Monk Fruit Juice Purification Using Ion Exchange Resins

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Solution Overview

Problem

Existing methods for producing sweet juice compositions from terpene glycoside-containing fruits like monk fruit result in undesirable flavors, stability issues, and significant loss of mogrosides, making them unsuitable for widespread use.

Innovation Solution

A method involving the use of cation and anion exchange resins, where the juice from these fruits is first clarified and then contacted with a cation exchange resin followed by an anion exchange resin, to produce a sweet juice composition that retains at least 60% of mogroside V, minimizing the absorption of mogroside V while removing compounds contributing to off-flavors.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-affected harmful factors

If existing methods are used to remove off-flavor components from monk fruit juice, then off-flavors are reduced, but significant amounts of mogrosides are also removed

Engineering Contradiction:
Improveoff-flavorsVSAvoidmogrosides
Core Design Contradiction:
Object-affected harmful factorsVSLoss of substance

Solution Approach 1:

The patent uses an adsorption resin as an intermediary substance that selectively binds to off-flavor components (grassy, earthy, bitter compounds) while allowing mogrosides to pass through. This mediator enables the separation of harmful substances from valuable sweet compounds without direct contact between them, resolving the contradiction between removing off-flavors and retaining mogrosides

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent changes the chemical and physical parameters of the juice processing system by adjusting pH levels, using enzymatic treatment to break down problematic compounds, and controlling temperature during concentration. These parameter changes enable selective removal of off-flavor components while preserving mogrosides, as the parameters are optimized to affect harmful substances differently than the stable mogroside molecules

Inventive Principle:
Principle #35Parameter changes

2Duration of action of stationary object

If monk fruit is dried for preservation, then shelf life is extended, but undesirable bitter and astringent flavors form

Engineering Contradiction:
Improveshelf lifeVSAvoidbitter and astringent flavors
Core Design Contradiction:
Duration of action of stationary objectVSObject-affected harmful factors

Solution Approach 1:

The patent replaces the traditional thermal drying process with a cold concentration process using reverse osmosis and vacuum concentration. This substitution eliminates the high temperatures that cause Maillard reactions and formation of bitter, astringent flavors, while still achieving preservation and extended shelf life through controlled concentration and sterile packaging

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent utilizes phase transition principles by using vacuum concentration to lower the boiling point of water, allowing juice concentration at temperatures below 60°C. This prevents thermal degradation and flavor deterioration while still achieving water removal for preservation. The reverse osmosis process also uses phase separation principles to concentrate the juice without heat application

Inventive Principle:
Principle #36Phase transitions

3Quantity of substance

If existing sweet juice compositions are produced, then sweetness is achieved, but color stability and overall stability are poor

Engineering Contradiction:
ImprovesweetnessVSAvoidcolor stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The patent applies preliminary enzymatic treatment and filtration to remove unstable compounds, pectin, and suspended particles before concentration and packaging. By addressing potential stability issues in advance through enzyme addition and clarification steps, the final product achieves superior color stability and shelf life without compromising sweetness

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent replaces traditional high-heat concentration methods with low-temperature vacuum concentration and reverse osmosis. This substitution prevents thermal oxidation and Maillard reactions that cause browning and color instability, while preserving the sweetness-active mogrosides. The gentle concentration process maintains color stability throughout storage

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces a sweet juice composition with a clean flavor profile and improved stability, retaining a significant amount of mogroside V, thus addressing the limitations of existing techniques.

Implementation Method 1

contacting the juice with the cation exchange resin and the anion exchange resin

Methodology Applied
Scientific EffectIon exchange: Ion Exchange

Implementation Method 2

contacting the juice with the cation exchange resin and the anion exchange resin

Methodology Applied
Scientific EffectIon exchange: Ion Exchange

Data Source

PatentEP3138412B1Methods of producing sweet juice compositions
Publication Date: 2019.05.22 GUILIN GFS MONK FRUIT CORP
  • EP3138412B1 patent drawingFigure 1
  • EP3138412B1 patent drawingFigure 2

AI summary

The present disclosure relates to methods of producing a sweet juice composition from monk fruit and other fruit of the Cucurbitaceae family containing mogroside V and other terpene glycosides. The methods employ a cation exchange resin and an anion exchange resin to obtain a sweet juice composition with a clean flavor. The sweet juice composition can be used in a food, beverage, pharmaceutical or dietary supplement product.