Microfocus X-Ray Window Structure for Sub-1 keV Transmission

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Solution Overview

Problem

Conventional x-ray sources with vacuum windows have low transmittance for low-energy x-rays (less than 1 keV), making them incompatible with applications requiring low-energy x-rays for materials characterization and imaging.

Innovation Solution

The x-ray source design includes a housing with an x-ray transmissive window that has a transmittance greater than or equal to 20% for x-rays with energies less than 1 keV, allowing low-energy x-rays to be transmitted effectively from a vacuum region to an ambient environment.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a conventional x-ray vacuum window is used to separate the vacuum region from ambient environment, then the vacuum integrity is maintained, but the transmittance for low-energy x-rays (less than 1 keV) becomes too low for practical applications

Engineering Contradiction:
Improvevacuum integrityVSAvoidx-ray transmittance
Core Design Contradiction:
ReliabilityVSUse of energy by moving object

Solution Approach 1:

The system is divided into separate vacuum and ambient regions with a specialized window structure. The window is segmented into different functional layers including a thin low-Z material layer for x-ray transmittance and a support structure for mechanical strength, allowing each segment to optimize its specific function while resolving the contradiction between vacuum integrity and x-ray transmittance.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The window material parameters are changed from conventional high-Z materials to low-Z materials (such as beryllium, aluminum, or silicon nitride) with optimized thickness. This parameter change enables high transmittance for low-energy x-rays while maintaining sufficient mechanical strength to preserve vacuum integrity, directly resolving the transmittance contradiction.

Inventive Principle:
Principle #35Parameter changes

2Strength

If the x-ray window thickness is increased to maintain mechanical strength, then structural integrity is improved, but x-ray transmittance for low-energy x-rays deteriorates

Engineering Contradiction:
Improvewindow structural integrityVSAvoidx-ray transmittance
Core Design Contradiction:
StrengthVSUse of energy by moving object

Solution Approach 1:

The window is constructed as a composite structure combining a thin low-Z material layer (for x-ray transmittance) with a support structure or frame (for mechanical strength). This composite approach allows the thin active layer to transmit low-energy x-rays effectively while the support structure provides the necessary mechanical integrity, resolving the contradiction between strength and transmittance.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The window utilizes a thin film structure of low-Z material that is sufficiently thin to transmit low-energy x-rays with high efficiency while being supported by a frame or mounting structure that provides mechanical strength. This thin film approach directly addresses the contradiction by decoupling the transmittance function from the structural support function.

Inventive Principle:
Principle #30Flexible shells and thin films

3Use of energy by moving object

If a thin window is used to improve low-energy x-ray transmittance, then x-ray flux is increased, but the window becomes fragile and difficult to manufacture

Engineering Contradiction:
Improvex-ray transmittanceVSAvoidwindow manufacturability
Core Design Contradiction:
Use of energy by moving objectVSEase of manufacture

Solution Approach 1:

The window employs a thin film structure that is mounted within a support frame or housing. This configuration allows the film to be sufficiently thin for high x-ray transmittance while the frame provides mechanical support during manufacturing, handling, and operation, making the thin window practical to manufacture and install.

Inventive Principle:
Principle #30Flexible shells and thin films

Solution Approach 2:

A support structure or frame acts as an intermediary between the thin low-Z material layer and the mounting system. This intermediary provides mechanical support and ease of handling during manufacturing and installation, while being transparent or minimally interfering with x-ray transmission, thus resolving the manufacturability contradiction.

Inventive Principle:
Principle #24Intermediary (Mediator)

4Reliability

If conventional x-ray sources are used with vacuum windows, then high vacuum can be maintained, but low-energy x-rays cannot be effectively transmitted for materials characterization applications

Engineering Contradiction:
Improvevacuum maintenanceVSAvoidapplication compatibility
Core Design Contradiction:
ReliabilityVSAdaptability or versatility

Solution Approach 1:

The window material parameters are changed to low-Z materials with optimized thickness to enable high transmittance for low-energy x-rays. This parameter change makes the vacuum system compatible with low-energy x-ray applications (such as photoelectron spectroscopy and soft x-ray imaging) while maintaining vacuum integrity, thus improving application compatibility without sacrificing vacuum reliability.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The specialized low-Z window design provides multi-functionality: it maintains vacuum integrity, transmits low-energy x-rays with high efficiency, and enables a wide range of applications including photoelectron spectroscopy, soft x-ray imaging, and materials characterization. This universal design resolves the contradiction by making the system adaptable to multiple application types while maintaining reliable vacuum operation.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This design enables the generation and transmission of high flux low-energy x-rays outside the vacuum vessel, addressing the limitations of conventional x-ray sources and enhancing their applicability in various materials analysis and imaging applications.

Implementation Method 1

an anode assembly within the at least one housing and configured to generate x-rays in response to electron bombardment by at least some of the electrons of the at least one electron beam from the electron source

Methodology Applied
Scientific EffectElectron bombardment: Electron Beam

Implementation Method 2

The at least one housing comprises an x-ray transmissive window having an x-ray transmittance greater than or equal to 20% for at least some x-rays having an x-ray energy less than 1 keV

Methodology Applied
Scientific EffectX-ray transmission: X-Ray

Data Source

PatentUS12278080B2Microfocus x-ray source for generating high flux low energy x-rays
Publication Date: 2025.04.15 SIGRAY INC
  • US12278080B2 patent drawing
  • US12278080B2 patent drawing
  • US12278080B2 patent drawing

AI summary

An x-ray source includes an x-ray transmissive window having an x-ray transmittance greater than or equal to 20% for at least some x-rays having an x-ray energy less than 1 keV. The x-ray source further includes an electron source configured to generate at least one electron beam and an anode assembly configured to generate x-rays in response to electron bombardment by at least some of the electrons of the at least one electron beam from the electron source. The x-ray source further includes at least one x-ray optic is configured to receive at least some of the x-rays from the anode assembly and to direct at least some of the received x-rays to the window to form an x-ray beam.