Modified AlN Source for Downfall Prevention in Face-Up Crystal Growth

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Solution Overview

Problem

The challenge of growing high-quality aluminum nitride (AlN) single crystals with large diameters is hindered by anisotropic growth, thermal expansion coefficient differences with SiC substrates leading to cracks, and the face-down method causing substrate deflection and downfall during crystal growth.

Innovation Solution

A modified aluminum nitride source with specific bulk density and porosity, manufactured through heat treatment and etching, is used in a face-up method to suppress downfall and defects during crystal growth.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If a face-down method is used for AlN crystal growth, then the substrate can be supported, but the substrate deflects and damages due to weight

Engineering Contradiction:
Improvesubstrate supportVSAvoidsubstrate integrity
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The patent inverts the conventional face-down growth method to a face-up method, where the substrate is positioned with its growth surface facing upward. This inversion eliminates substrate deflection and damage caused by weight while enabling stable large-diameter crystal growth without mechanical failure

Inventive Principle:
Principle #13The other way round (Inversion)

2Reliability

If the AlN source is positioned above the substrate in face-up method, then substrate deflection is prevented, but the source adheres to the substrate causing downfall

Engineering Contradiction:
Improvesubstrate stabilityVSAvoidsource downfall
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent modifies physical parameters of the AlN source including bulk density (2.0-3.0 g/cm³) and open porosity (5-20%), and controls particle size distribution (d10, d50, d90 values) to prevent source material from adhering to the substrate while maintaining stability in the face-up configuration

Inventive Principle:
Principle #35Parameter changes

3Area of stationary object

If AlN single crystal wafer diameter is increased, then large-diameter substrate is obtained, but anisotropic growth limits quality

Engineering Contradiction:
Improvewafer diameterVSAvoidcrystal quality
Core Design Contradiction:
Area of stationary objectVSManufacturing precision

Solution Approach 1:

The patent inverts the growth configuration to face-up method, which enables simultaneous achievement of large wafer diameter (6 inches or more) and high crystal quality by preventing substrate deflection and source downfall that previously limited scaling

Inventive Principle:
Principle #13The other way round (Inversion)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method enables the production of high-quality AlN single crystals with reduced defects by minimizing substrate deflection and polycrystallization, facilitating large-diameter crystal growth.

Implementation Method 1

a heat treatment step of heat treating an aluminum nitride source to produce an aluminum nitride sintered body

Methodology Applied
Scientific EffectHeat treatment: Heat Treatment

Implementation Method 2

an etching step of etching the aluminum nitride sintered body

Methodology Applied
Scientific EffectEtching:

Data Source

PatentUS12398038B2Manufacturing method of modified aluminum nitride raw material, modified aluminum nitride raw material, manufacturing method of aluminum nitride crystals, and downfall defect prevention method
Publication Date: 2025.08.26 TOYO ALUMINIUM KK
  • US12398038B2 patent drawing
  • US12398038B2 patent drawing
  • US12398038B2 patent drawing

AI summary

The purpose of the present is to provide a modified AlN source for suppressing downfall defects. This manufacturing method of a modified aluminum nitride source involves a heat treatment step for heat treating an aluminum nitride source and generating an aluminum nitride sintered body.