Continuous Microwave Extraction of Essential Oils Without Solvents

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Solution Overview

Problem

Microwave-assisted extraction of essential oils from plant biomass has limited commercial development due to challenges in scaling up and maintaining consistent quality and olfactive properties at an industrial scale, often requiring harmful solvents and altering the natural scent profiles.

Innovation Solution

A continuous microwave extraction method that introduces plant biomass into a vessel where microwave energy vaporizes water to produce a distillate containing essential oils, eliminating the need for solvents and allowing for improved olfactive profiles similar to fresh plant materials by controlling parameters like conveyor belt speed, microwave intensity, and treatment time.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional extraction methods are used, then extraction efficiency is improved, but harmful solvents are required and natural scent profiles are altered

Engineering Contradiction:
Improveextraction efficiencyVSAvoidharmful solvents and altered scent profiles
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The patent extracts only the essential oils and aromatic compounds from plant biomass using microwave energy and water vapor, eliminating the need for harmful chemical solvents. The continuous extraction system separates the desired aromatic components while leaving behind the plant residue, achieving both high extraction efficiency and preservation of natural scent profiles without solvent contamination

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent replaces conventional mechanical extraction methods that require solvents with a microwave-based thermal system. Microwave energy directly heats the plant biomass and water, enabling extraction through controlled vaporization and diffusion without mechanical solvent intervention, thereby eliminating harmful chemical factors while maintaining extraction productivity

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Productivity

If microwave extraction is scaled up to industrial scale, then production capacity is improved, but consistent quality and olfactive properties become difficult to maintain

Engineering Contradiction:
Improveproduction capacityVSAvoidconsistent quality and olfactive properties
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent employs a continuous extraction system where plant biomass is continuously fed through the microwave extraction chamber, and essential oils are continuously collected. This continuous operation ensures consistent processing conditions, uniform heating patterns, and steady-state extraction efficiency, maintaining both high production capacity and consistent quality/olfactive properties across large volumes of processed material

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The patent optimizes and controls critical parameters including microwave power intensity, water-to-biomass ratio, extraction temperature, and residence time to ensure consistent extraction performance at industrial scale. By precisely controlling these parameters, the system maintains uniform olfactive properties and quality characteristics while achieving high production capacity

Inventive Principle:
Principle #35Parameter changes

3Device complexity

If batch processing is used, then extraction simplicity is maintained, but time consumption and inefficiency increase

Engineering Contradiction:
Improveextraction simplicityVSAvoidtime consumption and inefficiency
Core Design Contradiction:
Device complexityVSLoss of time

Solution Approach 1:

The patent transitions from batch to continuous processing, where plant biomass is continuously fed through the extraction system and essential oils are continuously collected. This eliminates idle time between batches, maintains constant extraction efficiency, and significantly reduces total processing time while keeping the system relatively simple through standardized continuous-flow architecture

Inventive Principle:
Principle #20Continuity of useful action

4Device complexity

If traditional extraction methods are used, then equipment simplicity is maintained, but environmental impact and CO2 footprint increase

Engineering Contradiction:
Improveequipment simplicityVSAvoidenvironmental impact and CO2 footprint
Core Design Contradiction:
Device complexityVSObject-generated harmful factors

Solution Approach 1:

The patent replaces energy-intensive conventional extraction equipment with a microwave-based system that uses electromagnetic radiation for direct heating. This substitution eliminates the need for large volumes of solvent handling, storage, and disposal equipment, reducing environmental impact and CO2 footprint while maintaining relatively simple equipment architecture through integrated microwave chambers and condensation systems

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method enables efficient, solvent-free extraction of essential oils with improved olfactive profiles, reduced waste, and a lower CO2 footprint, maintaining the natural scent characteristics of the plant biomass while scaling up production.

Implementation Method 1

subjecting the plant biomass to microwave energy to vaporize water within the biomass, thereby producing a distillate

Methodology Applied
Scientific EffectMicrowave heating: Dielectric Heating

Implementation Method 2

vaporize water within the biomass, thereby producing a distillate

Methodology Applied
Scientific EffectVaporization: Evaporation

Data Source

PatentUS20220175003A1Microwave assisted extraction of essential oils from plant biomass
Publication Date: 2022.06.09 FIRMENICH SA
  • US20220175003A1 patent drawing
  • US20220175003A1 patent drawing
  • US20220175003A1 patent drawing

AI summary

The aspects presented herein provide essential oils, extracts, apparatus and methods for the extraction of the essential oils and extracts from plant biomass using microwaves.