Microwave Flash Evaporation for Scaling and Corrosion

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Solution Overview

Problem

Current evaporation technologies in the chemical and metallurgical industries face inefficiencies due to low heat transfer rates, scaling issues, high energy consumption, and complex, costly systems, particularly in multi-effect evaporation processes which suffer from heat loss, corrosion, and reduced efficiency due to high temperatures and pressures.

Innovation Solution

The implementation of a microwave flash evaporation process that integrates liquid spraying, droplet flash evaporation, and microwave enhancement, creating a liquid droplet micro-system for efficient energy transfer, reducing the need for circulation pumps and steam heat exchange systems, and optimizing the microwave resonant cavity design for improved efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If multi-effect evaporation is used to improve evaporation efficiency, then evaporation efficiency is improved, but device complexity increases and production cost increases

Engineering Contradiction:
Improveevaporation efficiencyVSAvoidsystem complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent replaces the traditional mechanical steam heat exchange system with a microwave field system. Instead of using steam heating through heat exchangers, the invention uses microwave radiation to directly heat the liquid feed, eliminating the need for complex multi-effect evaporation apparatus with multiple pumps, heat exchangers, and steam generation systems. This substitution of mechanical/thermal energy transfer with electromagnetic energy transfer simplifies the overall system while maintaining high evaporation efficiency.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The invention changes the fundamental parameter of energy transfer from thermal conduction/convection (steam heating) to electromagnetic radiation (microwave heating). This parameter change allows single-stage evaporation to achieve the same effect as multi-effect systems, reducing device complexity while improving energy efficiency and eliminating the need for multiple evaporation chambers and associated equipment.

Inventive Principle:
Principle #35Parameter changes

2Reliability

If steam heat exchange is used for evaporation energy supply, then evaporation process is maintained, but heat loss increases and energy consumption increases

Engineering Contradiction:
Improveevaporation process stabilityVSAvoidheat loss
Core Design Contradiction:
ReliabilityVSLoss of energy

Solution Approach 1:

The patent substitutes the steam heat exchange system with direct microwave heating. Instead of transferring heat through steam condensation on heat exchanger surfaces (which suffers from heat loss and scaling), the microwave field directly couples with the liquid molecules, causing dielectric heating throughout the bulk liquid. This eliminates the heat transfer interface and associated heat losses, improving energy efficiency while maintaining process stability.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The microwave field acts as an intermediary energy carrier that directly transfers energy to the liquid feed without requiring thermal contact through heat exchangers. This intermediary electromagnetic field enables efficient energy transfer without the heat loss, scaling, and corrosion problems associated with traditional steam heat exchange systems.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Productivity

If high temperature and high pressure are applied in evaporation, then evaporation rate is improved, but corrosion increases and equipment damage increases

Engineering Contradiction:
Improveevaporation rateVSAvoidequipment durability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The invention changes the energy input method from external thermal heating (steam) to internal dielectric heating (microwave). This allows the liquid to be heated rapidly and uniformly throughout its volume, achieving high evaporation rates at lower bulk temperatures and reduced pressure requirements. The microwave energy is absorbed directly by the liquid molecules, creating internal heat generation that eliminates the need for high-temperature steam and high-pressure operation, thereby reducing corrosion and equipment damage.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The microwave field induces dielectric relaxation and molecular rotation in the liquid, creating intense molecular-level agitation and vibration. This internal molecular motion facilitates rapid heat generation and mass transfer, enabling high evaporation rates without requiring high external temperatures or pressures, thus protecting equipment from thermal stress and corrosion.

Inventive Principle:
Principle #18Mechanical vibration

4Use of energy by stationary object

If heat exchanger is used for evaporation, then heat transfer is achieved, but scaling on heat exchanger surface reduces heat exchange efficiency and increases energy consumption

Engineering Contradiction:
Improveheat transfer efficiencyVSAvoidenergy consumption
Core Design Contradiction:
Use of energy by stationary objectVSLoss of energy

Solution Approach 1:

The patent eliminates the heat exchanger component entirely by replacing the thermal conduction-based heat transfer system with a microwave radiation-based heating system. The microwave field penetrates the liquid and causes dielectric heating throughout the bulk, bypassing the need for heat exchanger surfaces. This substitution prevents scaling issues completely, as there is no solid surface for scale deposition, thereby maintaining consistent heat transfer efficiency and avoiding the energy consumption increases associated with scale buildup.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances evaporation efficiency, reduces energy consumption, and minimizes scaling and corrosion, achieving a more cost-effective and environmentally friendly process by utilizing microwave energy for rapid and selective dehydration, thereby simplifying the evaporation process and improving heat transfer.

Implementation Method 1

through the coupling effect of the microwave, by means of one stage microwave flash evaporation

Methodology Applied
Scientific EffectDielectric heating: Dielectric Heating

Implementation Method 2

makes integration of those technologies for liquid spraying, liquid droplet flash evaporation

Methodology Applied
Scientific EffectLiquid spraying: Fluid Spray

Implementation Method 3

under the condition of high vacuum degree of flash evaporation chamber and the evaporation chamber

Methodology Applied
Scientific EffectVacuum: Vacuum

Implementation Method 4

an evaporation unit is one of operation units consuming a large amount of energy. This operation unit is widely used in those fields for seawater desalination, wastewater treatment, chemicals crystallization

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentUS10632396B2Microwave flash evaporation process and apparatus and use thereof
Publication Date: 2020.04.28 KUNMING UNIV OF SCI & TECH
  • US10632396B2 patent drawing
  • US10632396B2 patent drawing
  • US10632396B2 patent drawing

AI summary

The present disclosure discloses a microwave flash evaporation process and apparatus and uses thereof. A microwave flash evaporation process, wherein the process makes integration of those technologies for liquid spraying, liquid droplet flash evaporation, microwave enhancement, vacuum steam discharge, and simulation and optimization of multi-mode resonant cavity, wherein through the coupling effect of the microwave, by means of one stage microwave flash evaporation, the effect normally achieved by multi-effect evaporation and flash evaporation is obtained and a liquid droplet micro-system with microwave energy transfer in situ is formed so as to prevent a circulation pump and a steam heat exchange system from being corroded under high temperature and high pressure, and prevent scaling on a heat exchanger, and improve evaporation efficiency. The present disclosure makes integration of those technologies for liquid spraying, liquid droplet flash evaporation, microwave enhancement, vacuum steam discharge, and simulation and optimization of multi-mode resonant cavity, and can be used for performing the processes of effluent disposal, seawater desalination, evaporation concentration of spent liquor of Bayer process, concentration crystallization of chemical production, sterilization of solution, unoil of solution, the rectification separation for various organic mixed solutions, sterilization, unoil and dehydration of solid powder. There is a prospect for this new process of the present disclosure with short technological process to upgrade the evaporation process.