipment.

Implementation Method 1

filtering the saccharified liquid obtained in Step (a) through a microfiltration membrane to allow formation of a cake on the membrane surface

Methodology Applied
Scientific EffectFiltration: Filter (physical)

Implementation Method 2

saccharifying a pretreated product having a lignin content of not more than 8.5% obtained by pretreatment of a cellulose-containing biomass

Methodology Applied
Scientific EffectHydrolysis: Hydrolysis

Implementation Method 3

saccharification of cellulose and hemicellulose, which are polysaccharides

Methodology Applied
Scientific EffectEnzymatic reaction: Enzyme

Data Source

PatentEP3276008B1Method for producing sugar solution
Publication Date: 2023.09.13 TORAY INDUSTRIES INC
  • EP3276008B1 patent drawingFigure 1
  • EP3276008B1 patent drawing
  • EP3276008B1 patent drawing

AI summary

In solid-liquid separation of a saccharified liquid by filtration through a microfiltration membrane, the filtration performance can be increased by adjusting the lignin content in a pretreated product derived from a cellulose-containing biomass to not more than 8.5% to promote formation, on the membrane surface, of a cake in which the solid component in the saccharified liquid is concentrated. Collection of the cake formed on the membrane surface allows efficient solid-liquid separation of the saccharified liquid with the microfiltration membrane.