Microwave CO2 Capsule Decomposition Under Pressure

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Solution Overview

Problem

Existing methods lack a viable approach for producing carbon dioxide under pressure using thermal decomposition, particularly for beverages, as they do not utilize microwave energy effectively for this purpose.

Innovation Solution

A thermal decomposition system employing RF energy, a microwave generator, and a capsule chamber to decompose sodium bicarbonate, optimizing the sodium bicarbonate:water ratio and microwave frequency for efficient carbon dioxide production under pressure, utilizing dielectric heating and a custom-designed microwave cavity for rapid heating.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional thermal decomposition methods are used, then carbon dioxide can be produced, but the process is slow and inefficient

Engineering Contradiction:
Improvecarbon dioxide production rateVSAvoiddecomposition time
Core Design Contradiction:
ProductivityVSLoss of time

Solution Approach 1:

The patent replaces conventional electrical heating systems with microwave radiation heating. The microwave generator produces electromagnetic waves that directly heat the sodium bicarbonate and water mixture through dielectric heating, achieving rapid thermal decomposition and CO2 evolution without the slow heat transfer limitations of conventional heating methods.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent optimizes specific parameters including the sodium bicarbonate to water ratio (3:1 to 5:1), microwave frequency (2.4-2.5 GHz), and power levels (300-700 Watts) to maximize decomposition efficiency. These parameter changes enable the system to achieve over 90% decomposition within one minute, dramatically improving productivity compared to conventional methods.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If microwave energy is applied to sodium bicarbonate, then rapid decomposition occurs, but the system requires precise optimization of multiple parameters

Engineering Contradiction:
Improvedecomposition speedVSAvoidparameter optimization requirements
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent systematically optimizes key parameters including the sodium bicarbonate to water ratio (determined through thermodynamic modeling), microwave frequency (2.4-2.5 GHz range), and power levels (300-700 Watts). This parameter optimization enables rapid decomposition while providing a standardized operating protocol that reduces operational complexity.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs pressure sensors and temperature monitoring to track the decomposition process in real-time. This feedback mechanism allows the system to automatically adjust microwave power delivery and terminate heating when target CO2 pressure or temperature is reached, simplifying operation despite the multiple parameters involved.

Inventive Principle:
Principle #23Feedback

3Quantity of substance

If high pressure is generated during decomposition, then carbon dioxide production is enhanced, but the capsule and chamber must withstand significant stress

Engineering Contradiction:
Improvecarbon dioxide yieldVSAvoidpressure on capsule and chamber
Core Design Contradiction:
Quantity of substanceVSStress or pressure

Solution Approach 1:

The patent uses a flexible polymer capsule shell that can expand to accommodate the evolving CO2 gas while containing the high pressure. The capsule design includes a deformable structure that safely manages pressure buildup during rapid decomposition, preventing rupture while maximizing CO2 generation. The outer chamber provides additional containment for the pressurized environment.

Inventive Principle:
Principle #30Flexible shells and thin films

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system achieves rapid and efficient production of carbon dioxide, with over 90% decomposition of sodium bicarbonate occurring within one minute at optimal temperatures, effectively addressing the need for a method to produce CO2 under pressure for beverage carbonation.

Implementation Method 1

The microwave generator generates microwave energy applied to the capsule sufficient to cause thermal decomposition of the sodium bicarbonate to evolve carbon dioxide

Methodology Applied
Scientific EffectDielectric heating: Dielectric Heating

Implementation Method 2

application of RF energy to the thermally decomposable material in the capsule causes thermal decomposition which evolves gas

Methodology Applied
Scientific EffectThermal decomposition: Thermolysis

Data Source

PatentUS10106422B2Rapid high-pressure microwave thermal decomposition system, capsule and method for using same
Publication Date: 2018.10.23 SO SPARK
  • US10106422B2 patent drawing
  • US10106422B2 patent drawing
  • US10106422B2 patent drawing

AI summary

Carbon dioxide, such as may be used for a carbonated beverage, is produced by microwave thermal decomposition of a starting material. An apparatus for the process includes a microwave generator, a microwave chamber, a capsule received in the chamber containing starting material(s) and one or more channel(s) for recovering CO2 generated in the process.