Mixed Textile Recycling via Segmented Pulping and Supercritical CO2 Extraction

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Solution Overview

Problem

The textile industry faces challenges in efficiently recycling mixed textile feedstocks, particularly cotton and polyester blends, due to the resource-intensive and environmentally harmful processes currently used, which result in significant waste and inefficient material utilization.

Innovation Solution

A multi-stage process involving pretreatment and pulping/dissolution stages to isolate cellulose and polyester polymers from mixed textile feedstocks, allowing for the production of regenerated fibers with improved properties, utilizing techniques such as high temperature aqueous washing, supercritical CO2 treatment, and enzymatic processes to minimize environmental impact.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional recycling methods are used for mixed textile feedstock, then processing is simpler, but material separation efficiency is poor and environmental impact is high

Engineering Contradiction:
Improvematerial separation efficiencyVSAvoidprocessing complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The recycling process is divided into distinct stages: pretreatment stage (mechanical sorting, baling), pulping stage (chemical separation of cellulose and polyester), and regeneration stage (fiber production). Each stage targets specific separation objectives, enabling efficient material separation through systematic segmentation of the overall process.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Chemical intermediaries are introduced during the pulping stage to facilitate separation of cellulose and polyester components. Specific pulping agents act as mediators that selectively dissolve or separate one component from the other, enabling efficient material separation without direct mechanical conflict between different textile types.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Loss of substance

If resource-intensive processing is used, then material recovery is improved, but environmental harm increases

Engineering Contradiction:
Improvematerial recoveryVSAvoidenvironmental harm
Core Design Contradiction:
Loss of substanceVSObject-generated harmful factors

Solution Approach 1:

The process utilizes controlled changes in physical and chemical parameters during different stages. Temperature, pressure, pH levels, and chemical concentrations are adjusted to optimize both material recovery and environmental performance. For example, controlled pulping conditions maximize fiber recovery while minimizing chemical waste, and energy-efficient drying parameters reduce environmental impact.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The system implements comprehensive recovery of valuable materials including cellulose, polyester, and associated chemicals. Waste streams are minimized through efficient separation techniques, and recovered materials are reused in the process or converted to valuable products, significantly reducing environmental harm compared to conventional disposal methods.

Inventive Principle:
Principle #34Discarding and recovering

3Manufacturing precision

If multi-stage processing is implemented, then fiber quality is improved, but processing time increases

Engineering Contradiction:
Improvefiber qualityVSAvoidprocessing time
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

The process maintains continuous operation through overlapping stages where pretreatment, pulping, and regeneration occur in continuous sequences rather than discrete batches. This continuous flow eliminates idle time between stages and ensures that fiber quality is consistently maintained while minimizing total processing time through uninterrupted useful action.

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

Preliminary pretreatment stages prepare materials in advance before main processing begins. Mechanical sorting, baling, and initial size reduction are performed beforehand to optimize subsequent pulping and regeneration steps, reducing overall processing time while maintaining high fiber quality through proactive preparation.

Inventive Principle:
Principle #10Preliminary action

4Manufacturing precision

If chemical treatments are used, then material isolation is improved, but environmental impact increases

Engineering Contradiction:
Improvematerial isolationVSAvoidenvironmental impact
Core Design Contradiction:
Manufacturing precisionVSObject-generated harmful factors

Solution Approach 1:

Chemical treatments are applied with controlled parameters including concentration, temperature, pH, and contact time optimized to achieve effective material isolation with minimal environmental impact. The pulping stage uses specific chemical agents at controlled concentrations and temperatures to separate cellulose and polyester while minimizing harmful byproducts and waste.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The process converts potentially harmful chemical treatments into beneficial separation mechanisms. Chemical agents that could be considered harmful are applied in controlled amounts and conditions to achieve efficient material isolation, with subsequent steps neutralizing or recovering these chemicals, thereby transforming potential environmental harm into effective processing capability.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables the transformation of reclaimed textiles into high-quality regenerated fibers, reducing waste, conserving resources, and lowering environmental impact while producing fibers with customizable properties.

Implementation Method 1

pulping/dissolution stages to isolate cellulose and polyester polymers

Methodology Applied
Scientific EffectDissolution: Solvation

Implementation Method 2

enzymatic processes to minimize environmental impact

Methodology Applied
Scientific EffectEnzymatic breakdown: Enzyme

Implementation Method 3

high temperature aqueous washing

Methodology Applied
Scientific EffectThermal energy transfer: Heating

Implementation Method 4

high temperature aqueous washing

Methodology Applied
Scientific EffectWashing: Absorption (physical)

Implementation Method 5

supercritical CO2 treatment

Methodology Applied
Scientific EffectSupercritical fluid extraction: Supercritical Fluid Extraction

Implementation Method 6

extrusion to form regenerated fibers

Methodology Applied
Scientific EffectPressure-driven flow: Pressure Gradient

Implementation Method 7

extrusion to form regenerated fibers

Methodology Applied
Scientific EffectExtrusion: Extrusion

Data Source

PatentUS20230124761A1Methods and systems for processing mixed textile feedstock, isolating constituent molecules, and regenerating cellulosic and polyester fibers
Publication Date: 2023.04.20 EVRNU SPC
  • US20230124761A1 patent drawing
  • US20230124761A1 patent drawing
  • US20230124761A1 patent drawing

AI summary

Methods and systems of the present invention use mixed textile feedstock, which may include post-consumer waste garments, scrap fabric and/or other textile materials as a raw feed material to produce isolated cellulose and other isolated molecules having desirable properties that can be used and be used in the textile and apparel industries, and in other industries. A multi-stage process is provided, in which mixed textile feed material is subjected to one or more pretreatment stages, followed by at least two pulping treatments for isolating cellulose molecules and other molecular constituents, such as polyester. The isolated cellulose and polyester molecules may be used in a variety of downstream applications. In one application, isolated cellulose and polyester molecules are extruded to provide regenerated cellulose fibers and regenerated polyester fibers having desirable (and selectable) properties that are usable in various industrial applications, including textile production.