Monolithic MIM Test Coupon Design for Binder Distribution

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Solution Overview

Problem

Metal injection molding (MIM) test coupons face issues with binder shearing, premature cross-linking, and warping due to flow restrictions and uneven binder distribution, leading to defects such as flash and damage during ejection and sintering.

Innovation Solution

A monolithic precursor test coupon design with grip portions, an intermediate portion, and runners that provide stability and prevent breakage or warping, along with a specialized mold and flash-removal tool for accurate material property testing.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Speed

If feedstock injection pressure is increased to overcome the restriction in the reduced central cross-sectional area, then feedstock flow through the restriction is improved, but binder is sheared away from the feedstock causing non-uniform binder distribution

Engineering Contradiction:
Improvefeedstock flow speedVSAvoidbinder distribution uniformity
Core Design Contradiction:
SpeedVSStability of the object's composition

Solution Approach 1:

The test coupon is segmented into distinct geometric zones: a reduced central cross-sectional area section and enlarged end sections. This segmentation allows the feedstock to flow through the reduced area without excessive pressure buildup that would shear the binder, while the enlarged end sections provide reservoir space for uniform binder distribution throughout the green coupon.

Inventive Principle:
Principle #1Segmentation

2Stability of the object's composition

If feedstock is pushed through the restriction too slowly, then binder distribution is maintained, but binder cross-links before injection is completed causing feedstock to solidify

Engineering Contradiction:
Improvebinder distribution uniformityVSAvoidinjection completion speed
Core Design Contradiction:
Stability of the object's compositionVSProductivity

Solution Approach 1:

The enlarged end sections are designed to act as reservoirs that pre-accommodate feedstock before it passes through the reduced central area. This preliminary action allows the injection process to maintain slower speeds for binder distribution while ensuring complete filling before binder cross-linking occurs.

Inventive Principle:
Principle #10Preliminary action

3Adaptability or versatility

If a long, narrow green part with reduced central cross-sectional area is used, then material property testing capability is improved, but the coupon may warp at elevated sintering temperatures

Engineering Contradiction:
Improvetesting capabilityVSAvoidshape stability
Core Design Contradiction:
Adaptability or versatilityVSStability of the object's composition

Solution Approach 1:

The coupon design uses asymmetric thickening at the end sections relative to the central reduced area. This asymmetric geometry creates a more stable thermal mass distribution during sintering, reducing warping while preserving the reduced central area needed for accurate material property testing.

Inventive Principle:
Principle #4Asymmetry

4Speed

If elevated injection pressures are used, then feedstock flows through the restriction, but binder flows into spaces between ejector pins and mold causing ejector pins to stick

Engineering Contradiction:
Improvefeedstock flow speedVSAvoidbinder leakage
Core Design Contradiction:
SpeedVSObject-generated harmful factors

Solution Approach 1:

The geometric parameters of the coupon are changed to include enlarged end sections that reduce the pressure gradient during injection. This parameter change allows feedstock to flow through the reduced central area at lower pressures, preventing binder from leaking into ejector pin spaces and causing sticking.

Inventive Principle:
Principle #35Parameter changes

5Ease of manufacture

If conventional manual flash removal techniques are used on a long, narrow green part, then flash can be removed, but the coupon is at risk of damage

Engineering Contradiction:
Improveflash removal capabilityVSAvoidcoupon integrity
Core Design Contradiction:
Ease of manufactureVSStrength

Solution Approach 1:

The flash is removed in advance during the molding process itself by designing the mold to accommodate and redirect excess feedstock away from the coupon body. This preliminary flash removal eliminates the need for subsequent manual removal operations that could damage the long, narrow coupon structure.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution ensures proper binder distribution and integrity, preventing defects and facilitating accurate material property testing without complex alignment procedures, while maintaining structural stability throughout the molding and sintering processes.

Implementation Method 1

When injecting feedstock through the mold during the MIM process

Methodology Applied
Scientific EffectInjection pressure: Pressure Increase

Implementation Method 2

If binder is not uniformly distributed throughout the green test coupon after the injection-molding process is completed

Methodology Applied
Scientific EffectBinder distribution: Dispersion (of waves)

Implementation Method 3

the green part is subjected to de-binding, for example in a thermal or solvent-based process, to remove the binder

Methodology Applied
Scientific EffectThermal de-binding: Heating

Implementation Method 4

The brown part is then sintered at high temperatures to form the final, substantially metallic component

Methodology Applied
Scientific EffectSintering: Sintering

Implementation Method 5

If feedstock injection pressure is increased to overcome the restriction, in some cases feedstock material is pushed through the restriction too quickly, shearing the binder away from the feedstock

Methodology Applied
Scientific EffectShear stress: Shear Stress

Data Source

PatentEP3744447B1Monolithic precursor test coupons for testing material properties of metal-injection-molded components
Publication Date: 2024.01.24 THE BOEING CO
  • EP3744447B1 patent drawingFigure 1A
  • EP3744447B1 patent drawingFigure 1B
  • EP3744447B1 patent drawingFigure 1C

AI summary

A monolithic precursor test coupon (100) comprises a first grip portion (110), a second grip portion (112), and an intermediate portion (114), interconnecting the first grip portion (110) and the second grip portion (112). The monolithic precursor test coupon (100) also comprises runners (130), directly interconnecting the first grip portion (110) and the second grip portion (112) and not directly connected to the intermediate portion (114). The first grip portion (110), the second grip portion (112), the intermediate portion (114), and the runners (130) are composed of a substance (150) that comprises metal powder (748) and that is in a green state.