Monocrystal Growth H/R Ratio Control for Dislocation Inhibition

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Solution Overview

Problem

The existing methods for manufacturing monocrystals, such as those used for power MOS transistors, fail to adequately inhibit dislocation and maintain low resistivity, as the convection flow in the dopant-added melt leads to abnormal growth and dislocation issues.

Innovation Solution

Optimizing the amount of dopant-added melt in the crucible by controlling the distance from the lowermost portion to the top surface (H/R ratio) between 0.4 and 0.78, thereby stabilizing the melt temperature and reducing dislocation, while ensuring the resistivity at the upper end of the straight body remains at 1.0 mΩ·cm or less.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If the amount of dopant-added melt is increased, then the resistivity can be maintained at low levels, but the convection flow is strengthened causing abnormal growth and dislocation

Engineering Contradiction:
Improvedislocation inhibitionVSAvoidamount of dopant-added melt
Core Design Contradiction:
Manufacturing precisionVSQuantity of substance

Solution Approach 1:

The invention optimizes the H/R ratio parameter (distance from lowermost portion to top surface divided by top surface radius) to control convection flow intensity. By setting H/R within 0.4 to 0.78, the patent achieves stable temperature distribution that prevents abnormal growth and dislocation while maintaining low resistivity, resolving the contradiction between melt quantity and manufacturing precision

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies preliminary control of the H/R ratio before crystal growth begins to prevent convection-induced abnormalities. By pre-establishing the optimal melt configuration, the invention prevents abnormal growth and dislocation from occurring in the first place, rather than correcting them after they appear

Inventive Principle:
Principle #9Preliminary anti-action

2Temperature

If the H/R ratio is increased, then the convection flow is strengthened which can deliver heat upward, but this causes temperature fluctuation and abnormal growth

Engineering Contradiction:
Improvemelt temperature distributionVSAvoidtemperature stability
Core Design Contradiction:
TemperatureVSStability of the object's composition

Solution Approach 1:

The invention identifies and optimizes the H/R ratio as a critical parameter for temperature stability. By constraining H/R to the range of 0.4 to 0.78, the patent achieves stable temperature distribution in the melt that prevents abnormal growth, directly resolving the temperature stability issue

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If the apex angle of the shoulder is adjusted to 40-60 degrees, then dislocation occurrence can be inhibited, but this alone is insufficient to prevent abnormal growth in dopant-added melts

Engineering Contradiction:
Improvedislocation inhibitionVSAvoidprocess parameter requirements
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The invention combines multiple control parameters (H/R ratio and shoulder apex angle) into a unified approach. By merging the optimization of H/R ratio with the established shoulder angle requirements, the patent achieves comprehensive dislocation inhibition and abnormal growth prevention that neither parameter alone can accomplish

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively inhibits dislocation and maintains low resistivity in the monocrystal, allowing for the production of high-quality silicon wafers with reduced abnormal growth and improved manufacturing efficiency.

Implementation Method 1

a convection flow seems to be occurring in a dopant-added melt received in a crucible by a temperature difference between a part of the melt positioned at a lowermost portion of the crucible and a top surface of the melt

Methodology Applied
Scientific EffectConvection: Convection

Implementation Method 2

convection flow seems to be occurring in a dopant-added melt received in a crucible by a temperature difference between a part of the melt positioned at a lowermost portion of the crucible and a top surface of the melt

Methodology Applied
Scientific EffectNatural convection: Free Convection

Data Source

PatentUS10329686B2Method for producing single crystal
Publication Date: 2019.06.25 SUMCO CORP
  • US10329686B2 patent drawing
  • US10329686B2 patent drawing
  • US10329686B2 patent drawing

AI summary

A manufacturing method of a monocrystal includes: a shoulder-formation step to form a shoulder of the monocrystal; and a straight-body-formation step to form a straight body of the monocrystal, in which, in the shoulder-formation step, providing that a distance from a lowermost portion inside the crucible to a top surface of the dopant-added melt is defined as H (mm) and a radius of the top surface of the dopant-added melt is defined as R (mm), the shoulder starts to be formed in a condition that a relationship of 0.4<H/R<0.78 is satisfied.