Mineralogical Composition Correction Using Elemental Feedback

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Solution Overview

Problem

Current methods for determining the mineralogical composition of geological formations, such as those in oil fields, face challenges in achieving accurate and real-time results, especially when using field measurements, as they often rely on simplified sample preparation techniques like DRIFTS and XRD, which may not capture the complete mineralogical and elemental composition accurately.

Innovation Solution

A method and installation that utilize first and second detectors to measure mineralogical and elemental compositions, respectively, with a processing system applying a mineralogy break-down model to correct the mineralogical composition by adjusting mineral amounts within families or adding additional minerals, while maintaining constant total amounts, to improve accuracy and match predicted and measured elemental compositions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If simplified sample preparation techniques like DRIFTS or XRD are used for field measurements, then measurement speed and ease of operation are improved, but measurement precision and reliability of mineralogical composition determination deteriorate

Engineering Contradiction:
Improvemeasurement speedVSAvoidmineralogical composition accuracy
Core Design Contradiction:
ProductivityVSMeasurement precision

Solution Approach 1:

The system uses measured elemental composition as feedback to correct the mineralogical composition obtained from rapid field measurements. The elemental composition serves as a reference to validate and adjust the mineralogical results, ensuring accuracy while maintaining fast measurement capability.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

Elemental composition acts as an intermediary between the rapid field measurement (DRIFTS/XRD) and the accurate mineralogical composition determination. By introducing this intermediate measurement, the system bridges the gap between speed and precision without requiring complex sample preparation.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Measurement precision

If complex measurement procedures with rigorous sample preparation are used, then measurement precision is improved, but ease of operation and measurement time are worsened

Engineering Contradiction:
Improvemineralogical composition accuracyVSAvoidsample preparation complexity
Core Design Contradiction:
Measurement precisionVSEase of operation

Solution Approach 1:

The measurement process is segmented into two independent parts: rapid field measurement of mineralogical composition using DRIFTS or XRD, and separate measurement of elemental composition. This segmentation allows each measurement to be optimized independently, with the elemental composition serving as a correction reference without requiring complex sample preparation for the main field measurement.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The system changes the measurement parameters by introducing elemental composition analysis as a complementary measurement. Instead of relying solely on complex sample preparation for accurate mineralogical results, the system uses elemental composition parameters to correct and validate the mineralogical data, simplifying the overall operational process.

Inventive Principle:
Principle #35Parameter changes

3Loss of time

If field measurements with simplified preparation are used, then loss of time is reduced, but loss of information regarding complete mineralogical and elemental composition increases

Engineering Contradiction:
Improvetime to obtain resultsVSAvoidcompleteness of composition data
Core Design Contradiction:
Loss of timeVSLoss of information

Solution Approach 1:

The system merges two measurement approaches: rapid field measurement (DRIFTS or XRD) for mineralogical composition and elemental composition analysis. By combining these measurements and using the elemental data to correct the mineralogical results, the system recovers complete composition information without sacrificing the time advantage of field measurements.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The system performs preliminary measurement of mineralogical composition using rapid field techniques, then uses elemental composition analysis to correct and complete the data. This preliminary action approach allows the system to obtain initial results quickly while ensuring complete information through subsequent correction based on elemental measurements.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances the accuracy of mineralogical composition determination, particularly in near real-time field measurements, by iteratively correcting mineral amounts, leading to a more precise mineralogical composition that better matches the elemental composition, as demonstrated by significant reductions in error scores and improved correlation with reference measurements.

Implementation Method 1

XRD (X-Ray Diffraction) have been developed

Methodology Applied
Scientific EffectX-Ray Diffraction: X-Ray

Implementation Method 2

DRIFTS (Diffuse Reflectance Infrared Fourier Transform Spectroscopy)

Methodology Applied
Scientific EffectDiffuse Reflectance Infrared Fourier Transform Spectroscopy: Absorption Spectroscopy

Implementation Method 3

The elemental composition may indeed be measured accurately via known technique

Methodology Applied
Scientific EffectX-Ray Fluorescence: X-Ray

Data Source

PatentUS11340207B2Method and installation for determining an improved mineralogical composition of a rock sample
Publication Date: 2022.05.24 SCHLUMBERGER TECH CORP
  • US11340207B2 patent drawing
  • US11340207B2 patent drawing
  • US11340207B2 patent drawing

AI summary

A method for determining a mineralogical composition of a geological formation sample includes measuring a mineralogical composition of the sample and measuring an elemental composition of the sample. The mineralogical composition is processed to compute a predicted elemental composition of the sample based on known elemental compositions of predetermined minerals. The measured mineralogical composition is corrected to obtain a corrected mineralogical composition which is in turn processed to compute a corresponding corrected predicted elemental composition of the sample. The measured elemental composition is compared with the predicted elemental compositions to obtain error indicators. The error indicators are compared and evaluated to selected and output one of the measured or corrected measured mineralogical compositions.