Microgel Particles with Nanotube Loading for API Protection

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Current drug delivery systems face challenges in protecting active pharmaceutical ingredients (APIs) from enzymatic digestion in the gastrointestinal tract and achieving controlled release, especially for large molecules and proteins, due to instability and rapid degradation in acidic and enzymatic environments.

Innovation Solution

Incorporating nanotubes loaded with APIs into microgel particles, which exhibit a synergistic interaction with the gel-forming polymer, providing enhanced protection and a tailored release profile, using the vibrating nozzle technique for preparation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If liposomes or W/O microemulsions are used to provide a hydrophilic micro-environment for APIs, then the solubility of hydrophilic APIs is improved, but colloidal instability occurs upon dilution in the gastrointestinal tract

Engineering Contradiction:
Improvesolubility of hydrophilic APIsVSAvoidcolloidal stability
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent changes the physical-chemical parameters of the delivery system by using water-in-oil microemulsions with specific composition ratios (phospholipid 1-10%, co-surfactant 1-20%, oil phase 70-95%) that remain stable upon dilution in gastrointestinal fluids, preventing phase separation while maintaining API solubility

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite delivery system combining phospholipids, co-surfactants, and oil phases in a microemulsion formulation that provides both hydrophilic micro-environments for API dissolution and colloidal stability against enzymatic degradation and phase separation

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If standard lipid-based systems are used for drug delivery, then the delivery of lipophilic APIs is improved, but they cannot target specific regions of the gut and are digested by lipophilic enzymes

Engineering Contradiction:
Improvedelivery efficiency of lipophilic APIsVSAvoidresistance to enzymatic digestion
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent modifies the lipid-based system by incorporating co-surfactants and adjusting the water-to-oil ratio to create microemulsion droplets that resist phospholipase A2 degradation while maintaining lipophilic API solubility and gut region targeting capability

Inventive Principle:
Principle #35Parameter changes

3Reliability

If gels are used to protect APIs from enzymatic digestion, then the protection period is extended, but degradation can be fast and release cannot be easily tailored

Engineering Contradiction:
Improveprotection against enzymatic digestionVSAvoidtailorability of release profile
Core Design Contradiction:
ReliabilityVSAdaptability or versatility

Solution Approach 1:

The patent creates a dynamic release system where the microemulsion composition and droplet size can be adjusted to achieve different release profiles (sustained, controlled, or rapid), allowing the same base formulation to adapt to different therapeutic requirements while maintaining enzymatic protection

Inventive Principle:
Principle #15Dynamics

4Quantity of substance

If nanotubes are used to store APIs, then the loading capacity is increased, but the release is generally fast and protection against enzymatic digestion is inadequate

Engineering Contradiction:
Improveloading capacity of APIVSAvoidprotection against enzymatic digestion
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent employs a nested structure where nanotubes containing API are embedded within water-in-oil microemulsion droplets, providing dual protection: the nanotube maintains high loading capacity while the microemulsion matrix protects against enzymatic digestion and enables controlled release

Inventive Principle:
Principle #7Nested doll (Nesting)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The microgel particles effectively protect APIs from enzymatic digestion and offer a controlled release profile, improving bioavailability and stability of both hydrophilic and hydrophobic APIs, particularly for bulky molecules and proteins, while maintaining a hydrophilic environment for their transport and action.

Implementation Method 1

The microgel particles effectively protect APIs from enzymatic digestion

Methodology Applied
Scientific EffectPhysical containment: Physical Containment

Implementation Method 2

the interaction between the gel-forming polymer of the microgel particles and the nanotubes results in a certain release of the API which can be tailored

Methodology Applied
Scientific EffectDiffusion: Diffusion

Data Source

PatentEP3280391B1Microgel particles
Publication Date: 2019.10.30 TILLOTS PHARMA AG
  • EP3280391B1 patent drawingFigure 1
  • EP3280391B1 patent drawingFigure 2
  • EP3280391B1 patent drawingFigure 3

AI summary

The present invention relates to microgel particles, a process for their preparation and a pharmaceutical composition comprising the same.