Continuous Mixing Kneader for Counterflow Extraction of Superabsorbent Polymers

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Solution Overview

Problem

Current methods for drying superabsorbent polymers are inefficient and energy-intensive, particularly in batch processes, and mixing kneaders lack effective continuous extraction capabilities for separating components from complex mixtures.

Innovation Solution

A continuous mixing kneader design with counterflow extraction, utilizing a shaft with kneading elements and separate input and discharge devices for extraction material and extractant, enables efficient separation of components by comminution and mechanical separation, allowing for the use of an extractant to dissolve or modify the component of interest within the kneader.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of energy

If batch process drying with extractant is used for superabsorbent polymer, then extraction can be performed, but energy consumption is high and processing efficiency is low

Engineering Contradiction:
Improveenergy consumptionVSAvoidprocessing efficiency
Core Design Contradiction:
Loss of energyVSProductivity

Solution Approach 1:

The patent implements continuous extraction and drying processes replacing batch operations. The mixing kneader continuously processes superabsorbent polymer material while extractant circulates through the system, enabling uninterrupted operation that simultaneously improves energy efficiency and processing throughput compared to intermittent batch drying.

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The patent replaces conventional thermal drying mechanisms with mechanical extraction using a mixing kneader system. The kneader uses mechanical agitation and counter-current flow of extractant to remove water and solvents, substituting energy-intensive thermal processes with mechanical separation that consumes less energy while maintaining high productivity.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Adaptability or versatility

If conventional mixing kneader design is used, then mixing function is provided, but continuous extraction capability is insufficient

Engineering Contradiction:
Improveextraction capabilityVSAvoidkneader design
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The mixing kneader is designed to perform multiple functions simultaneously: mixing, kneading, and continuous extraction. The device integrates extractant injection systems, counter-current flow paths, and separation mechanisms within the kneader structure, allowing a single unit to handle both mechanical processing and chemical extraction operations that were previously required from separate equipment.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The kneader is divided into functional zones including material input sections, extractant injection points, mixing chambers, and discharge areas. This segmentation allows independent optimization of each zone for its specific function while maintaining overall system integration, enabling complex extraction capabilities through modular functional divisions.

Inventive Principle:
Principle #1Segmentation

3Loss of energy

If bound water is removed from superabsorbent polymer, then drying is achieved, but energy consumption increases and polymer structure may be damaged

Engineering Contradiction:
Improvedrying energyVSAvoidpolymer structure integrity
Core Design Contradiction:
Loss of energyVSReliability

Solution Approach 1:

The patent changes the physical-chemical parameters of water removal by using extractants that alter the boiling point and evaporation characteristics of bound water. By replacing water with extractants having different volatility profiles, the drying process occurs at lower temperatures or under milder conditions that preserve polymer structure while reducing energy requirements compared to conventional high-temperature drying.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

Extractants serve as intermediary substances that facilitate water removal from the polymer matrix. The extractant molecules intercalate between polymer chains, solvate bound water, and enable its gentle removal through controlled evaporation or phase separation, acting as a mediator that protects polymer structure during the drying process while consuming less energy than direct thermal drying.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables efficient and energy-efficient continuous extraction and drying of superabsorbent polymers, improving absorption rates and reducing energy consumption by replacing bound water with ethanol, which facilitates easier removal and maintains the polymer's porous structure.

Implementation Method 1

with the aid of an extractant, at least one component is dissolved from an extraction material

Methodology Applied
Scientific EffectDissolution: Solvation

Implementation Method 2

the term 'extraction' is also intended to cover methods in which the component to be extracted undergoes a chemical reaction, i.e. for example is chemically modified by the extractant

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 3

the shaft structures of the at least one shaft are configured to mesh, during operation, with the shaft structures of at least one second shaft... The extraction material is comminuted by the shaft structures

Methodology Applied
Scientific EffectMechanical comminution: Mechanical Force

Implementation Method 4

a dome (18) arranged above the working space (2)... The extract solution is discharged from the dome (18) via a second discharge device (5)

Methodology Applied
Scientific EffectGravitational separation: Gravitation

Data Source

PatentUS20240408512A1Mixing kneader and method for carrying out an extraction
Publication Date: 2024.12.12 LIST TECHNOLOGY AG
  • US20240408512A1 patent drawing
  • US20240408512A1 patent drawing
  • US20240408512A1 patent drawing

AI summary

Mixing kneader (1) for carrying out a continuous extraction in which, with the aid of an extractant, at least one component is released from an extraction material, the mixing kneader (1) comprising a working space (2), at least one shaft (14) extending in the working space (2), the at least one shaft (14) comprising shaft superstructures (11, 12, 29) in the form of kneading elements, wherein the shaft superstructures (11, 12, 29) of the at least one shaft (14) are configured to mesh during operation with the shaft superstructures (11, 12, 29) of at least one second shaft (14) or with stationary kneading elements (17) present in the mixing kneader (1), a first feed device (4) for feeding the extraction material into the mixing kneader (1), and a first discharge device (3) which lies substantially opposite the first feed device (4) and discharges the extraction residue, is intended to be characterized by a second feed device (6) for feeding the extractant, wherein this second feed device (6) is arranged substantially opposite the first feed device (4), further characterized by a second discharge device (5) for discharging the extract solution, wherein the second discharge device (5) is arranged substantially opposite the first discharge device (3), wherein the second discharge device (5) comprises a device for mechanical separation.